High purity and ultrafine DAAF(u-DAAF)is an emerging insensitive charge in initiators.Although there are many ways to obtain u-DAAF,developing a preparation method with stable operation,accurate control,good quality c...High purity and ultrafine DAAF(u-DAAF)is an emerging insensitive charge in initiators.Although there are many ways to obtain u-DAAF,developing a preparation method with stable operation,accurate control,good quality consistency,equipment miniaturization,and minimum manpower is an inevitable requirement to adapt to the current social technology development trend.Here reported is the microfluidic preparation of u-DAAF with tunable particle size by a passive swirling microreactor.Under the guidance of recrystallization growth kinetics and mixing behavior of fluids in the swirling microreactor,the key parameters(liquid flow rate,explosive concentration and crystallization temperature)were screened and optimized through screening experiments.Under the condition that no surfactant is added and only experimental parameters are controlled,the particle size of recrystallized DAAF can be adjusted from 98 nm to 785 nm,and the corresponding specific surface area is 8.45 m^(2)·g^(-1)to 1.33 m^(2)·g^(-1).In addition,the preparation method has good batch stability,high yield(90.8%-92.6%)and high purity(99.0%-99.4%),indicating a high practical application potential.Electric explosion derived flyer initiation tests demonstrate that the u-DAAF shows an initiation sensitivity much lower than that of the raw DAAF,and comparable to that of the refined DAAF by conventional spraying crystallization method.This study provides an efficient method to fabricate u-DAAF with narrow particle size distribution and high reproducibility as well as a theoretical reference for fabrication of other ultrafine explosives.展开更多
To study the influence of B4C particle size on the microstructure and damping capacities of(B_(4)C+Ti)/Mg composites,in situ reactive infiltration technique was utilized to prepare Mg-matrix composites.The microstruct...To study the influence of B4C particle size on the microstructure and damping capacities of(B_(4)C+Ti)/Mg composites,in situ reactive infiltration technique was utilized to prepare Mg-matrix composites.The microstructure,produced phases and damping capacities of the composites prepared with different particle size of B4C were characterized and analyzed.The results show that the reaction between B4C and Ti tends to be more complete when finer B_(4)C particle was used to prepare the composites.But the microstructure of the as-prepared composites is more homogenous when B4C and Ti have similar particle size.The strain-dependent damping capacities of(B_(4)C+Ti)/Mg composites improve gradually with the increase of strain amplitude,and composites prepared with coarser B4C particles tend to have higher damping capacities.The temperature-dependent damping capacities improve with increasing the measuring temperatures,and the kind of damping capacities of the composites prepared with 5mm B4C are inferior to those of coarser particles.The dominant damping mechanism for the strain-damping capacity is dislocation damping and plastic zone damping,while that for the temperature-damping capacity is interface damping or grain boundary damping.展开更多
Particle size and content of RDX are the two main factors that affect the burning stability of RDX-based propellants. However, these effects and the corresponding mechanisms are still controversial. In this work, we i...Particle size and content of RDX are the two main factors that affect the burning stability of RDX-based propellants. However, these effects and the corresponding mechanisms are still controversial. In this work, we investigated the physicochemical processes during burning and the corresponding mechanisms through the technologies of structure compactness analysis on the base of voidage measurement and theoretical interfacial area estimation, apparent burning rate measurement using closed vessel(CV)and extinguished burning surface characterization relying on interrupted closed vessel(ICV) and scanning electron microscope(SEM). The results indicate that the voidage increased with the increase of RDX content and particle size due to the increasing interfacial area and increasing interface gap size,respectively. The apparent burning rate increased with the increase of RDX particle size because of the decreasing RDX specific surface area on the burning surface, which could decrease the heat absorbing rates of the melting and evaporation processes of RDX in the condensed phase. Similarly, the apparent burning rate decreased with the increase of RDX content at pressures lower than around 55 MPa due to the increasing RDX specific surface area. Whereas, an opposite trend could be observed at pressures higher than around 55 MPa, which was attributed to the increasing heat feedback from the gas phase as the result of the increasing propellant energy. For propellants containing very coarse RDX particles, such as 97.8 and 199.4 μm average size, the apparent burning rate increased stably with a flat extinguished surface at pressures lower than around 30 MPa, while increased sharply above around 30 MPa with the extinguished surface becoming more and more rugged as the pressure increased. In addition, the turning degree of u-p curve increased with the increase of coarse RDX content and particle size, and could be reduced by improving the structure compactness.展开更多
