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Experimental and numerical study on dynamic mechanical behaviors of shale under true triaxial compression at high strain rate
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作者 Xiaoping Zhou Linyuan Han +1 位作者 Jing Bi Yundong Shou 《International Journal of Mining Science and Technology》 SCIE EI CAS CSCD 2024年第2期149-165,共17页
High-energy gas fracturing of shale is a novel,high efficacy and eco-friendly mining technique,which is a typical dynamic perturbing behavior.To effectively extract shale gas,it is important to understand the dynamic ... High-energy gas fracturing of shale is a novel,high efficacy and eco-friendly mining technique,which is a typical dynamic perturbing behavior.To effectively extract shale gas,it is important to understand the dynamic mechanical properties of shale.Dynamic experiments on shale subjected to true triaxial compression at different strain rates are first conducted in this research.The dynamic stress-strain curves,peak strain,peak stress and failure modes of shale are investigated.The results of the study indicate that the intermediate principal stress and the minor principal stress have the significant influence on the dynamic mechanical behaviors,although this effect decreases as the strain rate increases.The characteristics of compression-shear failure primarily occur in shale subjected to triaxial compression at high strain rates,which distinguishes it from the fragmentation characteristics observed in shale under dynamic uniaxial compression.Additionally,a numerical three-dimensional Split Hopkinson Pressure Bar(3D-SHPB),which is established by coupling PFC3D and FLAC3D methods,is validated to replicate the laboratory characteristics of shale.The dynamic mechanical characteristics of shale subjected to different confining stresses are systematically investigated by the coupling PFC3D and FLAC3D method.The numerical results are in good agreement with the experimental data. 展开更多
关键词 Dynamic behaviors True triaxial compression high strain rates Dynamic failure mechanism PFC3D-FLAC3D coupled method
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Preparation and performance evaluation of the slickwater using novel polymeric drag reducing agent with high temperature and shear resistance ability
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作者 Ming-Wei Zhao Zhen-Feng Ma +5 位作者 Cai-Li Dai WeiWu Yong-Quan Sun Xu-Guang Song Yun-Long Cheng Xiang-Yu Wang 《Petroleum Science》 SCIE EI CAS CSCD 2024年第2期1113-1121,共9页
Slickwater fracturing fluids are widely used in the development of unconventional oil and gas resources due to the advantages of low cost,low formation damage and high drag reduction performance.However,their performa... Slickwater fracturing fluids are widely used in the development of unconventional oil and gas resources due to the advantages of low cost,low formation damage and high drag reduction performance.However,their performance is severely affected at high temperatures.Drag reducing agent is the key to determine the drag reducing performance of slickwater.In this work,in order to further improve the temperature resistance of slickwater,a temperature-resistant polymeric drag reducing agent(PDRA)was synthesized and used as the basis for preparing the temperature-resistant slickwater.The slickwater system was prepared with the compositions of 0.2 wt%PDRA,0.05 wt%drainage aid nonylphenol polyoxyethylene ether phosphate(NPEP)and 0.5 wt%anti-expansion agent polyepichlorohydrindimethylamine(PDM).The drag reduction ability,rheology properties,temperature and shear resistance ability,and core damage property of slickwater were systematically studied and evaluated.In contrast to on-site drag reducing agent(DRA)and HPAM,the temperature-resistant slickwater demonstrates enhanced drag reduction efficacy at 90℃,exhibiting superior temperature and shear resistance ability.Notably,the drag reduction retention rate for the slickwater achieved an impressive 90.52%after a 30-min shearing period.Additionally,the core damage is only 5.53%.We expect that this study can broaden the application of slickwater in high-temperature reservoirs and provide a theoretical basis for field applications. 展开更多
关键词 Unconventional resources Polymeric drag reducing agent Slickwater high drag reduction rate temperature resistance
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Effect Analysis of High Strain Rate and Anisotropy on Tension⁃Compression Asymmetry of Aluminum Alloy 7050 被引量:2
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作者 FU Xiuli SHI Qihang +1 位作者 WANG Hui PAN Yongzhi 《Transactions of Nanjing University of Aeronautics and Astronautics》 EI CSCD 2020年第3期377-384,共8页
