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An optimal design of the liquid-cooling plate channel in a power battery based on response surface methodology
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作者 Jinbo Zheng Jibin Jiang +2 位作者 Xiwei Yu Bingjun Yan Guofu Lian 《中国科学技术大学学报》 北大核心 2025年第2期52-65,51,I0002,共16页
The work takes a new liquid-cooling plate in a power battery with pin fins inside the channel as the object.A mathematical model is established via the central composite design of the response surface to study the rel... The work takes a new liquid-cooling plate in a power battery with pin fins inside the channel as the object.A mathematical model is established via the central composite design of the response surface to study the relationships among the length,width,height,and spacing of pin fins;the maximum temperature and temperature difference of the battery module;and the pressure drop of the liquid-cooling plate.Model accuracy is verified via variance analysis.The new liquid-cooling plate enables the power battery to work within an optimal temperature range.Appropriately increasing the length,width,and height and reducing the spacing of pin fins could reduce the temperature of the power battery module and improve the temperature uniformity.However,the pressure drop of the liquid-cooling plate increases.The structural parameters of the pin fins are optimized to minimize the maximum temperature and the temperature difference of the battery module as well as the pressure drop of the liquid-cooling plate.The errors between the values predicted and actual by the simulation test are 0.58%,4%,and 0.48%,respectively,which further verifies the model accuracy.The results reveal the influence of the structural parameters of the pin fins inside the liquid-cooling plate on its heat dissipation performance and pressure drop characteristics.A theoretical basis is provided for the design of liquid-cooling plates in power batteries and the optimization of structural parameters. 展开更多
关键词 response surface methodology power battery cooling channel optimal design
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Study on Optimization of Extraction Conditions of Platycodon grandiflorum A. DC Polysaccharide Using Response Surface Methodology 被引量:12
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作者 RUAN Zheng ZHOU Quan-cheng +1 位作者 DENG Ze-yuan YIN Yu-long 《食品科学》 EI CAS CSCD 北大核心 2008年第12期283-287,共5页
Platycodon grandiflorum A.DC.(PAl)C)root was taken as experiment material to extract polysaccharide.On the base of single factor tests(extraction time,extraction temperature,liquid-solid ratio,solvent pH value and NaC... Platycodon grandiflorum A.DC.(PAl)C)root was taken as experiment material to extract polysaccharide.On the base of single factor tests(extraction time,extraction temperature,liquid-solid ratio,solvent pH value and NaCl concentration),the study concluded the main factors affecting the extraction of PADC polysaccharide,which are liquid-solid ratio,extraction time and extraction temperature.Then through central-composite test design,the extraction conditions were concluded as liquid-solid ratio 34.43,extraction time 89.83 min and extraction temperature 52.47℃.By means of validation experiments,the adequacy of this model was confirmed. 展开更多
关键词 response surface methodology Platycodon grandiflorum A.DC POLYSACCHARIDE extraction conditions OPTIMIZATION
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Optimal design of butterfly-shaped linear ultrasonic motor using finite element method and response surface methodology 被引量:9
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作者 时运来 陈超 赵淳生 《Journal of Central South University》 SCIE EI CAS 2013年第2期393-404,共12页