As a production quality index of hematite grinding process,particle size(PS)is hard to be measured in real time.To achieve the PS estimation,this paper proposes a novel data driven model of PS using stochastic configu...As a production quality index of hematite grinding process,particle size(PS)is hard to be measured in real time.To achieve the PS estimation,this paper proposes a novel data driven model of PS using stochastic configuration network(SCN)with robust technique,namely,robust SCN(RSCN).Firstly,this paper proves the universal approximation property of RSCN with weighted least squares technique.Secondly,three robust algorithms are presented by employing M-estimation with Huber loss function,M-estimation with interquartile range(IQR)and nonparametric kernel density estimation(NKDE)function respectively to set the penalty weight.Comparison experiments are first carried out based on the UCI standard data sets to verify the effectiveness of these methods,and then the data-driven PS model based on the robust algorithms are established and verified.Experimental results show that the RSCN has an excellent performance for the PS estimation.展开更多
To investigate effect of metallic ion activation on different particle sizes of quartz in butyl xanthate solution,six common ions(Pb^(2+),Cu^(2+),Fe^(3+),Fe^(2+),Mg^(2+) and Ca^(2+)) were introduced as activators.The ...To investigate effect of metallic ion activation on different particle sizes of quartz in butyl xanthate solution,six common ions(Pb^(2+),Cu^(2+),Fe^(3+),Fe^(2+),Mg^(2+) and Ca^(2+)) were introduced as activators.The approaches of micro-flotation,adsorption test and zeta potential measurement were adopted to reveal the mechanism of ion activation.The results show that Pb^(2+),Cu^(2+) and Fe^(3+) are effective activators for the flotation of quartz in butyl xanthate solution because of their absorption on activated quartz surface.Average recoveries of fine particles(<37 μm) are greater than those of coarser particles(37-74 μm),suggesting that the former is easier to be activated and more likely to be floated and thus entrained in sulphide concentrate.From another perspective,addition of metallic ions(Pb^(2+),Cu^(2+) and Fe^(3+)) renders zeta potentials move positively,and addition of the same metallic ions and butyl xanthate makes zeta potential drop apparently,which support a mechanism where they adsorb onto quartz surface,resulting in an expected increase in butyl xanthate collector adsorption with a concomitant increase in the flotation recoveries.展开更多
This paper presents the basic principles of particle size measurement and latest industrial results recorded using an innovative optical instrumentation system designed to measure the size distribution of particles in...This paper presents the basic principles of particle size measurement and latest industrial results recorded using an innovative optical instrumentation system designed to measure the size distribution of particles in a pneumatic suspension.The system is non-intrusive and cost-effective.A low-cost CCD camera is used to capture images of the particulate flow field,which is illuminated by a low-cost pulsed laser sheet generator.The particle size distribution is then determined by processing the particle images through the use of novel processing algorithms.Experimental results obtained in the past on a small scale particle flow test rig have demonstrated that the system is capable of measuring the size distribution of pneumatically conveyed particles with an accuracy of a few percent.For the present paper results obtained when testing the system at a 4 MW industrial test facility are presented.Comparisons are made with both off-line reference data achieved through sieving and on-line laser diffraction data recorded using an intrusive,extractive,Malvern Instruments system.In general there is good agreement between results when considering the characteristics and limitations of the individual methodologies.The novel imaging system shows itself to be rugged,practical and useful under genuine industrial conditions.展开更多
Nano hexahydro-1,3,5-trinitro-1,3,5-triazine(RDX) was prepared using a bi-directional rotation mill and dried under different conditions(liquid, temperature and drying). It shows that the samples cake seriously and th...Nano hexahydro-1,3,5-trinitro-1,3,5-triazine(RDX) was prepared using a bi-directional rotation mill and dried under different conditions(liquid, temperature and drying). It shows that the samples cake seriously and the particles grow up obviously by ordinary drying in different liquids at 70 C, which occurs again after vacuum drying. With the increase of temperature, the degrees of caking and aggregation are enhanced.Well dispersed sample maintaining constant particle size is extracted by supercritical drying, especially freeze drying. Furthermore, the mechanical sensitivities of I-RDX, O-RDX and F-RDX, of which the average sizes are 88.03 mm, 15.32 mm and 0.16 mm, respectively, are evaluated. Compared with I-RDX, the friction, impact and shock sensitivities of O-RDX are slightly lower. However, the friction, impact and shock sensitivities of F-RDX are reduced by 30%, 99.0% and 59.9%, respectively.展开更多