Using the devices of split Hopkinson tension bar(SHTB)and split Hopkinson pressure bar(SHPB),the dynamic tension and compression experiments in three typical forming directions(rolling direction(RD),transverse directi... Using the devices of split Hopkinson tension bar(SHTB)and split Hopkinson pressure bar(SHPB),the dynamic tension and compression experiments in three typical forming directions(rolling direction(RD),transverse direction(TD)and normal direction(ND))were carried out at strain rates of 1000,2000 and 4000 s-1,respectively.From the microscopic point of view,the effect of strain rate and anisotropy on tension compression asymmetry of aviation aluminum alloy 7050 was studied by scanning electron microscope(SEM),metallographic microscope and electron backscatter diffraction(EBSD).The results showed that there was obvious asymmetry between tension and compression,especially that the yield strength of the material in tension was higher than that in compression.The asymmetry in the elastic stage of tension-compression was weaker and the asymmetry in the strengthening stage was stronger with the increase of strain rate.At the same strain rate,the changing trend of the flow stress was distinct under different orientations of tension and compression,which was related to the stress direction of the grains.According to EBSD grain orientation analysis and raw material texture pole figure analysis,it was found that the larger the difference in the degree of grain refinement during tension and compression,the larger the macro-flow stress difference. 展开更多
关键词 aluminum alloy TEXTURE high strain rate ANISOTROPY tension-compression asymmetry
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Effects of strain rates on mechanical properties of limestone under high temperature 被引量:10
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作者 Tang Furong Mao Xianbiao +2 位作者 Zhang Lianying Yin Huiguang Li Yan 《Mining Science and Technology》 EI CAS 2011年第6期857-861,共5页
The experimental tests for limestone specimens at 700 °C in uniaxial compression were carried out to inves- tigate the mechanical effects of loading rates on limestone by using a MTS810 rock mechanics servo- cont... The experimental tests for limestone specimens at 700 °C in uniaxial compression were carried out to inves- tigate the mechanical effects of loading rates on limestone by using a MTS810 rock mechanics servo- controlled testing system considering the loading rate as a variable. The mechanical properties of limestone such as the stress-strain curve, variable characteristics of peak strength and the modulus of elasticity of limestone were studied under the strain rates ranging from 1.1 10à5 to 1.1 10à1 sà1. (1) Sharp decreases were shown for the peak strength and elastic modulus of limestone from 1.1 10à5 to 1.1 10à4 sà1 at 700 °C as well as a downward trend was shown from 1.1 10à4 to 1.1 10à1 sà1 with the rise of the strain rate. (2) The peak strain increased from 1.1 10à5 to 1.1 10à4 sà1, however, there was no obvious changes shown for the peak strain of limestone from 1.1 10à4 to 1.1 10à1 sà1. These results can provide valuable references for the rock blasting effect and design of mine. 展开更多
关键词 strain rates high temperature Mechanical properties Limestone
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Dynamic necking of a near α titanium alloy at high strain rates:Experiments and modelling
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作者 Long-hui Zhang Antonio Pellegrino Nik Petrinic 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2021年第4期1126-1134,共9页
The tensile behaviour of near a Ti3Al2.5 V alloy,conceived for applications in aerospace and automotive engineering,is characterized from quasi-static to high strain rates.The material is found to present noticeable s... The tensile behaviour of near a Ti3Al2.5 V alloy,conceived for applications in aerospace and automotive engineering,is characterized from quasi-static to high strain rates.The material is found to present noticeable strain rate sensitivity.The dynamic true strain rate in the necking cross-section reaches values up to ten times higher than the nominal strain rate.It is also observed that beyond necking the dynamic true stress-strain curves present limited rate dependence.The experimental results at different strain rates are used to determine a suitable constitutive model for finite element simulations of the dynamic tensile tests.The model predicts the experimentally macroscopic force-time response,true stress-strain response and effective strain rate evolution with good agreement. 展开更多
