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不同产地辽细辛质量比较 被引量:6
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作者 吴艳蓉 王庆 孙启时 《中国现代中药》 CAS 2015年第2期118-121,共4页
目的:比较不同产地中药材辽细辛的质量。方法:用水蒸气蒸馏法提取并测定挥发油的含量,GC-MS法测定挥发油中甲基丁香酚、黄樟醚和榄香脂素的相对含量,HPLC测定马兜铃酸A的含量,原子分光仪等测定药材中无机元素的含量,并用SPSS统计分析系... 目的:比较不同产地中药材辽细辛的质量。方法:用水蒸气蒸馏法提取并测定挥发油的含量,GC-MS法测定挥发油中甲基丁香酚、黄樟醚和榄香脂素的相对含量,HPLC测定马兜铃酸A的含量,原子分光仪等测定药材中无机元素的含量,并用SPSS统计分析系统进行聚类分析。结果:化学试验测定与聚类分析的结果基本一致,5个产地的辽细辛药材聚为3类。结论:应把挥发性成分(挥发油总量、甲基丁香酚、榄香脂素)、有益的无机元素含量高,毒副作用成分黄樟醚、马兜铃酸A和重金属元素含量低作为评价中药材辽细辛质量的依据。将化学试验与聚类分析相结合,使结果分析更为快速、准确。 展开更多
关键词 辽细辛 不同产地 质量比较 化学实验测定 聚类分析
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Development and Lubricating Properties of Rolling Oil for Stainless Steel Cold Rolling 被引量:4
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作者 Zhang Xu Wang Yizhu +2 位作者 Yao Wenjing Sun Jianlin Wang Shiting 《China Petroleum Processing & Petrochemical Technology》 SCIE CAS 2011年第2期57-64,共8页
Appropriate base oils and homologous additives such as extreme pressure and anti-wear agents,oiliness agents and antioxidants were selected,and experiments testing the compatibility performance between additive,base o... Appropriate base oils and homologous additives such as extreme pressure and anti-wear agents,oiliness agents and antioxidants were selected,and experiments testing the compatibility performance between additive,base oil and other components were carried out to develop the SK and SD series of rolling oils for cold rolling of stainless steel.The developed oils were used in the stainless steel cold rolling lubrication experiments,and were successfully applied in the actual cold rolling operation of stainless steel.Compared with a foreign product,the tribological properties,the thermal oxidation stability,and the rolling lubrication performance of the developed stainless steel cold rolling oils were studied.Test results showed that the tribological properties of the thereby developed rolling oils and the reference one were almost at the same level,and to some extent the performance of rolling was even better than the foreign product,at the same time the stainless steel sheet could retain its well annealed performance.Meanwhile,within a certain range,the lubrication of the rolling oil became better as its viscosity increased at the same level of saponification value,which could provide a lower friction coefficient,so that a higher maximum reduction ratio of the rolled piece through a constant roll gap and a minimum thickness could be secured.Also,similar phenomena appeared as the saponification value increased at a same viscosity level of the rolling oils. 展开更多
关键词 stainless steel cold rolling oil rolling lubrication FRICTION thermal analysis
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