Based on the steady-state strain measured by single-pass hot compression tests,the method by a double-pass hot compression testing was developed to measure the metadynamic-recrystallization kinetics.The metadynamic re...Based on the steady-state strain measured by single-pass hot compression tests,the method by a double-pass hot compression testing was developed to measure the metadynamic-recrystallization kinetics.The metadynamic recrystallization behavior of low-alloy steel Q345B during hot compression deformation was investigated in the temperature range of 1 000-1 100℃,the strain rate range of 0.01-0.10 s -1 and the interpass time range of 0.5-50 s on a Gleeble-3500 thermo-simulation machine.The results show that metadynamic recrystallization during the interpass time can be observed.As the deformation temperature and strain rate increase,softening caused by metadynamic recrystallization is obvious.According to the data of thermo-simulation,the metadynamic recrystallization activation energy is obtained to be Qmd=100.674 kJ/mol and metadynamic recrystallization kinetics model is set up.Finally,the error analysis of metadynamic recrystallization kinetics model proves that the model has high accuracy(correlation coefficient R=0.988 6).展开更多
The plastic deformation simulation of AZ31 magnesium alloy at different elevated temperatures （from 473 to 723 K） was performed on Gleeble-1500 thermal mechanical simulator at the strain rates of 0.01, 0.1, 1, 5 and...The plastic deformation simulation of AZ31 magnesium alloy at different elevated temperatures （from 473 to 723 K） was performed on Gleeble-1500 thermal mechanical simulator at the strain rates of 0.01, 0.1, 1, 5 and 10 s-t and the maximum deformation degree of 80%. The relationship between the flow stress and deformation temperature as well as strain rate was analyzed. The materials parameters and the apparent activation energy were calculated. The constitutive relationship was established with a Zener-Hollomon （Z） parameter. The results show that the flow stress increases with the increase of strain rate at a constant temperature, but it decreases with the increase of deformation temperature at a constant strain rate. The apparent activation energy is estimated to be 129-153 kJ/mol, which is close to that for self-diffusion of magnesium. The established constitutive relationship can reflect the change of flow stress during hot deformation.展开更多
Q345E as one of typical low alloy steels is widely used in manufacturing basic components in many fields because of its eminent formability under elevated temperature. In this work, the deformation behavior of Q345E s...Q345E as one of typical low alloy steels is widely used in manufacturing basic components in many fields because of its eminent formability under elevated temperature. In this work, the deformation behavior of Q345E steel was investigated by hot compression experiments on Gleeble-3500 thermo-mechanical simulator with the temperature ranging from 850 ℃ to 1150 ℃ and strain rate ranging from 0.01 s-1 to 10 s-1. The experimental results indicate that dynamic softening of Q345E benefits from increasing deformation temperature and decreasing strain rate. The mathematical relationship between dynamic softening degree and deformation conditions is established to predict the dynamic softening degree quantitatively, which is further proved by some optical microstructures of Q345E. In addition, the experimental results also reveal that the stress level decreases with increasing deformation temperature and decreasing strain rate. The constitutive equation for flow stress of Q345E is formulated by Arrihenius equation and the modified Zener-Hollomon parameter considering the compensation of both strain and strain rate. The flow stress values predicted by the constitutive equation agree well with the experimental values, realizing the accurate prediction of the flow stress of Q345E steel under hot deformation.展开更多
Thermal decomposition of 21 kinds of binary mixtures between typical medical compositions was investigated under nitrogen conditions by dynamic thermogravimetric analysis(TGA) at 25–800 °C. The weighed sum metho...Thermal decomposition of 21 kinds of binary mixtures between typical medical compositions was investigated under nitrogen conditions by dynamic thermogravimetric analysis(TGA) at 25–800 °C. The weighed sum method(WSM) coupled with thermal analysis was applied to study the interaction between components. Then, co-pyrolysis kinetic model of the binary mixtures(tube for transfusion(TFT) and gauze) was established to verify the reliability of conclusions. The results show the follows. 