This paper tried to analyze the particle size characteristics of the soil samples in Shuifang Spring catchment area,Jinfo Mt.,Chongqing with different land use patterns that are horse race grassland, rhododendron bush...This paper tried to analyze the particle size characteristics of the soil samples in Shuifang Spring catchment area,Jinfo Mt.,Chongqing with different land use patterns that are horse race grassland, rhododendron bush,bamboos,and the grassland near the Shuifang spring.The different land usepattern in karst area is of great affection to the particle size characteristics of soil.The median diameter of the karst surface layer soil becomes gradually smaller and smaller in following sequence:horse race grassland,grassland near the Shuifang Spring,展开更多
Effects of particle size and chain length on flotation of quaternary ammonium salts (QAS) onto kaolinite have been investigated by mico-flotation tests. The two kinds of quaternary ammonium salts [RN(CH3)3] with diffe...Effects of particle size and chain length on flotation of quaternary ammonium salts (QAS) onto kaolinite have been investigated by mico-flotation tests. The two kinds of quaternary ammonium salts [RN(CH3)3] with different chain lengths, dodecyltrimethylammonium chloride (DTAC) and cetyltrimethylammonium chloride (CTAC) were used as collectors for kaolinite in different particle size fractions (0.075–0.01 mm, 0.045–0.075 mm, 0–0.045 mm). The anomalous flotation behavior of kaolinite have been further explained based on crystal structure considerations by adsorption tests and molecular dynamics (MD) simulation. The results show that the flotation recovery of kaolinite in all different particle size fractions decreases with an increase in pH when DTAC and CTAC are used as collectors. As the concentration of collectors increases, the flotation recovery increases. The longer the carbon chain of QAS is, the higher the recoveries of coarse kaolinite (0.075–0.01 mm and 0.045–0.075 mm) are. But the flotation recovery of the finest kaolinite (0–0.045 mm) decreases with chain lengths of QAS collectors increasing, which is consistent with the flotation results of unsifted kaolinite (0–0.075 mm). It is explained by the froth stability related to the residual concentration of QAS collector. In lower residual concentration, the froth stability becomes worse. Within the range of flotation collector concentration, it's easy of CTAC to be completely adsorbed by kaolinite in the particle size fraction (0–0.045 mm), which led to lower flotation recovery. Moreover, it is interesting that the particle size of kaolinite is coarser, the flotation recovery is higher. The anomalous flotation behavior of kaolinite is rationalized based on crystal structure considerations. The results of MD simulations show that the (001) kaolinite surface has the strongest interaction with DTAC, compared with the (001), (010) and (110) surfaces. On the other hand, when particle size of kaolinite is altered, the number of basal planes and edge planes is changed. It is observed that the finer kaolinite particles size become, the greater relative surface area of edges is, and the more the number of edges is. It means that fine kaolinite particles have more edges to adsorb less cationic colletors than that of coarse kaolinite particles, which is responsible for the poorer floatability of fine kaolinite.展开更多
In this paper,the effects of four sorts of silica with the particle size range of 4～10μm on coated paper properties and printing performance were studied.The results showed that the smaller particle size silica can ...In this paper,the effects of four sorts of silica with the particle size range of 4～10μm on coated paper properties and printing performance were studied.The results showed that the smaller particle size silica can provide the coated paper with higher density and contrast, better definition and good printing performance.展开更多
Biological column leaching of Ni from low-grade Ni ore was studied,and the effects of ore particle size on leaching rate were investigated.The Ni ore with an average Ni content of 0.23%was crushed into four different ...Biological column leaching of Ni from low-grade Ni ore was studied,and the effects of ore particle size on leaching rate were investigated.The Ni ore with an average Ni content of 0.23%was crushed into four different particle size fractions:>10 mm,5−10 mm,2−5 mm and<2 mm.The main strain components at the genus level were acidithiobacillus(53.11%),leptospirillum(43.52%),and acidiphilium(3.37%).The leaching tests were carried out at pH 2.0 and~23℃.The Ni leaching rates from ores with particle sizes>10 mm(bioleaching),5–10 mm(acid leaching),5–10 mm(bioleaching),and 2–5 mm(bioleaching)were 23.76%,22.15%,32.42%and 54.17%,respectively,after 180 d of bioleaching.The ore particle size changed after leaching,compared with the original ore size,the proportion of the same size of 2−5 mm ore decreased to 44.64%.Ore with particle size of 2–5 mm was most suitable for column bioleaching,and effective Ni extraction was achieved with appropriate control of ore granularity.展开更多