A new method for optimizing a butterfly-shaped linear ultrasonic motor was proposed to maximize its mechanical output. The finite element analysis technology and response surface methodology were combined together to ... A new method for optimizing a butterfly-shaped linear ultrasonic motor was proposed to maximize its mechanical output. The finite element analysis technology and response surface methodology were combined together to realize the optimal design of the butterfly-shaped linear ultrasonic motor. First, the operation principle of the motor was introduced. Second, the finite element parameterized model of the stator of the motor was built using ANSYS parametric design language and some structure parameters of the stator were selected as design variables. Third, the sample points were selected in design variable space using latin hypercube Design. Through modal analysis and harmonic response analysis of the stator based on these sample points, the target responses were obtained. These sample points and response values were combined together to build a response surface model. Finally, the simplex method was used to find the optimal solution. The experimental results showed that many aspects of the design requirements of the butterfly-shaped linear ultrasonic motor have been fulfilled. The prototype motor fabricated based on the optimal design result exhibited considerably high dynamic performance, such as no-load speed of 873 ram/s, maximal thrust of 27.5 N, maximal efficiency of 43%, and thrust-weight ratio of 45.8. 展开更多
关键词 linear ultrasonic motor PIEZOELECTRIC optimal design response surface methodology finite element method
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Application of response surface methodology in optimization of bioleaching parameters for high-magnesium nickel sulfide ore 被引量:6
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作者 SUN Jian-zhi WU Biao +1 位作者 CHEN Bo-wei WEN Jian-kang 《Journal of Central South University》 SCIE EI CAS CSCD 2022年第5期1488-1499,共12页
The response surface methodology(RSM)was used to optimize the operating parameters during the bioleaching of Jinchuan high-magnesium nickel sulfide ore.The particle size,acid addition,pulp density and inoculation amou... The response surface methodology(RSM)was used to optimize the operating parameters during the bioleaching of Jinchuan high-magnesium nickel sulfide ore.The particle size,acid addition,pulp density and inoculation amount were chosen as the investigated parameters.To maximize the leaching efficiency of nickel,copper,cobalt and minimize the dissolution of magnesium and iron ions,the model suggested a combination of optimal parameters of particles less than 0.074 mm being 72.11%,sulfuric acid addition being 300 kg/t,pulp density being 5%and inoculation amount being 12.88%.Under the conditions,the average results of three parallel experiments were 89.43%of nickel leaching efficiency,36.78%of copper leaching efficiency,84.07%of cobalt leaching efficiency,49.19%of magnesium leaching efficiency and 0.20 g/L of iron concentration.The model indicated that the most significant factor in response of the leaching efficiency of valuable metal is the particle size,and the most significant factor in response to the leaching efficiency of harmful ions(Mg2+)is the amount of sulfuric acid addition.And according to the suggested models,no significance of the interaction effect between particle size and acid addition was shown.Under the optimized parameters suggested by models,the valuable metals could be separated from harmful ions during the bioleaching process. 展开更多
关键词 high-magnesium nickel sulfide ore BIOLEACHING response surface methodology particle size acid consumption
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Deformation prediction and analysis of underground mining during stacking of dry gangue in open-pit based on response surface methodology 被引量:6
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作者 QIU Xian-yang CHEN Jia-yao +3 位作者 SHI Xiu-zhi ZHANG Shu ZHOU Jian CHEN Xin 《Journal of Central South University》 SCIE EI CAS CSCD 2018年第2期406-417,共12页
