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雷公藤提取物溶解性能的研究 被引量:3
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作者 管咏梅 张霄潇 +3 位作者 朱卫丰 杨明 乐西薇 乐志燕 《中成药》 CAS CSCD 北大核心 2008年第4期501-504,共4页
目的:考察雷公藤提取物及其指标成分雷公藤甲素在透皮制剂常用试剂中的溶解情况,研究在各溶剂中提取物溶解情况、指标成分溶解情况以及雷公藤提取物分散情况三者的关系。方法:运用沉淀法、指标成分含量测定法、粒径法对提取物溶解量、... 目的:考察雷公藤提取物及其指标成分雷公藤甲素在透皮制剂常用试剂中的溶解情况,研究在各溶剂中提取物溶解情况、指标成分溶解情况以及雷公藤提取物分散情况三者的关系。方法:运用沉淀法、指标成分含量测定法、粒径法对提取物溶解量、指标成分溶解量以及混悬液粒径进行测定。结果:①对提取物的溶解能力为:无水乙醇>异丙醇>油酸>肉豆蔻酸异丙酯>水>甘油;②对指标成分的溶解能力为:无水乙醇>异丙醇>油酸>肉豆蔻酸异丙酯>水>甘油;③混悬液粒径为:肉豆蔻酸异丙酯>油酸>无水乙醇>异丙醇。结论:①提取物溶解性能变化趋势与指标成分溶解性能变化趋势相同;②混悬液的粒径变化趋势与提取物溶解性能变化趋势基本呈反相关。 展开更多
关键词 雷公藤提取物 溶解性能 雷公藤甲素 粒径测定 混悬液 HPLC
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Growth of metallic iron particles during reductive roasting of boron-bearing magnetite concentrate 被引量:4
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作者 ZHANG Xin LI Guang-hui +5 位作者 RAO Ming-jun MI Huan-peng LIANG Bin-jun YOU Jin-xiang PENG Zhi-wei JIANG Tao 《Journal of Central South University》 SCIE EI CAS CSCD 2020年第5期1484-1494,共11页
The growing characteristics of metallic iron particles during reductive roasting of boron-bearing magnetite concentrate under different conditions were investigated.The size of the metallic iron particles was quantita... The growing characteristics of metallic iron particles during reductive roasting of boron-bearing magnetite concentrate under different conditions were investigated.The size of the metallic iron particles was quantitatively measured via optical image analysis with consideration of size calibration and weighted ratio of image numbers in the core,middle and periphery zones of cross-section of pellets.In order to guarantee the measurement accuracy,54 images were captured in total for each specimen,with a weighted ratio of 1:7:19 with respect to the core,middle and periphery section of the cross-section of pellets.Increasing reduction temperature and time is favorable to the growth of metallic iron particles.Based on the modification of particle size measurement,in terms of time(t)and temperature(T)a predicting model of metallic iron particle size(D),was established as:D=125−0.112t−0.2352T−5.355×10^−4t^2+2.032×10^−4t∙T+1.134×10^−4T^2. 展开更多
关键词 ludwigite ore reductive roasting metallic iron grain growth size measurement
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