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石灰岩中游离二氧化硅化学物相分析方法的标准化研究 被引量:11
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作者 韩秀卿 《岩矿测试》 CAS CSCD 北大核心 2000年第4期259-263,共5页
介绍了石灰岩中游离二氧化硅的化学物相分析方法。选择磷酸溶矿 ,再以氟硼酸解聚已溶出的硅酸 ,使游离二氧化硅与其他矿物分离 ,再用重量法进行测定 ,并按GB 6379- 86测试方法的精密度 ,通过实验室间试验确定标准测试方法的重复性和再... 介绍了石灰岩中游离二氧化硅的化学物相分析方法。选择磷酸溶矿 ,再以氟硼酸解聚已溶出的硅酸 ,使游离二氧化硅与其他矿物分离 ,再用重量法进行测定 ,并按GB 6379- 86测试方法的精密度 ,通过实验室间试验确定标准测试方法的重复性和再现性。通过取样、制样、样品均匀性检查、精密度试验等步骤 。 展开更多
关键词 游离二氧化硅 化学物相分析方法 碳岩矿床
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鸡蛋中氟苯尼考残留的AlphaLISA检测方法的建立
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作者 孙志文 王忠 +5 位作者 于莹 赵营 张晶晶 魏紫嫣 方芳 马立才 《中国兽医杂志》 北大核心 2025年第4期11-19,共9页
本试验旨在建立可检测鸡蛋中氟苯尼考(FF)残留的均相光激化学发光免疫分析方法(AlphaLISA)。通过化学方法合成FF生物素半抗原,利用O-羧甲基羟胺法偶联FF抗体与受体微球,通过筛选确定鸡蛋样品稀释倍数,采用棋盘法确定FF抗体标记受体微球... 本试验旨在建立可检测鸡蛋中氟苯尼考(FF)残留的均相光激化学发光免疫分析方法(AlphaLISA)。通过化学方法合成FF生物素半抗原,利用O-羧甲基羟胺法偶联FF抗体与受体微球,通过筛选确定鸡蛋样品稀释倍数,采用棋盘法确定FF抗体标记受体微球和FF生物素半抗原的浓度,最后基于FF抗体标记受体微球、FF生物素半抗原和链霉亲和素修饰供体微球,优化建立了检测鸡蛋中FF残留的AlphaLISA检测方法,并评价其灵敏度、特异性、准确性和重复性,及与国家标准方法GB 31658.20—2022《动物性食品中酰胺醇类药物及其代谢物残留量的测定液相色谱-串联质谱法》的一致性。质谱分析结果显示,FF生物素半抗原与目标分子的分子量一致(636 Da)。经评估,鸡蛋样品离心上清液采用25倍稀释方案。建立的AlphaLISA方法对鸡蛋中FF的检测限为0.57μg/kg,定量限为0.92μg/kg;添标回收率介于87.00%~99.50%,日内和日间变异系数均低于5%;与氟苯尼考胺的交叉反应率较高(93.27%),与12种常见兽药的交叉反应率极低(<0.1%);与国家标准方法比较,2种方法在5个添加浓度点的检测结果高度一致(R2=0.997)。结果表明,本试验建立的AlphaLISA具有高灵敏度、准确性、重复性和操作简便等优点,适用于鸡蛋中FF残留的快速检测,为鸡蛋安全监测提供了高效且可行的方案。 展开更多
关键词 鸡蛋 氟苯尼考 光激化学发光免疫分析方法(AlphaLISA) 半抗原
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沉积相的一些术语定义的新思考:基于迈尔(Miall,1985)的文章 被引量:2
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作者 冯增昭 《古地理学报》 CAS CSCD 北大核心 2022年第2期I0001-I0008,共8页
近年来,《古地理学报》(中文版及英文版)连续收到一些来稿,其作者根据迈尔(Miall,1985)文章的观点和方法,把他们研究地区碎屑岩剖面中的每个岩层中的岩石挑出来,归纳出一些岩石类型,如砾岩、砂岩、细粒岩等,并称它们为岩相(lithofacies... 近年来,《古地理学报》(中文版及英文版)连续收到一些来稿,其作者根据迈尔(Miall,1985)文章的观点和方法,把他们研究地区碎屑岩剖面中的每个岩层中的岩石挑出来,归纳出一些岩石类型,如砾岩、砂岩、细粒岩等,并称它们为岩相(lithofacies)。这不符合沉积相的定义。我曾写过几篇文章,即冯增昭(2018,2020)及Feng(2019),指出这些问题,希望国内外的作者、尤其是国内的作者,不再继续盲目地引用和传播迈尔(1985)文章的观点和方法。迈尔是第1个称岩石(实际上是沉积物)为岩相的人,他的观点和他提出的相分析方法误导了沉积相的正确定义及正常的相分析方法。本文主要讨论迈尔(Miall,1985)文章中的问题,即他把沉积物当作岩相并用岩相分析相。不讨论他文章的贡献及建筑单元中的一些术语欠严谨的问题。在这里,必须申明,本文中的相,是沉积岩石学中的相,不是火成岩岩石学、变质岩岩石学、古生物学、地层学、地球物理学、地球化学等地质学分支学科中的相。岩相、相和沉积相是同义的术语。当然,这些术语的定义是有争议的,希望遵循“百花齐放和百家争鸣”的方针和地质实践,逐步地解决这些争议。 展开更多
关键词 岩石 沉积物 沉积环境 沉积 岩性 相分析方法 百花齐放和百家争鸣 地质实践
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电涡流相位梯度及其在导电材料缺陷识别中的应用 被引量:7
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作者 张荣华 叶松 +2 位作者 马明 赵倩 王化祥 《仪器仪表学报》 EI CAS CSCD 北大核心 2018年第10期134-141,共8页
使用空间域相频谱分析方法,将相位梯度作为缺陷检测信号特征量,对不同类型的缺陷进行检测和分类。数字相敏解调技术用于提取检测信号的相位梯度。采用双空气芯线圈涡流传感器并施加1-10 kHz多频激励信号,对平板金属样件进行表面缺陷、... 使用空间域相频谱分析方法,将相位梯度作为缺陷检测信号特征量,对不同类型的缺陷进行检测和分类。数字相敏解调技术用于提取检测信号的相位梯度。采用双空气芯线圈涡流传感器并施加1-10 kHz多频激励信号,对平板金属样件进行表面缺陷、下表面缺陷、内部缺陷的识别及分类。实验结果证明,实验系统可以有效地检测出缺陷,并通过空间域相频谱分析得到可视化检测结果,采用相位梯度作为特征量有效抑制了提离噪声对检测结果的影响。 展开更多
关键词 涡流检测 空间域频谱分析方法 敏解调 位梯度 缺陷分类
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基于复合信息空间的语音识别训练系统研究
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作者 耿睿 崔德光 《计算机工程与应用》 CSCD 北大核心 2002年第1期82-84,共3页
首先介绍了复杂系统、复合信息空间等相关知识,在此基础上提出一种在复合信息空间中基于知识的、定性与定量相结合的分析方法,并结合一个语音识别训练系统的实例对这种方法的应用进行详细介绍。
关键词 复杂系统 复合信息空间 基于知识的 定性与定量结合的分析方法 定性分析方法 定量分析方法
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Temporal-spatial cross-correlation analysis of non-stationary near-surface wind speed time series 被引量:3
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作者 ZENG Ming LI Jing-hai +1 位作者 MENG Qing-hao ZHANG Xiao-nei 《Journal of Central South University》 SCIE EI CAS CSCD 2017年第3期692-698,共7页