Deformation prediction and the analysis of underground goaf are important to the safe and efficient recovery of residual ore when shifting from open-pit mining to underground mining.To address the comprehensive proble... Deformation prediction and the analysis of underground goaf are important to the safe and efficient recovery of residual ore when shifting from open-pit mining to underground mining.To address the comprehensive problem of stability in the double mined-out area of the Tong-Lv-Shan(TLS)mine,which employed the dry stacked gangue technology,this paper applies the function fitting theory and a regression analysis method to screen the sensitive interval of four influencing factors based on single-factor experiments and the numerical simulation software FLAC3D.The influencing factors of the TLS mine consist of the column thickness(d),gob area span(D),boundary pillar thickness(h)and height of tailing gangue(H).The fitting degree between the four factors and the displacement of the gob roof(W)is reasonable because the correlation coefficient(R2)is greater than0.9701.After establishing29groups that satisfy the principles of Box-Behnken design(BBD),the dry gangue tailings process was re-simulated for the selected sensitive interval.Using a combination of an analysis of variance(ANOVA),regression equations and a significance analysis,the prediction results of the response surface methodology(RSM)show that the significant degree for the stability of the mined-out area for the factors satisfies the relationship of h>D>d>H.The importance of the four factors cannot be disregarded in a comparison of the prediction results of the engineering test stope in the TLS mine.By comparing the data of monitoring points and function prediction,the proposed method has shown promising results,and the prediction accuracy of RSM model is acceptable.The relative errors of the two test stopes are1.67%and3.85%,respectively,which yield satisfactory reliability and reference values for the mines. 展开更多
关键词 response surface methodology (RSM) Box-Behnken design (BBD) numerical simulation boundary pillar deformation prediction
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Optimization of processing parameters for microwave drying of selenium-rich slag using incremental improved back-propagation neural network and response surface methodology 被引量:4
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作者 李英伟 彭金辉 +2 位作者 梁贵安 李玮 张世敏 《Journal of Central South University》 SCIE EI CAS 2011年第5期1441-1447,共7页
In the non-linear microwave drying process, the incremental improved back-propagation (BP) neural network and response surface methodology (RSM) were used to build a predictive model of the combined effects of ind... In the non-linear microwave drying process, the incremental improved back-propagation (BP) neural network and response surface methodology (RSM) were used to build a predictive model of the combined effects of independent variables (the microwave power, the acting time and the rotational frequency) for microwave drying of selenium-rich slag. The optimum operating conditions obtained from the quadratic form of the RSM are: the microwave power of 14.97 kW, the acting time of 89.58 min, the rotational frequency of 10.94 Hz, and the temperature of 136.407 ℃. The relative dehydration rate of 97.1895% is obtained. Under the optimum operating conditions, the incremental improved BP neural network prediction model can predict the drying process results and different effects on the results of the independent variables. The verification experiments demonstrate the prediction accuracy of the network, and the mean squared error is 0.16. The optimized results indicate that RSM can optimize the experimental conditions within much more broad range by considering the combination of factors and the neural network model can predict the results effectively and provide the theoretical guidance for the follow-up production process. 展开更多
关键词 microwave drying response surface methodology optimization incremental improved back-propagation neural network PREDICTION