关键词 Nearαtitanium alloy high strain rate Locking effect Constitutive modeling Finite element simulation
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HIGH STRAIN RATE SU PERPLASTICITY IN SiCp REINFORCED AZ31 MAGNESIUM MATRIX COMPOSITE 被引量:2
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作者 陈培生 吕庆风 +2 位作者 孙扬善 蒋建清 马爱斌 《Transactions of Nanjing University of Aeronautics and Astronautics》 EI 2001年第1期17-21,共5页
Superplasticity of AZ 31 magnesium matrix composites reinforced with 10 vol% SiC(2 μm) particulate i s investigated at temperature range from 365℃ to 565℃ and strain rate from 2.0 8×10<sup>-3</sup&g... Superplasticity of AZ 31 magnesium matrix composites reinforced with 10 vol% SiC(2 μm) particulate i s investigated at temperature range from 365℃ to 565℃ and strain rate from 2.0 8×10<sup>-3</sup> to 5.21×10<sup>-1</sup> s<sup>-1</sup>. The maximum total elongation of 228 % is obtained at a strain rate of 2.08×10<sup>-1</sup> s<sup>-1</sup>. The strain rate se nsitivity exponent (m) higher than 0.3, is observed when the strain rate is high er than 10<sup>-1</sup> s<sup>-1</sup> at 525℃. Increasing the test temperature to 540℃, the maximum total elongation exceeding 195% is achieved at a higher strain rate of 5.21×10<sup>-1</sup> s<sup>-1</sup> than that at 525℃. SiC in AZ31/SiCp composite ca n fine the matrix grain size. Filament is observed on the fracture surface of th e specimens showing superplasticity. 展开更多
关键词 magnesium alloys SiC p articulate composite high strain rate and superplasticity
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High strain rate compressive strength behavior of cemented paste backfill using split Hopkinson pressure bar 被引量:7
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作者 Xin Chen Xiuzhi Shi +3 位作者 Jian Zhou Enming Li Peiyong Qiu Yonggang Gou 《International Journal of Mining Science and Technology》 SCIE EI CAS CSCD 2021年第3期387-399,共13页
The stability of cemented paste backfill(CPB)is threatened by dynamic disturbance,but the conventional low strain rate laboratory pressure test has difficulty achieving this research purpose.Therefore,a split Hopkinso... The stability of cemented paste backfill(CPB)is threatened by dynamic disturbance,but the conventional low strain rate laboratory pressure test has difficulty achieving this research purpose.Therefore,a split Hopkinson pressure bar(SHPB)was utilized to investigate the high strain rate compressive behavior of CPB with dynamic loads of 0.4,0.8,and 1.2 MPa.And the failure modes were determined by macro and micro analysis.CPB with different cement-to-tailings ratios,solid mass concentrations,and curing ages was prepared to conduct the SHPB test.The results showed that increasing the cement content,tailings content,and curing age can improve the dynamic compressive strength and elastic modulus.Under an impact load,a higher strain rate can lead to larger increasing times of the dynamic compressive strength when compared with static loading.And the dynamic compressive strength of CPB has an exponential correlation with the strain rate.The macroscopic failure modes indicated that CPB is more seriously damaged under dynamic loading.The local damage was enhanced,and fine cracks were formed in the interior of the CPB.This is because the CPB cannot dissipate the energy of the high strain rate stress wave in a short loading period. 展开更多
关键词 high strain rate Compressive strength behavior Cemented paste backfill Split Hopkinson pressure bar TAILINGS
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Influences of Stress Wave Propagation upon Studying Dynamic Response of Materials at High Strain Rates 被引量:4
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作者 王礼立 《Journal of Beijing Institute of Technology》 EI CAS 2004年第3期225-235,共11页
How the wave propagation analysis plays a key role in the studies of dynamic response of materials at high strain rates is analyzed. For the wave propagation technique, the followings are important: the loading and un... How the wave propagation analysis plays a key role in the studies of dynamic response of materials at high strain rates is analyzed. For the wave propagation technique, the followings are important: the loading and unloading constitutive relation presumed, the positions of the sensors embedded, the interactions between loading waves and unloading waves. For the split Hopkinson pressure bar (SHPB) technique, the assumption of one-dimensional stress wave propagation and the assumption of stress uniformity along the specimen should be satisfied. When the larger diameter bars are employed, the wave dispersion effects should be considered, including the high frequency oscillations, non-uniform stress distribution across the bar section, increase of rise time, and amplitude attenuation. The stress uniformity along the specimen is influenced by the reflection times in specimen, the wave impedance ratio of the specimen and the bar, and the waveform. 展开更多