Temporal-spatial cross-correlation analysis of non-stationary wind speed time series plays a crucial role in wind field reconstruction as well as in wind pattern recognition.Firstly,the near-surface wind speed time se... Temporal-spatial cross-correlation analysis of non-stationary wind speed time series plays a crucial role in wind field reconstruction as well as in wind pattern recognition.Firstly,the near-surface wind speed time series recorded at different locations are studied using the detrended fluctuation analysis(DFA),and the corresponding scaling exponents are larger than 1.This indicates that all these wind speed time series have non-stationary characteristics.Secondly,concerning this special feature( i.e.,non-stationarity)of wind signals,a cross-correlation analysis method,namely detrended cross-correlation analysis(DCCA) coefficient,is employed to evaluate the temporal-spatial cross-correlations between non-stationary time series of different anemometer pairs.Finally,experiments on ten wind speed data synchronously collected by the ten anemometers with equidistant arrangement illustrate that the method of DCCA cross-correlation coefficient can accurately analyze full-scale temporal-spatial cross-correlation between non-stationary time series and also can easily identify the seasonal component,while three traditional cross-correlation techniques(i.e.,Pearson coefficient,cross-correlation function,and DCCA method) cannot give us these information directly. 展开更多
关键词 temporal-spatial cross-correlation near-surface wind speed time series detrended cross-correlation analysis (DCCA) cross-correlation coefficient Pearson coefficient cross-correlation function
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Nonlinear finite-element-based structural system failure probability analysis methodology for gravity dams considering correlated failure modes 被引量:5
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作者 胡江 马福恒 吴素华 《Journal of Central South University》 SCIE EI CAS CSCD 2017年第1期178-189,共12页
The structural system failure probability(SFP) is a valuable tool for evaluating the global safety level of concrete gravity dams.Traditional methods for estimating the failure probabilities are based on defined mathe... The structural system failure probability(SFP) is a valuable tool for evaluating the global safety level of concrete gravity dams.Traditional methods for estimating the failure probabilities are based on defined mathematical descriptions,namely,limit state functions of failure modes.Several problems are to be solved in the use of traditional methods for gravity dams.One is how to define the limit state function really reflecting the mechanical mechanism of the failure mode;another is how to understand the relationship among failure modes and enable the probability of the whole structure to be determined.Performing SFP analysis for a gravity dam system is a challenging task.This work proposes a novel nonlinear finite-element-based SFP analysis method for gravity dams.Firstly,reasonable nonlinear constitutive modes for dam concrete,concrete/rock interface and rock foundation are respectively introduced according to corresponding mechanical mechanisms.Meanwhile the response surface(RS) method is used to model limit state functions of main failure modes through the Monte Carlo(MC) simulation results of the dam-interface-foundation interaction finite element(FE) analysis.Secondly,a numerical SFP method is studied to compute the probabilities of several failure modes efficiently by simple matrix integration operations.Then,the nonlinear FE-based SFP analysis methodology for gravity dams considering correlated failure modes with the additional sensitivity analysis is proposed.Finally,a comprehensive computational platform for interfacing the proposed method with the open source FE code Code Aster is developed via a freely available MATLAB software tool(FERUM).This methodology is demonstrated by a case study of an existing gravity dam analysis,in which the dominant failure modes are identified,and the corresponding performance functions are established.Then,the dam failure probability of the structural system is obtained by the proposed method considering the correlation relationship of main failure modes on the basis of the mechanical mechanism analysis with the MC-FE simulations. 展开更多
