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溶胶-凝胶法制备Al_2O_3-Y_3Al_5O_(12)(YAG)复相纤维 被引量:1
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作者 乔健 刘和义 +1 位作者 朱玉龙 崔宏亮 《耐火材料》 CAS 北大核心 2015年第1期48-51,共4页
为了节约成本,制备直径均匀的纤维,以无水氯化铝、铝粉、硝酸钇、醋酸钇和醋酸为原料,通过溶胶-凝胶法和离心纺丝技术制备了多晶Al2O3-Y3Al5O12(YAG)复相纤维。并用 FT-IR、XRD、TG、SEM对其进行了表征。结果表明,前驱体溶胶... 为了节约成本,制备直径均匀的纤维,以无水氯化铝、铝粉、硝酸钇、醋酸钇和醋酸为原料,通过溶胶-凝胶法和离心纺丝技术制备了多晶Al2O3-Y3Al5O12(YAG)复相纤维。并用 FT-IR、XRD、TG、SEM对其进行了表征。结果表明,前驱体溶胶具有良好的稳定性和可纺性。凝胶纤维在800℃热处理2h,由无定形转变成γ-Al2O3相,1300℃则完全转变成α-Al2O3和Y3Al5O12相。凝胶纤维经干燥后,表面光滑、直径均匀(9~10μm)。随着热处理温度的升高,晶粒逐渐长大、纤维强度逐渐下降。 展开更多
关键词 氧化铝-钇铝石榴石 溶胶-凝胶法 复相纤维 微观形貌
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Effect of nanofibers at surface of carbon fibers on microstructure of carbon/carbon composites during chemical vapor infiltration 被引量:1
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作者 肖鹏 陈洁 +1 位作者 徐先锋 卢雪峰 《Journal of Central South University》 SCIE EI CAS 2014年第7期2590-2595,共6页
Before densification by chemical vapor infiltration,carbon or SiC nanofibers were grown on the surface of carbon fibers by catalytic chemical vapor deposition using electroplated Ni as catalyst.The modification and me... Before densification by chemical vapor infiltration,carbon or SiC nanofibers were grown on the surface of carbon fibers by catalytic chemical vapor deposition using electroplated Ni as catalyst.The modification and mechanism of nanofibers on the pyrocarbon deposition during chemical vapor infiltration were investigated.The results show that the nanofibers improve the surface activity of the carbon fibers and become active nucleation centers during chemical vapor infiltration.They can induce the ordered deposition of pyrocarbon and adjust the interface bonding between pyrocarbon and carbon fibers during the infiltration. 展开更多
关键词 carbon nanofiber SiC nanofiber PYROCARBON interface bonding
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