Two different kinds of experimental techniques were used to in-situ study the austenite formation during intercritical annealing in C-Mn dual phase steel. The microstructure evolution was observed by confocal laser sc...Two different kinds of experimental techniques were used to in-situ study the austenite formation during intercritical annealing in C-Mn dual phase steel. The microstructure evolution was observed by confocal laser scanning microscope, and the austenite isothermal and non-isothermal transformation kinetics were studied by dilatometry. The results indicate that banded structure is produced for the reason of composition segregation and the competition between recrystallization and phase transformation. Austenite prefers to nucleate not only at ferrite/ferrite grain boundaries, but also inside the grains of ferrite.Furthermore, the austenitizing process is accomplished mainly via migration of the existing austenite/ferrite interface rather than nucleation of new grains. The incubation process can be divided into two stages which are controlled by carbon and manganese diffusion, respectively. During the incubation process, the nucleation rate of austenite decreases, and austenite growth changes from two-dimensional to one-dimensional. The partitioning coefficient, defined as the ratio of manganese content in the austenite to that in the adjacent ferrite, increases with increasing soaking time.展开更多
The convection in melt crystal growth influences the crystal integrity deeply.During space crystal growth,the buoyancy driven convection has been eliminated for the microgravity environment,therefroe,surface tension d...The convection in melt crystal growth influences the crystal integrity deeply.During space crystal growth,the buoyancy driven convection has been eliminated for the microgravity environment,therefroe,surface tension driven convection (Marangoni Convection) become the main convection form.But the Marangoni convection forms,starting condition,development process and its influence on crystal growth are still unclear now.At the present time,Many studies focused on simulating liquid Marangoni convection or numerical simulation.However,few studies concerned on real melt,especially on oxide melt. In this paper,an in situ observation is carried out to study the start and development of Marangoni convection of Bi 12 SiO 20 melt in a 2mm diameter loop like platinum crucible.The different states of steady convection and the transition from steady to oscillatory convection are observed.The critical Marangoni number is obtained as 22433 and it agreed with a dependence Ma c=2884Pr 0.638 for high Prandtl number melt.The authors also obtained a dependence of convection oscillatory frequency on melt temperature.It increases with temperature rising.展开更多
Sodium chlorate is a no coloured,no smell and no poisonous transparent crystal with the formula of NaClO 3.Its structure belongs to the cubic( T 23)class and exhibits optical activity.The space group is P 2 13 and the...Sodium chlorate is a no coloured,no smell and no poisonous transparent crystal with the formula of NaClO 3.Its structure belongs to the cubic( T 23)class and exhibits optical activity.The space group is P 2 13 and there are four molecules per cubic unit cell with a =0.6570nm.We chose the crystal as a research system based on two reasons:(1)since the crystal structure belongs to the cubic class,the crystal faces,such as(100),(010),(001)are possessed of homogeneity,it is the suitable system for studying kinetics of crystal growth;(2)since the solubility of the NaClO 3 is higher in the H 2O and the crystal could be grown from low temperature solution,this is a suitable system for studying a influence of gravity on the boundary layer characteristics of the crystal growth under the microgravity condition.展开更多
基金Project(2013AA031601)supported by the National High Technology Research and Development Program of ChinaProject(2012BAF04B01)supported by the National Science and Technology Pillar Program During the 12th Five-year Plan Period of China
文摘Two different kinds of experimental techniques were used to in-situ study the austenite formation during intercritical annealing in C-Mn dual phase steel. The microstructure evolution was observed by confocal laser scanning microscope, and the austenite isothermal and non-isothermal transformation kinetics were studied by dilatometry. The results indicate that banded structure is produced for the reason of composition segregation and the competition between recrystallization and phase transformation. Austenite prefers to nucleate not only at ferrite/ferrite grain boundaries, but also inside the grains of ferrite.Furthermore, the austenitizing process is accomplished mainly via migration of the existing austenite/ferrite interface rather than nucleation of new grains. The incubation process can be divided into two stages which are controlled by carbon and manganese diffusion, respectively. During the incubation process, the nucleation rate of austenite decreases, and austenite growth changes from two-dimensional to one-dimensional. The partitioning coefficient, defined as the ratio of manganese content in the austenite to that in the adjacent ferrite, increases with increasing soaking time.
文摘The convection in melt crystal growth influences the crystal integrity deeply.During space crystal growth,the buoyancy driven convection has been eliminated for the microgravity environment,therefroe,surface tension driven convection (Marangoni Convection) become the main convection form.But the Marangoni convection forms,starting condition,development process and its influence on crystal growth are still unclear now.At the present time,Many studies focused on simulating liquid Marangoni convection or numerical simulation.However,few studies concerned on real melt,especially on oxide melt. In this paper,an in situ observation is carried out to study the start and development of Marangoni convection of Bi 12 SiO 20 melt in a 2mm diameter loop like platinum crucible.The different states of steady convection and the transition from steady to oscillatory convection are observed.The critical Marangoni number is obtained as 22433 and it agreed with a dependence Ma c=2884Pr 0.638 for high Prandtl number melt.The authors also obtained a dependence of convection oscillatory frequency on melt temperature.It increases with temperature rising.
文摘Sodium chlorate is a no coloured,no smell and no poisonous transparent crystal with the formula of NaClO 3.Its structure belongs to the cubic( T 23)class and exhibits optical activity.The space group is P 2 13 and there are four molecules per cubic unit cell with a =0.6570nm.We chose the crystal as a research system based on two reasons:(1)since the crystal structure belongs to the cubic class,the crystal faces,such as(100),(010),(001)are possessed of homogeneity,it is the suitable system for studying kinetics of crystal growth;(2)since the solubility of the NaClO 3 is higher in the H 2O and the crystal could be grown from low temperature solution,this is a suitable system for studying a influence of gravity on the boundary layer characteristics of the crystal growth under the microgravity condition.
