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乳化炸药水油相集中制备的应用
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作者 郑卫东 李峰 潘伟纲 《爆破器材》 CAS 2010年第5期22-23,共2页
文章介绍了单独设置乳化炸药水相、油相制备工房,为多条乳化炸药生产线提供水油相溶液的应用情况,可减少危险工房的定员定量,提高生产线的安全性。
关键词 乳化炸药 水油相 集中制备 应用
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水油混相协同微波提取辣椒碱工艺优化及应用研究 被引量:3
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作者 阙小峰 方志成 +2 位作者 余雁 司文会 谢恩耀 《食品与机械》 北大核心 2021年第7期159-164,206,共7页
目的:优化干辣椒中辣椒碱的提取工艺并探究其加工特性。方法:采用高压水油混相浸提技术预处理干辣椒,再协同微波辅助溶剂法提取辣椒碱,并应用于食品加工中。结果:水油混相预处理工艺条件为干辣椒粗粉加湿量20%、浸提温度150℃、搅拌机转... 目的:优化干辣椒中辣椒碱的提取工艺并探究其加工特性。方法:采用高压水油混相浸提技术预处理干辣椒,再协同微波辅助溶剂法提取辣椒碱,并应用于食品加工中。结果:水油混相预处理工艺条件为干辣椒粗粉加湿量20%、浸提温度150℃、搅拌机转速300 r/min;微波辅助提取工艺条件为预处理的辣椒粉在600 W微波功率下处理120 s,然后按料液比(m_(辣椒粉)∶V_(乙醇))1∶20(g/mL)添加65%的乙醇,在30℃恒温水浴锅中浸提2.5 h,辣椒碱最佳提取量为4.12 g/kg干辣椒,初次提取率达82.4%,3次理论得率可达99.45%。结论:高压水油混相浸提技术预处理后的干辣椒辣椒碱提取率显著优于传统浸提工艺,且加工性能稳定。 展开更多
关键词 辣椒碱 预处理 微波辅助 提取率
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水油两相体系生物还原-化学沉淀耦合反应制备纳米二硫化锡 被引量:2
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作者 马兴泰 辛宝平 +3 位作者 吴莹 陈岗 吴锋 陈实 《无机化学学报》 SCIE CAS CSCD 北大核心 2011年第4期687-691,共5页
针对Sn4+易于水解而难以在水相稳定存在的不利条件,尝试了在水油两相体系中应用生物转化-化学沉淀耦合反应工艺制备SnS2纳米材料。研究了水油两相体系制备SnS2的优化条件,并借助XRD、SEM、EDS表征了制备材料的结构、形貌和物相。研究表... 针对Sn4+易于水解而难以在水相稳定存在的不利条件,尝试了在水油两相体系中应用生物转化-化学沉淀耦合反应工艺制备SnS2纳米材料。研究了水油两相体系制备SnS2的优化条件,并借助XRD、SEM、EDS表征了制备材料的结构、形貌和物相。研究表明,生物水相pH值7、水油两相反应温度35℃,油相Sn4+与水相SO42-之物质的量浓度比1∶2的条件下有利于SnS2的生成。制备的SnS2为纳米片花瓣,纳米片平均厚度约为30 nm,花状微晶直径约1~5μm,纯度高,无杂质。 展开更多
关键词 SnS2 体系 生物还原 纳米微粒
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低温固化阻水透油防砂材料的室内研究 被引量:3
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作者 郭鸿宇 李丽华 +4 位作者 马诚 杨超 黄金 刘正奎 刘淼 《油田化学》 CAS CSCD 北大核心 2023年第1期61-67,共7页
针对浅层低温地层出砂和油井采出液高含水的问题,开展低温固化阻水透油防砂材料室内研究。将石英砂、环氧树脂、相对渗透率调节剂等通过共混工艺制备了一种低温固化阻水透油防砂材料,利用FT-IR、热重、扫描电子显微镜等分析了防砂材料... 针对浅层低温地层出砂和油井采出液高含水的问题,开展低温固化阻水透油防砂材料室内研究。将石英砂、环氧树脂、相对渗透率调节剂等通过共混工艺制备了一种低温固化阻水透油防砂材料,利用FT-IR、热重、扫描电子显微镜等分析了防砂材料及其人造岩心的固化机理、热稳定性、微观形貌等,通过岩心驱替装置考察了人造岩心的抗压强度和水/油相渗透率。实验结果表明,含有30%相对渗透率调节剂的防砂材料在低温(30~70℃)条件下,固化形成的人造岩心抗压强度达到4.22 MPa以上;同时,相对渗透率调节剂加量为30%的人造岩心的水相渗透率和油相渗透率分别为963×10^(-3)和5513×10^(-3)μm^(2),表现出优异的阻水透油性。所合成的防砂材料在低温(30~70℃)条件下能满足低温浅层井的防砂阻水的要求。 展开更多
关键词 低温浅井 防砂材料 对渗透率调节剂 抗压强度 /渗透率
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Displacement behavior and mechanism of long-term water flooding in sandstone oil reservoirs 被引量:2
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作者 CAO Ren-yi DAI Zong +4 位作者 WANG Zhi-kai WANG Ya-hui JIANG Jun LI hai-long JIA Zhi-hao 《Journal of Central South University》 SCIE EI CAS CSCD 2021年第3期834-847,共14页
Sandstone oil reservoirs with huge bottom water and high permeability are generally developed with high flow rate.After long-term water flooding(LTWF),the water flooding characteristics are quite different from that o... Sandstone oil reservoirs with huge bottom water and high permeability are generally developed with high flow rate.After long-term water flooding(LTWF),the water flooding characteristics are quite different from that of original reservoir.In this