The deformation behavior of hot-rolled AZ31 magnesium(Mg)alloy sheet was analyzed when subjected to uniaxial tension along its normal direction at temperatures ranging from 100 to 400℃and strain rates ranging from 0....The deformation behavior of hot-rolled AZ31 magnesium(Mg)alloy sheet was analyzed when subjected to uniaxial tension along its normal direction at temperatures ranging from 100 to 400℃and strain rates ranging from 0.5 to 100 mm/min.Based on the stress−strain curves and the dynamic material model,the hot processing map was established,which demonstrates that the power dissipation factor(η)is the most sensitive to strain rate at 400℃via absorption of dislocations.At 400℃,sample at 0.5 mm/min possessesηof 0.89 because of its lower kernel average misorientation(KAM)value of 0.51,while sample at 100 mm/min possessesηof 0.46 with a higher KAM value of 1.147.In addition,the flow stress presents a slight decrease of 25.94 MPa at 10 mm/min compared to that at 100 mm/min and 100℃.The reasons are twofold:a special~34°texture component during 100℃-100 mm/min favoring the activation of basal slip,and dynamic recrystallization(DRX)also providing softening effect to some extent by absorbing dislocations.Difference in activation of basal slip among twin laminas during 100℃-100 mm/min results in deformation inhomogeneity within the grains,which generates stress that helps matrix grains tilt to a direction favorable to basal slip,forming the special~34°texture component.展开更多
通过Gleeble-3500热模拟试验机对电解厚镍进行热加工,研究不同的热轧工艺下电解厚镍的晶面取向、晶粒度、组织、耐蚀性以及电化学溶解性能的变化。采用X-射线衍射仪分析热轧加工后电解厚镍的晶面取向及晶粒度;采用金相显微镜观察电解厚...通过Gleeble-3500热模拟试验机对电解厚镍进行热加工,研究不同的热轧工艺下电解厚镍的晶面取向、晶粒度、组织、耐蚀性以及电化学溶解性能的变化。采用X-射线衍射仪分析热轧加工后电解厚镍的晶面取向及晶粒度;采用金相显微镜观察电解厚镍的金相组织;采用电化学工作站测试电解厚镍的耐蚀性以及溶解性能。结果发现电解厚镍在热轧加工过程中,产生了严重的变形织构,使电解厚镍呈现(220)晶面取向择优,同时伴随着晶粒粗大等问题。电化学测试表明热轧加工改变了电解厚镍的耐蚀性能和溶解性能,经热轧加工后的电解厚镍,其自腐蚀电位由-475 m V变为-401 m V,自腐蚀倾向降低,耐蚀性能提高;自腐蚀电流密度从603.7 m A/m^2降低到216.2 m A/m^2,腐蚀速率减慢;电化学溶解速率减缓,溶解性能与INCO镍较为接近。展开更多
基金Project(52005362) supported by the National Natural Science Foundation of ChinaProjects(202303021221005,202303021211045) supported by the Natural Science Foundation of Shanxi Province,China+1 种基金Project(202402003) supported by the Patent Commercialization Program of Shanxi Province,ChinaProject supported by the Key Research and Development Plan of Xinzhou City,China。
文摘The deformation behavior of hot-rolled AZ31 magnesium(Mg)alloy sheet was analyzed when subjected to uniaxial tension along its normal direction at temperatures ranging from 100 to 400℃and strain rates ranging from 0.5 to 100 mm/min.Based on the stress−strain curves and the dynamic material model,the hot processing map was established,which demonstrates that the power dissipation factor(η)is the most sensitive to strain rate at 400℃via absorption of dislocations.At 400℃,sample at 0.5 mm/min possessesηof 0.89 because of its lower kernel average misorientation(KAM)value of 0.51,while sample at 100 mm/min possessesηof 0.46 with a higher KAM value of 1.147.In addition,the flow stress presents a slight decrease of 25.94 MPa at 10 mm/min compared to that at 100 mm/min and 100℃.The reasons are twofold:a special~34°texture component during 100℃-100 mm/min favoring the activation of basal slip,and dynamic recrystallization(DRX)also providing softening effect to some extent by absorbing dislocations.Difference in activation of basal slip among twin laminas during 100℃-100 mm/min results in deformation inhomogeneity within the grains,which generates stress that helps matrix grains tilt to a direction favorable to basal slip,forming the special~34°texture component.
文摘通过Gleeble-3500热模拟试验机对电解厚镍进行热加工,研究不同的热轧工艺下电解厚镍的晶面取向、晶粒度、组织、耐蚀性以及电化学溶解性能的变化。采用X-射线衍射仪分析热轧加工后电解厚镍的晶面取向及晶粒度;采用金相显微镜观察电解厚镍的金相组织;采用电化学工作站测试电解厚镍的耐蚀性以及溶解性能。结果发现电解厚镍在热轧加工过程中,产生了严重的变形织构,使电解厚镍呈现(220)晶面取向择优,同时伴随着晶粒粗大等问题。电化学测试表明热轧加工改变了电解厚镍的耐蚀性能和溶解性能,经热轧加工后的电解厚镍,其自腐蚀电位由-475 m V变为-401 m V,自腐蚀倾向降低,耐蚀性能提高;自腐蚀电流密度从603.7 m A/m^2降低到216.2 m A/m^2,腐蚀速率减慢;电化学溶解速率减缓,溶解性能与INCO镍较为接近。