1) Strong or weak interactions are shown between binary mixtures containing polyvinyl chloride(PVC), the main ingredient of TFT. The addition of other medical waste could enhance first stage decomposition of TFT. While, the secondary stage pyrolysis may be suppressed or enhanced or not affected by the addition. 2) There exists no interaction between catheter and other component, the DTG peak temperature representing Ca CO3 decomposition in catheter fraction is obviously lower than that of pure catheter; while,the shape of DTG peak keeps unchanged. 3) No evident reaction occurs between the other mix-samples, it is considered that their co-pyrolysis characteristics are linear superposition of mono-component pyrolysis characteristics.展开更多
The method of numerical simulation was applied to investigate the effects of jet impinging plate thickness and its thermal conductivity on the local heat flux distribution along the impinging plate. The results show t...The method of numerical simulation was applied to investigate the effects of jet impinging plate thickness and its thermal conductivity on the local heat flux distribution along the impinging plate. The results show that the two factors have great effects on the heat flux distribution. The non-uniformity of the local heat-flux on the impinging plate surface gets more profound as the plate becomes thicker and thermal conductivity gets larger. When Reynolds number is 5000, the ratio of nozzle-to-plate spacing to nozzle diameter is 5 and thermal conductivity is 16W/(m·K), and even for the plate with only 25μm in thickness, the non-uniformity of the heat flux cannot be neglected. When the plate thickness is 50 μm, only when thermal conductivity is as small as 1W/(m·K), the heat flux curve can be approximately treated as an iso-heat-flux boundary. In the experimental research, a real non-iso-heat-flux boundary is treated as an iso-heat-flux boundary, which would result in under-estimated Nusselt number value in the stagnation zone and an over-estimated value outside. Such an experimental Nusselt number distribution is taken to evaluate turbulent model, and the conclusion would be drawn that the turbulent model over-predicts the stagnation heat transfer. This is one of the important reasons why many literatures reported that k-ε turbulent model dramatically over-predicts the impinging jet heat transfer in the stagnation region.展开更多
基金Project(101048) supported by Fok Ying Tung Education FoundationProject(E2008000835) supported by the Natural Science Foundation of Hebei Province,China
文摘Based on the steady-state strain measured by single-pass hot compression tests,the method by a double-pass hot compression testing was developed to measure the metadynamic-recrystallization kinetics.The metadynamic recrystallization behavior of low-alloy steel Q345B during hot compression deformation was investigated in the temperature range of 1 000-1 100℃,the strain rate range of 0.01-0.10 s -1 and the interpass time range of 0.5-50 s on a Gleeble-3500 thermo-simulation machine.The results show that metadynamic recrystallization during the interpass time can be observed.As the deformation temperature and strain rate increase,softening caused by metadynamic recrystallization is obvious.According to the data of thermo-simulation,the metadynamic recrystallization activation energy is obtained to be Qmd=100.674 kJ/mol and metadynamic recrystallization kinetics model is set up.Finally,the error analysis of metadynamic recrystallization kinetics model proves that the model has high accuracy(correlation coefficient R=0.988 6).
基金Project supported by China-Canada-USA Collaborative Research and Development Project (Magnesium Front End Research and Development (MFERD))
文摘The plastic deformation simulation of AZ31 magnesium alloy at different elevated temperatures （from 473 to 723 K） was performed on Gleeble-1500 thermal mechanical simulator at the strain rates of 0.01, 0.1, 1, 5 and 10 s-t and the maximum deformation degree of 80%. The relationship between the flow stress and deformation temperature as well as strain rate was analyzed. The materials parameters and the apparent activation energy were calculated. The constitutive relationship was established with a Zener-Hollomon （Z） parameter. The results show that the flow stress increases with the increase of strain rate at a constant temperature, but it decreases with the increase of deformation temperature at a constant strain rate. The apparent activation energy is estimated to be 129-153 kJ/mol, which is close to that for self-diffusion of magnesium. The established constitutive relationship can reflect the change of flow stress during hot deformation.
