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陆相页岩CO_(2)前置压裂缝面微观力学损伤与支撑剂嵌入规律
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作者 孙廉贺 王海柱 +7 位作者 李根生 王斌 STANCHITS Sergey 毛泽龙 张耀辰 CHEREMISIN Alexey 郑永 金家成 《石油勘探与开发》 北大核心 2025年第4期919-929,共11页
为了揭示CO_(2)前置压裂过程中超临界CO_(2)(SCCO_(2))-水-页岩相互作用对陆相页岩支撑剂嵌入影响机制,选取渤海湾盆地陆相页岩,开展SCCO_(2)-水-页岩相互作用实验,通过X射线衍射、扫描电镜大面积高分辨率成像、全自动矿物分析及纳米压... 为了揭示CO_(2)前置压裂过程中超临界CO_(2)(SCCO_(2))-水-页岩相互作用对陆相页岩支撑剂嵌入影响机制,选取渤海湾盆地陆相页岩,开展SCCO_(2)-水-页岩相互作用实验,通过X射线衍射、扫描电镜大面积高分辨率成像、全自动矿物分析及纳米压痕等测试方法分析缝面微观力学损伤机制及支撑剂嵌入特征变化规律。研究表明:随着相互作用时间的延长,白云石、长石及黏土矿物含量降低,石英含量增加,其中白云石溶蚀效果最为显著;页岩硬度及弹性模量均呈现幂律衰减模式,在作用1 d内劣化率最大,随后劣化速度呈现缓慢降低的趋势;样品表面压嵌坑数量及嵌入深度呈增大趋势,作用时间超过3 d后支撑剂出现团簇嵌入现象,样品表面开始出现大深度压嵌坑。 展开更多
关键词 CO_(2)前置压裂 陆相页岩 SCCO_(2)-水-页岩相互作用 微观力学性质 支撑剂压嵌
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Mechanical heterogeneity characterization of coal materials based on nano-indentation experiments
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作者 ZHANG Qi LI Xiang-chun +3 位作者 LI Biao MENG Jun-qing NIE Bai-sheng LU Wei-dong 《Journal of Central South University》 SCIE EI CAS CSCD 2024年第9期3142-3155,共14页
To investigate the complex macro-mechanical properties of coal from a micro-mechanical perspective,we have conducted a series of micro-mechanical experiments on coal using a nano-indentation instrument.These experimen... To investigate the complex macro-mechanical properties of coal from a micro-mechanical perspective,we have conducted a series of micro-mechanical experiments on coal using a nano-indentation instrument.These experiments were conducted under both dynamic and static loading conditions,allowing us to gather the micro-mechanical parameters of coal for further analysis of its micro-mechanical heterogeneity using the box counting statistical method and the Weibull model.The research findings indicate that the load–displacement curves of the coal mass under the two different loading modes exhibit noticeable discreteness.This can be attributed to the stress concentration phenomenon caused by variations in the mechanical properties of the micro-units during the loading process of the coal mass.Consequently,there are significant fluctuations in the micro-mechanical parameters of the coal mass.Moreover,the mechanical heterogeneity of the coal at the nanoscale was confirmed based on the calculation results of the standard deviation coefficient and Weibull modulus of the coal body’s micromechanical parameters.These results reveal the influence of microstructural defects and minerals on the uniformity of the stress field distribution within the loaded coal body,as well as on the ductility characteristics of the micro-defect structure.Furthermore,there is a pronounced heterogeneity in the micromechanical parameters.Furthermore,we have established a relationship between the macro and micro elastic modulus of coal by applying the Mori-Tanaka homogenization method.This relationship holds great significance for revealing the micro-mechanical failure mechanism of coal. 展开更多
关键词 nano-indentation experiment MICROMECHANICS heterogeneity characterization COAL
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