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Multiple-response optimization for melting process of aluminum melting furnace based on response surface methodology with desirability function 被引量:3
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作者 周孑民 王计敏 +2 位作者 闫红杰 李世轩 贵广臣 《Journal of Central South University》 SCIE EI CAS 2012年第10期2875-2885,共11页
To reduce the fuel consumption and emissions and also enhance the molten aluminum quality, a mathematical model with user-developed melting model and burning capacity model, were established according to the features ... To reduce the fuel consumption and emissions and also enhance the molten aluminum quality, a mathematical model with user-developed melting model and burning capacity model, were established according to the features of melting process of regenerative aluminum melting furnaces. Based on validating results by heat balance test for an aluminum melting furnace, CFD (computational fluid dynamics) technique, in association with statistical experimental design were used to optimize the melting process of the aluminum melting furnace. Four important factors influencing the melting time, such as horizontal angle between burners, height-to-radius ratio, natural gas mass flow and air preheated temperature, were identified by PLACKETT-BURMAN design. A steepest descent method was undertaken to determine the optimal regions of these factors. Response surface methodology with BOX-BEHNKEN design was adopted to further investigate the mutual interactions between these variables on RSD (relative standard deviation) of aluminum temperature, RSD of furnace temperature and melting time. Multiple-response optimization by desirability function approach was used to determine the optimum melting process parameters. The results indicate that the interaction between the height-to-radius ratio and horizontal angle between burners affects the response variables significantly. The predicted results show that the minimum RSD of aluminum temperature (12.13%), RSD of furnace temperature (18.50%) and melting time (3.9 h) could be obtained under the optimum conditions of horizontal angle between burners as 64°, height-to-radius ratio as 0.3, natural gas mass flow as 599 m3/h, and air preheated temperature as 639 ℃. These predicted values were further verified by validation experiments. The excellent correlation between the predicted and experimental values confirms the validity and practicability of this statistical optimum strategy. 展开更多
关键词 aluminum melting furnace melting process response surface methodology desirability function multiple response parameter optimization numerical simulation PLACKETT-BURMAN design BOX-BEHNKEN design
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Regeneration of waste activated carbon after extracting gold with steam under microwave heating:Optimization using response surface methodology 被引量:2
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作者 左勇刚 张利波 +3 位作者 彭金辉 C.SRINIVASAKANNAN 刘秉国 马爱元 《Journal of Central South University》 SCIE EI CAS 2014年第8期3233-3240,共8页
The technology that waste activated carbon after extracting gold is regenerated with steam under microwave heating was studied. The influence of the activation temperature, activation duration and steam flow rate on i... The technology that waste activated carbon after extracting gold is regenerated with steam under microwave heating was studied. The influence of the activation temperature, activation duration and steam flow rate on iodine adsorption value and regeneration yield of activated carbon was investigated. The response surface methodology (RSM) technique was utilized to optimize the process conditions. The optimum conditions for the preparation of activated carbon are identified to be activation temperature of 831 ℃, activation duration of 40 min and steam flow rate of 2.67 mL/min. The optimum conditions result in an activated carbon with an iodine number of 1048 mg/g and a yield of 40%, and the BET surface area evaluated using nitrogen adsorption isotherm is 1493 m2/g, with total pore volume of 1.242 cm3/g. And the pore structure of activated carbon regenerated is mainly composed of micropores and a small amount of mesopores. 展开更多