Multi-grain chips processed by screw extrusion processing have high nutrition and production value with a low glycemic index.To analyze the effects of particle sizes on the qualities of multi-grain chips extrusion pro...Multi-grain chips processed by screw extrusion processing have high nutrition and production value with a low glycemic index.To analyze the effects of particle sizes on the qualities of multi-grain chips extrusion processing by using a single screw extruder,mesh numbers were selected as 80,100 and 120 to describe different grain particle sizes.It was found that the particle sizes of the raw materials had effects on the basic components,sensory properties,texture properties,antioxidant activities and in vitro digestibilities of extruded chips.The results showed that with the decrease of particle sizes,the moisture contents,starch contents of the chips decreased,and fat contents,dietary fiber contents increased.The edible qualities of the chips increased with the decrease of the grain sizes of raw materials.The antioxidant capacities and estimated glycemic indexes of the three kinds of chips showed a trend of decreasing first,and then increasing with the decrease of particle sizes.Correlation analysis showed that the total antioxidant capacities of chips were negatively correlated with the estimated glycemic indexes.The research results provided valuable guidance for the quality processing of multi-grain chips under extrusion processing.展开更多
The effective medium approximation (EMA) theory is the basis of a capacitance sensor used for concen-tration measurementof a particulate solid flow, its measurementresultis independenton particle size. In existence of...The effective medium approximation (EMA) theory is the basis of a capacitance sensor used for concen-tration measurementof a particulate solid flow, its measurementresultis independenton particle size. In existence ofparticle agglomeration or aggradation, however, it is found that the effective permittivity of a gas/solid mixture is de-pendent on particle size. In this paper, a parallel plate, differential capacitance sensor is utilized to investigate theinfluence of particle size on the effective permittivity of the mixture in such a case. Static experiments using threematerials including glass, limestone and quartz particles were carried out in an off-line manner. The volume fractionof particles being tested ranged from20×10-6to 600×10-6, while the particle size was between 3 and 100μm.Experimental results showthat the effective permittivity of a particle-gas mixture with particle agglomeration is largerthan that predicted by EMA and the smaller the particle size, the larger the effective permittivity. The experimentprocess and analysis results are discussed in detail in the paper.展开更多
In order to deal with the disadvantages of excessive grinding and non-uniformity in finished particle under high-pressure grinding rolls （HPGR） finished grinding system, four aspects were investigated, including eva...In order to deal with the disadvantages of excessive grinding and non-uniformity in finished particle under high-pressure grinding rolls （HPGR） finished grinding system, four aspects were investigated, including evaluating indicators, effects of operating factors, effect of particle uniformity on the flotation and formation mechanism of particle uniformity. Experiment of HPGR finished grinding system, cationic reverse flotation experiment and simulation test of particle bed comminution under the condition of quasi-static were carried out. Theoretical analyses indicated that both of uniformity coefficient and average particle size should be included in the uniformity analysis of the mineral particles. The results show that the effect of circulation fan impeller speed on particle uniformity is the most evident, HPGR working pressure and roll gap are second and HPGR roller speed is the last. Average particle size has a more obvious effect on the grade of flotation concentrate while uniformity coefficient has a more obvious effect on the flotation recovery. Considering the two aspects of grade and recovery, the optimal uniformity coefficient for flotation is 1.1-1.2 and the optimal average particle size for flotation is 50-55 μm. The operating factors which promote the shielding effect and compact effect in the HPGR finished grinding system should be strengthened based on the uniformity of particles.展开更多
基金the National Natural Science Foundation of China (Grant No.22105184)Research Fund of SWUST for PhD (Grant No.22zx7175)+1 种基金Sichuan Science and Technology Program (Grant No.2019ZDZX0013)Institute of Chemical Materials Program (Grant No.SXK-2022-03)for financial support。
