The paper reports the method applieable for determination of traces of mercury in 2.0mol·L -1 HCl 1.5 mol·L -1 NaCl 1.0μg·ml -1 Cd 2+ medium with differential pulse anoldic stripping voltammetry.Stripp...The paper reports the method applieable for determination of traces of mercury in 2.0mol·L -1 HCl 1.5 mol·L -1 NaCl 1.0μg·ml -1 Cd 2+ medium with differential pulse anoldic stripping voltammetry.Stripping peak and concentration of Hg is linear in range of 0.50～100ng·ml -1 when the deposition time is 5min.The relative standard deviation of 4.0ng·ml -1 Hg 2+ is 8.87% while n=8.After enrichment and separation of Hg in synthetic samples is obtained by using a microcolumn of sulfhydry cotton,the average recovery is about 80%.展开更多
基金financially supported by Natural Science Foundation of Daton(No.2019168,No.201819)Natural Science Foundation of Shanxi Province(No.201701D121016)research funds of Innovation&Application Engineering Research Center for Mesoporous Materials of Shanxi Province(No.MMIA2019105).
文摘The paper reports the method applieable for determination of traces of mercury in 2.0mol·L -1 HCl 1.5 mol·L -1 NaCl 1.0μg·ml -1 Cd 2+ medium with differential pulse anoldic stripping voltammetry.Stripping peak and concentration of Hg is linear in range of 0.50～100ng·ml -1 when the deposition time is 5min.The relative standard deviation of 4.0ng·ml -1 Hg 2+ is 8.87% while n=8.After enrichment and separation of Hg in synthetic samples is obtained by using a microcolumn of sulfhydry cotton,the average recovery is about 80%.