关键词 stress wave dynamic response of materials high strain rates SHPB
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Investigation on the strain of SiGe/Si heteroepitaxial system during high temperature annealing byBiBS/Channeling
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作者 CHENChang-Chun ZHANGShi-Li 《Nuclear Science and Techniques》 SCIE CAS CSCD 2001年第4期295-301,共7页
The influence of the high temperature processing on the strain stored in SiGe hetero-epilayer was studied by means of RBS/Channeling. Channeling angular scan along the ,< 110> axial direction in the (100) plane ... The influence of the high temperature processing on the strain stored in SiGe hetero-epilayer was studied by means of RBS/Channeling. Channeling angular scan along the ,< 110> axial direction in the (100) plane was used to characterize the tetragonal distortion in the SiGe strained layer. The strained crystal structure parameters were acquired by combining the determination of strain with the elasticity theory. It is shown that the strain stored in the SiGe epilayer has significantly change (relaxation factor from 0.023 to 0.84) after high temperature annealing. The potential strain relaxation mechanisms were discussed. 展开更多
关键词 合金薄膜 高温退火 集成电路
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Experimental and numerical investigation on penetration of clay masonry by small high-speed projectile 被引量:2
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作者 Cheng-zong Wang Ai-jun Chen +3 位作者 Zi-qing Li Chao-an Gong Shu Wang Wen-min Yan 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2021年第4期1514-1530,共17页
This study investigates a kind of masonry consisting of clay-fired brick(f_(c)=10 MPa;r=1:38 g/cm^(3))and mortar(f_(c)=10 MPa;r=1:8 g/cm^(3)).Clay-fired brick masonry connotes a traditional construction material of ol... This study investigates a kind of masonry consisting of clay-fired brick(f_(c)=10 MPa;r=1:38 g/cm^(3))and mortar(f_(c)=10 MPa;r=1:8 g/cm^(3)).Clay-fired brick masonry connotes a traditional construction material of old architecture and public buildings.We carried out penetration experiments in which four clay-fired brick walls employing two different patterns were subjected to impact from small high-speed projectile,i.e.12.7 mm armor-piercing explosive incendiary projectile and material tests in which the static and dynamic compressive strengths of clay-fired brick and mortar were determined by quasi-static and SHPB(Split Hopkinson Pressure Bar)tests.The experimental data include hit and exit velocities,damage configuration of clay brick masonry and mechanical properties of material at low and high strain rates,though which influence of thickness and bonding patterns of wall on kinetic loss of bullet,the damage patterns of masonry observed experimentally and dynamic increase of material strengths are analyzed.To keep minimum boundary inconsistency with reality,full 3D detailed finite element model consisting of two different material is established.Sharing common nodes and employing automatic tiebreak contact are combined to reduce computational time usage of large-scale model.For description of clay-fired brick and mortar RiedeleHiermaiereThoma(RHT)material model is employed.Material parameter set is derived based on experimental data,available literature and engineering assumptions.The numerical simulations study the mesh resolution dependency of material model,reproduce the crucial phenomena of masonry in experiment acceptably and offer more time-resolved insight into motion of bullet in the process of penetration.The feasibility of means of constructing finite element model and applying RHT model to the masonry herein and analogous constructions is explored through numerical investigation. 展开更多
关键词 Clay-fired brick Penetration of masonry RHT model Impact high strain rate
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Effect of loading rates on the characteristics of thermal damage for mudstone under different temperatures 被引量:8
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作者 Mao Rongrong Mao Xianbiao +1 位作者 Zhang Lianying Liu Ruixue 《International Journal of Mining Science and Technology》 SCIE EI CSCD 2015年第5期797-801,共5页