文摘High purity and ultrafine DAAF(u-DAAF)is an emerging insensitive charge in initiators.Although there are many ways to obtain u-DAAF,developing a preparation method with stable operation,accurate control,good quality consistency,equipment miniaturization,and minimum manpower is an inevitable requirement to adapt to the current social technology development trend.Here reported is the microfluidic preparation of u-DAAF with tunable particle size by a passive swirling microreactor.Under the guidance of recrystallization growth kinetics and mixing behavior of fluids in the swirling microreactor,the key parameters(liquid flow rate,explosive concentration and crystallization temperature)were screened and optimized through screening experiments.Under the condition that no surfactant is added and only experimental parameters are controlled,the particle size of recrystallized DAAF can be adjusted from 98 nm to 785 nm,and the corresponding specific surface area is 8.45 m^(2)·g^(-1)to 1.33 m^(2)·g^(-1).In addition,the preparation method has good batch stability,high yield(90.8%-92.6%)and high purity(99.0%-99.4%),indicating a high practical application potential.Electric explosion derived flyer initiation tests demonstrate that the u-DAAF shows an initiation sensitivity much lower than that of the raw DAAF,and comparable to that of the refined DAAF by conventional spraying crystallization method.This study provides an efficient method to fabricate u-DAAF with narrow particle size distribution and high reproducibility as well as a theoretical reference for fabrication of other ultrafine explosives.
基金Project(51901095)supported by the National Natural Science Foundation of China。
文摘To study the influence of B4C particle size on the microstructure and damping capacities of(B_(4)C+Ti)/Mg composites,in situ reactive infiltration technique was utilized to prepare Mg-matrix composites.The microstructure,produced phases and damping capacities of the composites prepared with different particle size of B4C were characterized and analyzed.The results show that the reaction between B4C and Ti tends to be more complete when finer B_(4)C particle was used to prepare the composites.But the microstructure of the as-prepared composites is more homogenous when B4C and Ti have similar particle size.The strain-dependent damping capacities of(B_(4)C+Ti)/Mg composites improve gradually with the increase of strain amplitude,and composites prepared with coarser B4C particles tend to have higher damping capacities.The temperature-dependent damping capacities improve with increasing the measuring temperatures,and the kind of damping capacities of the composites prepared with 5mm B4C are inferior to those of coarser particles.The dominant damping mechanism for the strain-damping capacity is dislocation damping and plastic zone damping,while that for the temperature-damping capacity is interface damping or grain boundary damping.
基金the support of Key Laboratory of Special Energy Materials,Ministry of Education,Nanjing,210094,China.
文摘Particle size and content of RDX are the two main factors that affect the burning stability of RDX-based propellants. However, these effects and the corresponding mechanisms are still controversial. In this work, we investigated the physicochemical processes during burning and the corresponding mechanisms through the technologies of structure compactness analysis on the base of voidage measurement and theoretical interfacial area estimation, apparent burning rate measurement using closed vessel(CV)and extinguished burning surface characterization relying on interrupted closed vessel(ICV) and scanning electron microscope(SEM). The results indicate that the voidage increased with the increase of RDX content and particle size due to the increasing interfacial area and increasing interface gap size,respectively. The apparent burning rate increased with the increase of RDX particle size because of the decreasing RDX specific surface area on the burning surface, which could decrease the heat absorbing rates of the melting and evaporation processes of RDX in the condensed phase. Similarly, the apparent burning rate decreased with the increase of RDX content at pressures lower than around 55 MPa due to the increasing RDX specific surface area. Whereas, an opposite trend could be observed at pressures higher than around 55 MPa, which was attributed to the increasing heat feedback from the gas phase as the result of the increasing propellant energy. For propellants containing very coarse RDX particles, such as 97.8 and 199.4 μm average size, the apparent burning rate increased stably with a flat extinguished surface at pressures lower than around 30 MPa, while increased sharply above around 30 MPa with the extinguished surface becoming more and more rugged as the pressure increased. In addition, the turning degree of u-p curve increased with the increase of coarse RDX content and particle size, and could be reduced by improving the structure compactness.