关键词 gravity dam structural system failure probability nonlinear finite element response surface method computational platform
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Multi-attributed decision making for mining methods based on grey system and interval numbers 被引量:8
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作者 刘浪 陈建宏 +1 位作者 王革民 劳德正 《Journal of Central South University》 SCIE EI CAS 2013年第4期1029-1033,共5页
In the case of unknown weights, theories of multi-attributed decision making based on interval numbers and grey related analysis were used to optimize mining methods. As the representative of independence for the indi... In the case of unknown weights, theories of multi-attributed decision making based on interval numbers and grey related analysis were used to optimize mining methods. As the representative of independence for the indicator, the smaller the correlation of indicators is, the greater the weight is. Hence, the weights of interval numbers of indicators were determined by using correlation coefficient. Relative closeness based on positive and negative ideal methods was calculated by introducing distance between interval numbers, which made decision making more rational and comprehensive. A new method of ranking interval numbers based on normal distribution was proposed for the optimization of mining methods, whose basic properties were discussed. Finally, the feasibility and effectiveness of this method were verified by theories and practice. 展开更多
关键词 mining method interval number multi-attributed decision making grey related analysis correlation coefficient normaldistribution RANKING
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Vari-gram language model based on word clustering
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作者 袁里驰 《Journal of Central South University》 SCIE EI CAS 2012年第4期1057-1062,共6页
Category-based statistic language model is an important method to solve the problem of sparse data.But there are two bottlenecks:1) The problem of word clustering.It is hard to find a suitable clustering method with g... Category-based statistic language model is an important method to solve the problem of sparse data.But there are two bottlenecks:1) The problem of word clustering.It is hard to find a suitable clustering method with good performance and less computation.2) Class-based method always loses the prediction ability to adapt the text in different domains.In order to solve above problems,a definition of word similarity by utilizing mutual information was presented.Based on word similarity,the definition of word set similarity was given.Experiments show that word clustering algorithm based on similarity is better than conventional greedy clustering method in speed and performance,and the perplexity is reduced from 283 to 218.At the same time,an absolute weighted difference method was presented and was used to construct vari-gram language model which has good prediction ability.The perplexity of vari-gram model is reduced from 234.65 to 219.14 on Chinese corpora,and is reduced from 195.56 to 184.25 on English corpora compared with category-based model. 展开更多
关键词 word similarity word clustering statistical language model vari-gram language model
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