关键词 microwave heating STEAM waste activated carbon EXTRACTING response surface methodology
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Response surface methodology-based hybrid robust design optimization for complex product under mixed uncertainties 被引量:1
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作者 WAN Liangqi CHEN Hongzhuan OUYANG Linhan 《Journal of Systems Engineering and Electronics》 SCIE EI CSCD 2019年第2期308-318,共11页
Minimizing the impact of the mixed uncertainties(i.e.,the aleatory uncertainty and the epistemic uncertainty) for a complex product of compliant mechanism(CPCM) quality improvement signifies a fascinating research top... Minimizing the impact of the mixed uncertainties(i.e.,the aleatory uncertainty and the epistemic uncertainty) for a complex product of compliant mechanism(CPCM) quality improvement signifies a fascinating research topic to enhance the robustness.However, most of the existing works in the CPCM robust design optimization neglect the mixed uncertainties, which might result in an unstable design or even an infeasible design. To solve this issue, a response surface methodology-based hybrid robust design optimization(RSM-based HRDO) approach is proposed to improve the robustness of the quality characteristic for the CPCM via considering the mixed uncertainties in the robust design optimization. A bridge-type amplification mechanism is used to manifest the effectiveness of the proposed approach. The comparison results prove that the proposed approach can not only keep its superiority in the robustness, but also provide a robust scheme for optimizing the design parameters. 展开更多
关键词 response surface methodology (RSM) HYBRID robust design optimization (HRDO) uncertainty complex product of compliant mechanism (CPCM)
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Leaching of copper from chalcopyrite concentrate by using ammonium persulphate in an autoclave:Determination of most suitable impeller type by using response surface methodology 被引量:1
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作者 M.D.Turan H.S.Altundogan 《Journal of Central South University》 SCIE EI CAS 2013年第3期622-628,共7页
Some effective parameters on the copper extraction from Kiire chalcopyrite concentrate were optimized by using response surface methodology (RSM). Experiments designed by RSM were carried out in the presence of ammo... Some effective parameters on the copper extraction from Kiire chalcopyrite concentrate were optimized by using response surface methodology (RSM). Experiments designed by RSM were carried out in the presence of ammonium persulfate (APS) and different types of impeller in an autoclave system. Ammonium persulfate concentration and leaching temperature were defined numerically and three types of impellers were defined categorically as independent variables using experimental design software. The optimum condition for copper extraction from the chalcopyrite concentrate is found to be ammonium persulfate concentration of 277.77 kg/m3, leaching temperature of 389.98 K and wheel type of impeller. The proposed model equation using RSM has shown good agreement with the experimental data, with correlation coefficients R2 and RaZaj for the model as 0.89 and 0.84, respectively. 展开更多
关键词 COPPER CHALCOPYRITE LEACHING response surface methodology ammonium persulfate optimization
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Heat treatment optimization for tensile properties of 8011 Al/15% SiCp metal matrix composite using response surface methodology 被引量:7
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作者 V.VEMBU G.GANESAN 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2015年第4期390-395,共6页