基金Project(51135007)supported by the National Natural Science Foundation of ChinaProject(IRT13087)supported by the Innovative Research Team Development Program of Ministry of Education of China+1 种基金Project(2012-86)supported by the High-end Talent Leading Program of Hubei Province,ChinaProject(2012-P08)supported by State Key Laboratory of Materials Processing and Die&Mould Technology,China
文摘Q345E as one of typical low alloy steels is widely used in manufacturing basic components in many fields because of its eminent formability under elevated temperature. In this work, the deformation behavior of Q345E steel was investigated by hot compression experiments on Gleeble-3500 thermo-mechanical simulator with the temperature ranging from 850 ℃ to 1150 ℃ and strain rate ranging from 0.01 s-1 to 10 s-1. The experimental results indicate that dynamic softening of Q345E benefits from increasing deformation temperature and decreasing strain rate. The mathematical relationship between dynamic softening degree and deformation conditions is established to predict the dynamic softening degree quantitatively, which is further proved by some optical microstructures of Q345E. In addition, the experimental results also reveal that the stress level decreases with increasing deformation temperature and decreasing strain rate. The constitutive equation for flow stress of Q345E is formulated by Arrihenius equation and the modified Zener-Hollomon parameter considering the compensation of both strain and strain rate. The flow stress values predicted by the constitutive equation agree well with the experimental values, realizing the accurate prediction of the flow stress of Q345E steel under hot deformation.
基金Projects(51105269,51406133)supported by the National Natural Science Foundation of ChinaProject supported by the ScientificResearch Foundation for the Returned Overseas Chinese Scholars,Ministry of Education,ChinaProject supported by the Ministry ofEducation Key Laboratory Program,China
文摘Thermal decomposition of 21 kinds of binary mixtures between typical medical compositions was investigated under nitrogen conditions by dynamic thermogravimetric analysis(TGA) at 25–800 °C. The weighed sum method(WSM) coupled with thermal analysis was applied to study the interaction between components. Then, co-pyrolysis kinetic model of the binary mixtures(tube for transfusion(TFT) and gauze) was established to verify the reliability of conclusions. The results show the follows. 1) Strong or weak interactions are shown between binary mixtures containing polyvinyl chloride(PVC), the main ingredient of TFT. The addition of other medical waste could enhance first stage decomposition of TFT. While, the secondary stage pyrolysis may be suppressed or enhanced or not affected by the addition. 2) There exists no interaction between catheter and other component, the DTG peak temperature representing Ca CO3 decomposition in catheter fraction is obviously lower than that of pure catheter; while,the shape of DTG peak keeps unchanged. 3) No evident reaction occurs between the other mix-samples, it is considered that their co-pyrolysis characteristics are linear superposition of mono-component pyrolysis characteristics.
基金Project(50376076) supported by the National Natural Science Foundation of China
文摘The method of numerical simulation was applied to investigate the effects of jet impinging plate thickness and its thermal conductivity on the local heat flux distribution along the impinging plate. The results show that the two factors have great effects on the heat flux distribution. The non-uniformity of the local heat-flux on the impinging plate surface gets more profound as the plate becomes thicker and thermal conductivity gets larger. When Reynolds number is 5000, the ratio of nozzle-to-plate spacing to nozzle diameter is 5 and thermal conductivity is 16W/(m·K), and even for the plate with only 25μm in thickness, the non-uniformity of the heat flux cannot be neglected. When the plate thickness is 50 μm, only when thermal conductivity is as small as 1W/(m·K), the heat flux curve can be approximately treated as an iso-heat-flux boundary. In the experimental research, a real non-iso-heat-flux boundary is treated as an iso-heat-flux boundary, which would result in under-estimated Nusselt number value in the stagnation zone and an over-estimated value outside. Such an experimental Nusselt number distribution is taken to evaluate turbulent model, and the conclusion would be drawn that the turbulent model over-predicts the stagnation heat transfer. This is one of the important reasons why many literatures reported that k-ε turbulent model dramatically over-predicts the impinging jet heat transfer in the stagnation region.