paper,the effects of the PV number,viscosity,and displacement rate during LTWF are studied through experiments.The mechanism is analyzed based on analysis of changes in oil composition,rock mineral composition and wettability.The oil-water relative permeability curves,oil recovery and wettability were obtained with new experiments methods,which avoids the oil metering error by measuring oil and water separately.The research indicates that when the viscosity increases,the water phase permeability decreases,the residual oil saturation increases,and the water content rate increases earlier.A higher water flooding rate results in a higher ultimate recovery.A higher asphaltene content results in a higher viscosity and more oil-wet reservoir conditions.After LTWF,the wettability tends to water-wet,which is more favorable for heavy oil recovery.Moreover,LTWF reduces the clay content,which creates a more water-wet surface and a larger reservoir pore throat environment.This research provides insightful characteristics of offshore sandstone oil reservoirs,which can be used to enhance oil recovery. 展开更多
关键词 long-term water flooding sandstone reservoir relative permeability curve WETTABILITY
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Oil–water two-phase flow pattern analysis with ERT based measurement and multivariate maximum Lyapunov exponent 被引量:9
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作者 谭超 王娜娜 董峰 《Journal of Central South University》 SCIE EI CAS CSCD 2016年第1期240-248,共9页
Oil–water two-phase flow patterns in a horizontal pipe are analyzed with a 16-electrode electrical resistance tomography(ERT) system. The measurement data of the ERT are treated as a multivariate time-series, thus th... Oil–water two-phase flow patterns in a horizontal pipe are analyzed with a 16-electrode electrical resistance tomography(ERT) system. The measurement data of the ERT are treated as a multivariate time-series, thus the information extracted from each electrode represents the local phase distribution and fraction change at that location. The multivariate maximum Lyapunov exponent(MMLE) is extracted from the 16-dimension time-series to demonstrate the change of flow pattern versus the superficial velocity ratio of oil to water. The correlation dimension of the multivariate time-series is further introduced to jointly characterize and finally separate the flow patterns with MMLE. The change of flow patterns with superficial oil velocity at different water superficial velocities is studied with MMLE and correlation dimension, respectively, and the flow pattern transition can also be characterized with these two features. The proposed MMLE and correlation dimension map could effectively separate the flow patterns, thus is an effective tool for flow pattern identification and transition analysis. 展开更多
关键词 oil-water two-phase flow flow patterns electrical resistance tomography (ERT) multivariate time-series multivariate maximum Lyapunov exponent correlation dimension
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