In this study,a mathematical model was developed to optimize the heat treatment process for maximum tensile strength and ductility of aluminum(8011) silicon carbide particulate composites.The process parameters are so... In this study,a mathematical model was developed to optimize the heat treatment process for maximum tensile strength and ductility of aluminum(8011) silicon carbide particulate composites.The process parameters are solutionizing time,aging temperature,and aging time.The experiments were performed on an universal testing machine according to centre rotatable design matrix.A mathematical model was developed with the main and interactive effects of the parameters considered.The analysis of variance technique was used to check the adequacy of the developed model.The optimum parameters were obtained for maximum tensile strength.Fractographic examination shows the cracks and dimples on the fractured surfaces of heat-treated specimen. 展开更多
关键词 热处理工艺优化 颗粒复合材料 响应曲面法 拉伸性能 金属基体 万能试验机 开发模型
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Optimization of process parameters of aluminum alloy AA 2014-T6 friction stir welds by response surface methodology 被引量:7
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作者 Ramanjaneyulu KADAGANCHI Madhusudhan Reddy GANKIDI Hina GOKHALE 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2015年第3期209-219,共11页
The heat treatable aluminum-copper alloy AA2014 finds wide application in the aerospace and defence industry due to its high strength-toweight ratio and good ductility. Friction stir welding(FSW) process, an emerging ... The heat treatable aluminum-copper alloy AA2014 finds wide application in the aerospace and defence industry due to its high strength-toweight ratio and good ductility. Friction stir welding(FSW) process, an emerging solid state joining process, is suitable for joining this alloy compared to fusion welding processes. This work presents the formulation of a mathematical model with process parameters and tool geometry to predict the responses of friction stir welds of AA 2014-T6 aluminum alloy, viz yield strength, tensile strength and ductility. The most influential process parameters considered are spindle speed, welding speed, tilt angle and tool pin profile. A four-factor, five-level central composite design was used and a response surface methodology(RSM) was employed to develop the regression models to predict the responses.The mechanical properties, such as yield strength(YS), ultimate tensile strength(UTS) and percentage elongation(%El), are considered as responses. Method of analysis of variance was used to determine the important process parameters that affect the responses. Validation trials were carried out to validate these results. These results indicate that the friction stir welds of AA 2014-T6 aluminum alloy welded with hexagonal tool pin profile have the highest tensile strength and elongation, whereas the joints fabricated with conical tool pin profile have the lowest tensile strength and elongation. 展开更多
关键词 焊接工艺参数 搅拌摩擦焊 铝合金焊接 响应面分析法 抗拉强度 优化 焊接接头 屈服强度
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Optimization of Supercritical Fluid Extraction of Tea Flower Polysaccharides by Using Response Surface Method 被引量:1
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作者 Xing-Hai Zhang Fei Que +2 位作者 Jin-Wei Xu Pei-Li Yu You-Ying Tu 《茶叶》 2013年第4期442-451,共10页