基金Projects(61603393,61741318)supported in part by the National Natural Science Foundation of ChinaProject(BK20160275)supported by the Natural Science Foundation of Jiangsu Province,China+1 种基金Project(2015M581885)supported by the Postdoctoral Science Foundation of ChinaProject(PAL-N201706)supported by the Open Project Foundation of State Key Laboratory of Synthetical Automation for Process Industries of Northeastern University,China
文摘As a production quality index of hematite grinding process,particle size(PS)is hard to be measured in real time.To achieve the PS estimation,this paper proposes a novel data driven model of PS using stochastic configuration network(SCN)with robust technique,namely,robust SCN(RSCN).Firstly,this paper proves the universal approximation property of RSCN with weighted least squares technique.Secondly,three robust algorithms are presented by employing M-estimation with Huber loss function,M-estimation with interquartile range(IQR)and nonparametric kernel density estimation(NKDE)function respectively to set the penalty weight.Comparison experiments are first carried out based on the UCI standard data sets to verify the effectiveness of these methods,and then the data-driven PS model based on the robust algorithms are established and verified.Experimental results show that the RSCN has an excellent performance for the PS estimation.
基金Project(51274255)supported by the National Natural Science Foundation of ChinaProject(2015CX005)supported by Innovation Driven Plan of Central South University,China+1 种基金Project(2016RS2016)supported by Hunan Provincial Science and Technology Leader(Innovation Team of Interface Chemistry of Efficient and Clean Utilization of Complex Mineral Resources),ChinaProject supported by the Postdoctoral Research Station of Central South University,China
文摘To investigate effect of metallic ion activation on different particle sizes of quartz in butyl xanthate solution,six common ions(Pb^(2+),Cu^(2+),Fe^(3+),Fe^(2+),Mg^(2+) and Ca^(2+)) were introduced as activators.The approaches of micro-flotation,adsorption test and zeta potential measurement were adopted to reveal the mechanism of ion activation.The results show that Pb^(2+),Cu^(2+) and Fe^(3+) are effective activators for the flotation of quartz in butyl xanthate solution because of their absorption on activated quartz surface.Average recoveries of fine particles(<37 μm) are greater than those of coarser particles(37-74 μm),suggesting that the former is easier to be activated and more likely to be floated and thus entrained in sulphide concentrate.From another perspective,addition of metallic ions(Pb^(2+),Cu^(2+) and Fe^(3+)) renders zeta potentials move positively,and addition of the same metallic ions and butyl xanthate makes zeta potential drop apparently,which support a mechanism where they adsorb onto quartz surface,resulting in an expected increase in butyl xanthate collector adsorption with a concomitant increase in the flotation recoveries.
文摘This paper presents the basic principles of particle size measurement and latest industrial results recorded using an innovative optical instrumentation system designed to measure the size distribution of particles in a pneumatic suspension.The system is non-intrusive and cost-effective.A low-cost CCD camera is used to capture images of the particulate flow field,which is illuminated by a low-cost pulsed laser sheet generator.The particle size distribution is then determined by processing the particle images through the use of novel processing algorithms.Experimental results obtained in the past on a small scale particle flow test rig have demonstrated that the system is capable of measuring the size distribution of pneumatically conveyed particles with an accuracy of a few percent.For the present paper results obtained when testing the system at a 4 MW industrial test facility are presented.Comparisons are made with both off-line reference data achieved through sieving and on-line laser diffraction data recorded using an intrusive,extractive,Malvern Instruments system.In general there is good agreement between results when considering the characteristics and limitations of the individual methodologies.The novel imaging system shows itself to be rugged,practical and useful under genuine industrial conditions.
