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羟基磷灰石的实验合成研究 被引量:4
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作者 田从学 《陶瓷学报》 CAS 2003年第1期20-24,共5页
本文采用中和反应和复分解反应制备HA ,并分析讨论了温度、pH值、加料方式、加料速率及超声波等对合成HA的影响。成品用化学分析法测定Ca P值 ,部分采用X射线衍射法 (XRD)和电镜照相 (SEM)来鉴定样品HA的纯度。
关键词 羟基磷灰石 实验合成 研究 中和反应 复分解反应 温度 PH值 加料方式 加料速率 超声波 磷酸钙陶瓷
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Brazing behavior of ultrafine cemented carbide with stainless steel 被引量:1
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作者 杨天恩 杨力 +3 位作者 熊计 孙兰 郭智兴 郑晓鸣 《Journal of Central South University》 SCIE EI CAS 2014年第8期2991-2999,共9页
In order to investigate the effects of brazing temperature, heating rate and cooling methods on shear strength, hardness, magnetic saturation and coercivity of the ultrafine cemented carbide, the ultrafine cemented ca... In order to investigate the effects of brazing temperature, heating rate and cooling methods on shear strength, hardness, magnetic saturation and coercivity of the ultrafine cemented carbide, the ultrafine cemented carbide was fabricated according to conventional powder metallurgical procedures, and then brazed to the stainless steel with silver-based filler alloy by supersonic frequency induction brazing. The microstructure was observed using scanning electron microscope (SEM), energy dispersive spectroscopy (EDS) and the magnetic properties were tested utilizing coercimeter and cobalt magnetism instrument. The results show that no micro-crack is found in the cemented carbide after brazing because of silver-based sandwich compound used as filler alloy. In the melted silver layer, there is more carbon in the region adjacent to the cemented carbide. Varied shear strengths, hardnesses, magnetic saturations and coercivities are present under different brazing temperatures, heating rates and coolings. This phenomenon is correlated with some factors such as wettability and fluidity of filler alloy, brazing stress, oxidation of cemented carbide, and allotrope transition of cobalt. Shear strength reaches the maximum of 340 MPa and hardness of ultrafine cemented carbide remains 1879 HV at the brazing temperature of 730℃. The carbon increases with the of increase of the heating rate. What's more, and there is no r/phase found under this condition. content decreases with the increase of brazing temperature, and it the lowest magnetic saturation reaches 81.8% of the theoretic value, 展开更多
关键词 ultrafine cemented carbide BRAZING HARDNESS magnetic properties carbon content
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Experimental and numerical study on loading rate effects of rock-like material specimens containing two unparallel fissures 被引量:13
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作者 黄彦华 杨圣奇 曾卫 《Journal of Central South University》 SCIE EI CAS CSCD 2016年第6期1474-1485,共12页
A series of laboratory experiments and PFC numerical simulations for rock-like material specimens containing two unparallel fissures were carried out.On the basis of experimental and numerical results,the stress-strai... A series of laboratory experiments and PFC numerical simulations for rock-like material specimens containing two unparallel fissures were carried out.On the basis of experimental and numerical results,the stress-strain curves,mechanical properties,AE events,cracking behavior and energy characteristics were analyzed to reveal the macro-mechanical behavior and meso-mechanism of pre-fissured specimens under different loading rates.Investigated results show that:1)When the loading rate is relatively low,the stress-strain curves show a brittle response.When the loading rate is relatively high,the curve shows a more ductile response.Both of the peak strength and elastic mudulus increase with the increase of loading rate,which can be expressed as power functions.2)Four crack types are identified,i.e.,tensile crack,shear crack,far-field crack and surface spalling.Moreover,the tensile crack,far-field crack and surface spalling are under tensile mechanism,while the shear crack is under shear mechanism.3)The drops of the stress-strain curves all correspond to the crack initiation or coalescence,which is also linked to a sudden increasing in the accumulated micro-crack curve.4)Both of the maximum bond force and energy have the similar trend with the increase of loading rate to peak strength,which indicates that the trend of peak strength can be explained by the meso-mechanics and energy. 展开更多
关键词 rock mechanics two pre-existing fissures strength parameters crack coalescence particle flow simulation
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