Polysaccharide production from tea flower(TFPS) was carried out using supercritical fluid extraction(SFE).Response surface methodology(RSM),based on a five level,four variable small central composite design,was employ... Polysaccharide production from tea flower(TFPS) was carried out using supercritical fluid extraction(SFE).Response surface methodology(RSM),based on a five level,four variable small central composite design,was employed to obtain the best possible combination of extraction time,pressure,temperature and ethanol content of modifier for maximum production.The optimum conditions were as follows:extraction time of 170 min,pressure of45 MPa,temperature of 75 ℃,and 50% aqueous ethanol solution as modifier.Under these conditions,the experimental yield was 6.56 ± 0.37%,which was similar to the value predicted by the model.Monosaccharide composition of TFPS was fucose,rhamnose,arabinose,xylose,galactose,glucose,mannose,fructose,ribose,galacturonic acid and glucuronic acid in a molar percent of 31.69,0.21,0.49,1.29,35.82,0.97,1.63,18.34,7.88,1.06 and 0.63.Compared to other extraction methods,SFE could achieve higher yield and gain more types of monosaccharide. 展开更多
关键词 超临界流体萃取 茶多糖 响应曲面法 葡萄糖醛酸 半乳糖醛酸 优化 花卉 中心复合设计
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Evaluation of surface roughness and optimization of cutting parameters in turning of AA2024 alloy under different cooling-lubrication conditions using RSM method 被引量:3
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作者 Seyed Hasan MUSAVI Behnam DAVOODI Behzad ESKANDARI 《Journal of Central South University》 SCIE EI CAS CSCD 2020年第6期1714-1728,共15页
In the present study,the effect of reduction of cutting fluid consumption on the surface quality and tool wear was studied.Mathematical models were developed to predict the surface roughness using response surface met... In the present study,the effect of reduction of cutting fluid consumption on the surface quality and tool wear was studied.Mathematical models were developed to predict the surface roughness using response surface methodology(RSM).Analysis of variance(ANOVA)was used to investigate the significance of the developed regression models.The results showed that the coefficient of determination values(R^2)for the developed models was 97.46%for dry,89.32%for flood mode(FM),and 99.44%for MQL,showing the high accuracy of fitted models.Also,under the minimum quantity lubrication(MQL)condition,the surface roughness improved by 23%−44%and 19%−41%compared with dry and FM,respectively,and the SEM images of machined surface proved the statement.The prepared SEM images of tool rake face also showed a considerable decrease in adhesion wear.Built-up edge and built-up layer were the two main products of the adhesion wear,and energy-dispersive X-ray spectroscopy(EDX)analysis of specific points on the tool faces helped to discover the chemical compositions of adhered materials.By changing dry and FM to MQL mode,dominant mechanism of tool wear in machining aluminum alloy was significantly decreased.Breakage wear that led to early failure of cutting edge was also controlled by MQL technique. 展开更多
关键词 cooling-lubrication methods surface roughness minimum quantity lubrication response surface methodology AA2024 aluminum alloy
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响应面法结合深度神经网络优化刺五加果多糖提取工艺 被引量:3
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作者 苏适 董立强 +3 位作者 黎莉 王双侠 王喜庆 张金凤 《包装与食品机械》 北大核心 2025年第2期66-74,共9页
为提高刺五加果多糖的提取率,提出基于Box-Behnken响应面法与深度神经网络模型(deep neural network,DNN)协同优化的微波辅助离子液体提取工艺。通过响应面设计,筛选微波功率、离子液体浓度、提取时间及料液比等参数,并构建二次回归模型... 为提高刺五加果多糖的提取率,提出基于Box-Behnken响应面法与深度神经网络模型(deep neural network,DNN)协同优化的微波辅助离子液体提取工艺。通过响应面设计,筛选微波功率、离子液体浓度、提取时间及料液比等参数,并构建二次回归模型;利用DNN模型解析多因素间非线性关系,优化工艺条件。结果表明,DNN模型得到的最优工艺条件为微波功率350 W、离子液体浓度0.6 mol/L、提取时间35 min、料液比1∶24(g/mL),多糖提取率为16.71%,高于响应面法优化的提取工艺结果。体外抗氧化试验显示,刺五加果多糖对羟基自由基、DPPH自由基和ABTS^(+)·自由基的半数抑制浓度(IC_(50))分别为2.36,2.05,2.47 mg/mL。研究为刺五加果在功能性食品及抗衰老保健品开发中的应用提供理论依据。 展开更多
关键词 刺五加果 多糖 工艺优化 响应面法 深度神经网络 抗氧化活性
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基于响应面法-遗传算法的船舶推进轴系多目标优化设计 被引量:2
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作者 张聪 疏炳南 +1 位作者 张江涛 金勇 《上海交通大学学报》 北大核心 2025年第4期466-475,I0001,共11页
为降低船舶在航行过程中传动设备的功率损失,提高推进轴系的传递效率,并改善轴系振动性能,基于响应面模型与遗传算法(GA)对某船舶轴系实验台进行了多目标优化设计.采用星点设计(CCD)方法,在优化设计空间中选取合理实验点,拟合构建最小... 为降低船舶在航行过程中传动设备的功率损失,提高推进轴系的传递效率,并改善轴系振动性能,基于响应面模型与遗传算法(GA)对某船舶轴系实验台进行了多目标优化设计.采用星点设计(CCD)方法,在优化设计空间中选取合理实验点,拟合构建最小总功耗和振动响应幅值的响应面模型.基于GA,利用MATLAB软件求解响应面模型回归函数的Pareto最优解.对比分析各组优化结果,获得最佳优化设计方案,研究结果表明采用这种联合方法后,轴系功耗损失降低了约7.10%,轴系振动幅值降低了2.30%,能有效提高轴系传递效率和抑制推进轴系振动问题,从而验证了船舶推进轴系多目标优化方法的正确性和可行性. 展开更多