文摘Nano hexahydro-1,3,5-trinitro-1,3,5-triazine(RDX) was prepared using a bi-directional rotation mill and dried under different conditions(liquid, temperature and drying). It shows that the samples cake seriously and the particles grow up obviously by ordinary drying in different liquids at 70 C, which occurs again after vacuum drying. With the increase of temperature, the degrees of caking and aggregation are enhanced.Well dispersed sample maintaining constant particle size is extracted by supercritical drying, especially freeze drying. Furthermore, the mechanical sensitivities of I-RDX, O-RDX and F-RDX, of which the average sizes are 88.03 mm, 15.32 mm and 0.16 mm, respectively, are evaluated. Compared with I-RDX, the friction, impact and shock sensitivities of O-RDX are slightly lower. However, the friction, impact and shock sensitivities of F-RDX are reduced by 30%, 99.0% and 59.9%, respectively.
文摘This paper tried to analyze the particle size characteristics of the soil samples in Shuifang Spring catchment area,Jinfo Mt.,Chongqing with different land use patterns that are horse race grassland, rhododendron bush,bamboos,and the grassland near the Shuifang spring.The different land usepattern in karst area is of great affection to the particle size characteristics of soil.The median diameter of the karst surface layer soil becomes gradually smaller and smaller in following sequence:horse race grassland,grassland near the Shuifang Spring,
文摘Effects of particle size and chain length on flotation of quaternary ammonium salts (QAS) onto kaolinite have been investigated by mico-flotation tests. The two kinds of quaternary ammonium salts [RN(CH3)3] with different chain lengths, dodecyltrimethylammonium chloride (DTAC) and cetyltrimethylammonium chloride (CTAC) were used as collectors for kaolinite in different particle size fractions (0.075–0.01 mm, 0.045–0.075 mm, 0–0.045 mm). The anomalous flotation behavior of kaolinite have been further explained based on crystal structure considerations by adsorption tests and molecular dynamics (MD) simulation. The results show that the flotation recovery of kaolinite in all different particle size fractions decreases with an increase in pH when DTAC and CTAC are used as collectors. As the concentration of collectors increases, the flotation recovery increases. The longer the carbon chain of QAS is, the higher the recoveries of coarse kaolinite (0.075–0.01 mm and 0.045–0.075 mm) are. But the flotation recovery of the finest kaolinite (0–0.045 mm) decreases with chain lengths of QAS collectors increasing, which is consistent with the flotation results of unsifted kaolinite (0–0.075 mm). It is explained by the froth stability related to the residual concentration of QAS collector. In lower residual concentration, the froth stability becomes worse. Within the range of flotation collector concentration, it's easy of CTAC to be completely adsorbed by kaolinite in the particle size fraction (0–0.045 mm), which led to lower flotation recovery. Moreover, it is interesting that the particle size of kaolinite is coarser, the flotation recovery is higher. The anomalous flotation behavior of kaolinite is rationalized based on crystal structure considerations. The results of MD simulations show that the (001) kaolinite surface has the strongest interaction with DTAC, compared with the (001), (010) and (110) surfaces. On the other hand, when particle size of kaolinite is altered, the number of basal planes and edge planes is changed. It is observed that the finer kaolinite particles size become, the greater relative surface area of edges is, and the more the number of edges is. It means that fine kaolinite particles have more edges to adsorb less cationic colletors than that of coarse kaolinite particles, which is responsible for the poorer floatability of fine kaolinite.
文摘In this paper,the effects of four sorts of silica with the particle size range of 4～10μm on coated paper properties and printing performance were studied.The results showed that the smaller particle size silica can provide the coated paper with higher density and contrast, better definition and good printing performance.
基金Project(U1608254)supported by the Special Fund for the National Natural Science Foundation of ChinaProjects(ZJKY2017(B)KFJJ01,ZJKY2017(B)KFJJ02)supported by the Zijin Mining Group Co.,Ltd.,China。
文摘Biological column leaching of Ni from low-grade Ni ore was studied,and the effects of ore particle size on leaching rate were investigated.The Ni ore with an average Ni content of 0.23%was crushed into four different particle size fractions:>10 mm,5−10 mm,2−5 mm and<2 mm.The main strain components at the genus level were acidithiobacillus(53.11%),leptospirillum(43.52%),and acidiphilium(3.37%).The leaching tests were carried out at pH 2.0 and~23℃.The Ni leaching rates from ores with particle sizes>10 mm(bioleaching),5–10 mm(acid leaching),5–10 mm(bioleaching),and 2–5 mm(bioleaching)were 23.76%,22.15%,32.42%and 54.17%,respectively,after 180 d of bioleaching.The ore particle size changed after leaching,compared with the original ore size,the proportion of the same size of 2−5 mm ore decreased to 44.64%.Ore with particle size of 2–5 mm was most suitable for column bioleaching,and effective Ni extraction was achieved with appropriate control of ore granularity.
基金Support by the National Key Research and Development Project of the 13th Five-Year Plan,China(2017YFD0401204)。
文摘Multi-grain chips processed by screw extrusion processing have high nutrition and production value with a low glycemic index.To analyze the effects of particle sizes on the qualities of multi-grain chips extrusion processing by using a single screw extruder,mesh numbers were selected as 80,100 and 120 to describe different grain particle sizes.It was found that the particle sizes of the raw materials had effects on the basic components,sensory properties,texture properties,antioxidant activities and in vitro digestibilities of extruded chips.The results showed that with the decrease of particle sizes,the moisture contents,starch contents of the chips decreased,and fat contents,dietary fiber contents increased.The edible qualities of the chips increased with the decrease of the grain sizes of raw materials.The antioxidant capacities and estimated glycemic indexes of the three kinds of chips showed a trend of decreasing first,and then increasing with the decrease of particle sizes.Correlation analysis showed that the total antioxidant capacities of chips were negatively correlated with the estimated glycemic indexes.The research results provided valuable guidance for the quality processing of multi-grain chips under extrusion processing.
文摘The effective medium approximation (EMA) theory is the basis of a capacitance sensor used for concen-tration measurementof a particulate solid flow, its measurementresultis independenton particle size. In existence ofparticle agglomeration or aggradation, however, it is found that the effective permittivity of a gas/solid mixture is de-pendent on particle size. In this paper, a parallel plate, differential capacitance sensor is utilized to investigate theinfluence of particle size on the effective permittivity of the mixture in such a case. Static experiments using threematerials including glass, limestone and quartz particles were carried out in an off-line manner. The volume fractionof particles being tested ranged from20×10-6to 600×10-6, while the particle size was between 3 and 100μm.Experimental results showthat the effective permittivity of a particle-gas mixture with particle agglomeration is largerthan that predicted by EMA and the smaller the particle size, the larger the effective permittivity. The experimentprocess and analysis results are discussed in detail in the paper.
基金Project(2013EG132088)supported by Special Program for Research Institutes of the Ministry of Science and Technology,ChinaProject(12010402c187)supported by Key Science and Technology Program of Anhui Province,China
文摘In order to deal with the disadvantages of excessive grinding and non-uniformity in finished particle under high-pressure grinding rolls （HPGR） finished grinding system, four aspects were investigated, including evaluating indicators, effects of operating factors, effect of particle uniformity on the flotation and formation mechanism of particle uniformity. Experiment of HPGR finished grinding system, cationic reverse flotation experiment and simulation test of particle bed comminution under the condition of quasi-static were carried out. Theoretical analyses indicated that both of uniformity coefficient and average particle size should be included in the uniformity analysis of the mineral particles. The results show that the effect of circulation fan impeller speed on particle uniformity is the most evident, HPGR working pressure and roll gap are second and HPGR roller speed is the last. Average particle size has a more obvious effect on the grade of flotation concentrate while uniformity coefficient has a more obvious effect on the flotation recovery. Considering the two aspects of grade and recovery, the optimal uniformity coefficient for flotation is 1.1-1.2 and the optimal average particle size for flotation is 50-55 μm. The operating factors which promote the shielding effect and compact effect in the HPGR finished grinding system should be strengthened based on the uniformity of particles.