关键词 推进轴系 传递效率 响应面法 遗传算法
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羊肚菌酶解工艺优化及酶解液挥发性风味物质分析 被引量:1
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作者 曾小峰 颜蜜 +5 位作者 盖智星 高伦江 尹旭敏 刁源 商桑 曾顺德 《食品工业科技》 北大核心 2025年第4期147-154,共8页
为优化羊肚菌酶解工艺,探究酶解液挥发性风味物质,研究采用响应面试验设计优化酶解工艺,顶空固相微萃取-气相色谱-质谱(Headspace-solid phase microextraction-gas chromatography-mass spectrometry,HS-SPMEGC-MS)结合香气活性值(Odor... 为优化羊肚菌酶解工艺,探究酶解液挥发性风味物质,研究采用响应面试验设计优化酶解工艺,顶空固相微萃取-气相色谱-质谱(Headspace-solid phase microextraction-gas chromatography-mass spectrometry,HS-SPMEGC-MS)结合香气活性值(Odor activity value,OAV)分析鉴定关键风味物质。结果表明,加酶量5000 U/g、pH6.7、酶解温度44℃、酶解时间2 h为最佳酶解工艺,此条件下水解度达34.11%;GC-MS分析共鉴定出挥发性风味物质23种,其中空白组17种,酶解组21种,酶解后风味物质含量增加了203.71%,醛类是最主要的挥发性风味物质,占整个风味物质的78.50%。进一步分析OAV≥1的化合物,空白组7种,酶解组9种,并确定异戊醛、苯乙醛、正己醛、苯甲醛、壬醛、芳樟醇、2-戊基呋喃、柠檬烯、萘为羊肚菌酶解液的关键风味化合物。该研究表明酶解可促进风味物质的释放,为羊肚菌的风味利用、调味料深加工开发提供数据基础。 展开更多
关键词 羊肚菌 酶解工艺 响应面法 风味 香气活性值(OAV)
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原子吸收光谱法测定矿石中Au的分析技术及最优化模型研究 被引量:2
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作者 王鹏 门倩妮 +7 位作者 甘黎明 白金峰 王啸 井斌强 寇少磊 刘慧蓝 何涛 刘玖芬 《光谱学与光谱分析》 北大核心 2025年第2期426-433,共8页
矿石中Au通常以颗粒金或者晶格金的形式存在,在不同类型的金矿石中赋存状态不同,其特殊的延展性引起的颗粒效应对于Au样品的分析技术带来挑战,并且其制备流程要素繁多且不易控制,直接影响Au分析的准确性和稳定性。以矿石中金元素为研究... 矿石中Au通常以颗粒金或者晶格金的形式存在,在不同类型的金矿石中赋存状态不同,其特殊的延展性引起的颗粒效应对于Au样品的分析技术带来挑战,并且其制备流程要素繁多且不易控制,直接影响Au分析的准确性和稳定性。以矿石中金元素为研究对象,建立泡塑吸附-原子吸收光谱法测定矿石中Au的分析方法,针对样品测试流程中的关键要素进行定性判断和定量计算,提出基于灰色关联度-响应曲面法的最优化模型。讨论样品分析技术中焙烧、消解、富集和解脱等重要环节,确定焙烧方式、消解酸度、富集时间和硫脲浓度为优化要素,设计正交试验并进行相关性分析,计算灰色关联系数并进行极差确定,定性判断各优化要素的显著性。中心组合设计结合响应曲面法原理制作显著水平表,建立二次多项式回归方程的预测模型并进行显著性分析,绘制三维响应曲面图和二维等高线图对实验数据进行拟合分析,确定最优化模型参数焙烧方式、消解酸度、富集时间和硫脲浓度分别为阶梯式分段焙烧、10.58%、40.00 min、11.65 g·L^(-1)。实验结果表明,在最优化模型条件下对金矿石国家一级标准物质进行制备测试,其方法检出限为0.021,测定下限为0.077,加标回收率为91.6%~104.5%,其正确度和精密度均符合GB/T 20899.2—2019质量控制要求;同时对陕西西秦岭地区和甘肃梅川地区外检样品进行方法验证比对,其相对偏差不超过10%且评价结果均为优秀,表明该检测优化模型方法在实际样品中的应用依然准确可靠,具备正确性和科学性。该研究对于地质矿产实验室快速、准确、简便分析Au元素提出新方法,为检验检测领域中优化多目标参数组合的课题提供了新的思路,同时为新一轮战略找矿行动的准确测试贡献力量。 展开更多
关键词 原子吸收光谱法 灰色关联度 响应曲面法 中心组合设计 质量控制
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藤茶解酒功能发酵乳的制备及功效评价 被引量:1
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作者 李冬梅 李晴晖 +4 位作者 李宝玉 郝志明 梁锦钊 文炎 李春莲 《中国酿造》 北大核心 2025年第2期128-135,共8页
以纯牛奶为主要原料,添加藤茶(Ampelopsis grossedentata)提取液,研制一款口味和解酒功效俱佳的藤茶功能发酵乳。通过单因素试验,以二氢杨梅素(DMY)含量、乙醇脱氢酶(ADH)激活率、超氧化物歧化酶(SOD)活力和感官评价为综合评价指标,筛... 以纯牛奶为主要原料,添加藤茶(Ampelopsis grossedentata)提取液,研制一款口味和解酒功效俱佳的藤茶功能发酵乳。通过单因素试验,以二氢杨梅素(DMY)含量、乙醇脱氢酶(ADH)激活率、超氧化物歧化酶(SOD)活力和感官评价为综合评价指标,筛选出最佳的发酵剂菌种和各成分最佳添加量;在单因素试验基础上,利用响应面试验优化藤茶发酵乳的配方,并采用体外和体内小鼠试验评价其解酒功效。结果表明,藤茶发酵乳最佳制备工艺条件为采用66菌型发酵剂,藤茶提取液添加量12%、纯牛奶添加量75%、木糖醇添加量6%、菌种添加量0.125%。在此最佳条件下,藤茶发酵乳综合评价为68.33,二氢杨梅素含量为0.62 mg/mL。藤茶解酒功能发酵乳对解酒酶乙醇脱氢酶和乙醛脱氢酶(ALDH)激活率分别为70.05%和82.38%、SOD酶活力达72.66 U/g;且能极显著延长醉酒小鼠酒精耐受时间、缩短睡眠时间和醒酒时间(P<0.01)。藤茶发酵乳功能因子明确,功效成分含量高,解酒功效优良,市场前景广阔。 展开更多
关键词 藤茶 发酵乳 配方优化 响应面法 解酒功能
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基于再生胶凝固化剂的季冻区路基固化土工程性能研究 被引量:1
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作者 姜鹏 刘林 +4 位作者 邹仁 仝亚刚 张小宁 王帅 郎永贤 《铁道科学与工程学报》 北大核心 2025年第2期636-648,共13页
为实现工业固废在道路与铁道路基工程中的高值化利用,助力双碳目标在交通运输工程领域中的达成,采用钢渣、矿渣与2种脱硫产物(DP-1、DP-2)等工业固废制备再生胶凝固化剂。基于响应面法考察不同工业固废的交互作用并得到其最优组配。采... 为实现工业固废在道路与铁道路基工程中的高值化利用,助力双碳目标在交通运输工程领域中的达成,采用钢渣、矿渣与2种脱硫产物(DP-1、DP-2)等工业固废制备再生胶凝固化剂。基于响应面法考察不同工业固废的交互作用并得到其最优组配。采用最优组配下的固化剂对粉土进行改良固化,并表征本研究固化粉土微观结构。与水泥固化粉土作对比,探究了固化剂掺量、养护龄期对固化粉土力学性能和耐久性的影响规律,并分析2种固化粉土的矿物成分,探究再生胶凝固化剂的粉土固化机理。研究结果表明:7 d无侧限抗压强度(p_(usc))响应面模型经残差正态概率分布检验,模型可靠度较高。钢渣与矿渣、钢渣与DP-2交互作用对7 d p_(usc)值的影响极其显著,再生胶凝固化剂最优配比(%)为钢渣∶矿渣∶DP-1∶DP-2=52.1∶19.9∶19.5∶8.5。研究可知,固化粉土具有良好的力学性能和耐久性,在养护后期(28 d)与水泥固化粉土p_(usc)值、加州承载比值、水稳性能系数值、冻融循环系数值分别相差1.9%、0.5%、1.0%、2.3%。再生胶凝固化剂组分在碱性环境中发挥协同作用,水化产物交错生长填充了粉土颗粒之间的孔隙,从而提高了固化粉土的力学性能。同掺量的再生胶凝固化剂碳排放仅为水泥的1.66%,推荐再生胶凝固化剂路床固化工程最优掺量为6%~8%,该技术的推广应用具有重要环保和社会意义。 展开更多
关键词 工业固废 响应面法 固化剂 力学性能 耐久性 固化机理
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