The uniaxial compression tests for mudstone specimens are carried out with four different loading rates from room temperature to 400℃ by using the Rock Mechanics Servo-controlled Testing System MTS810 and high temper... The uniaxial compression tests for mudstone specimens are carried out with four different loading rates from room temperature to 400℃ by using the Rock Mechanics Servo-controlled Testing System MTS810 and high temperature furnace MTS652.02.The mechanical properties of mudstone with various loading rates are studied under different temperature conditions.The results show that when temperature increases from room temperature to 400℃ and loading rate is less than 0.03 mm/s,the peak strength of mudstone specimen decreases as loading rate increases,while the various peak strengths show significant differences when loading rate exceeds 0.03 mm/s.At room temperature,the elastic modulus decreases at the first time and then increases with loading rate rising.When the temperature is between200 and 400℃,the elastic modulus presents a decreasing trend with increasing loading rate.With increasing the loading rate,the number of fragments in mudstone becomes larger and even the powder is observed in mudstone with higher loading rate.Under high loading rate,the failure mode of mudstone specimens under different temperatures is mainly conical damage. 展开更多
关键词 MUDSTONE high temperature Loading rate Characteristics of thermal damage
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Effect of Strain Rate on Compression Behavior of Vinyl Ester Resin Casting
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作者 XIONG Tao YANG Bin XIONG Jie XU Xian-jian ZHOU Kai MAO Ming-zhong 《材料工程》 EI CAS CSCD 北大核心 2006年第5期63-67,72,共6页
Quasi-static and high strain rate compressive experiments on vinyl ester casting were carried out by means of MTS (Material Test System) and Hopkinson bar. The behaviors of the compressed unstable and fracture of the ... Quasi-static and high strain rate compressive experiments on vinyl ester casting were carried out by means of MTS (Material Test System) and Hopkinson bar. The behaviors of the compressed unstable and fracture of the resin casting at different strain rates were investigated.The results indicate that the response behavior of the resin casting is controlled by different mechanisms at different strain rate, and some mechanical properties of vinyl ester casting are rate-dependent: the casting are destroyed in toughness model under strain rate 3.3×10 -4~6.6×10 -3/s, while the casting are destroyed in brittleness model under strain rate 950~5800/s. The yield stress, yield strain energy density are all increased with the increasing strain rates at quasi-static as well as at high strain rates. What is interesting is that the yield strain decreased with the strain rates increasing at quasi-static while increased at high strain rates. It is considered that the casting occurred forcing high elastic deformation at high strain rates. The damage of the specimens is mainly controlled by axial stress before unstable deformation, while mainly controlled by shear stress after unstable deformation, and then developed to fracture finally. This progress is rate-dependent: the development of the cracks inside the castings increased with the strain rate increasing. 展开更多
关键词 vinyl ester resin QUASI-STATIC high strain rate strain rate response and crack development
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The Mechanism of Critical Strain of Serrated Yielding in Strain Rate Domain
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作者 符师桦 蔡玉龙 +2 位作者 杨素丽 张青川 伍小平 《Chinese Physics Letters》 SCIE CAS CSCD 2016年第2期79-82,共4页
The mechanism of the critical strain of serrated yielding is studied via tension tests at various strain rates. Betore the critical strain, it is deduced that dislocations are not pinned at high strain rates, and disl... The mechanism of the critical strain of serrated yielding is studied via tension tests at various strain rates. Betore the critical strain, it is deduced that dislocations are not pinned at high strain rates, and dislocations at low strain rates are pinned but cannot escape. The critical strain depends on the first pinning process at high strain rates and on the first unpinning process at low strain rates. The calculated results based on the two criteria are in good consistency with the experiment. 展开更多
关键词 of IS The Mechanism of Critical strain of Serrated Yielding in strain rate Domain that rate high
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Study on Rheological Characteristics of a Grease Used in High Speed Bearing
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作者 Wang Yanshuang Li Shaochuan Guo Dan 《China Petroleum Processing & Petrochemical Technology》 SCIE CAS 2017年第1期55-62,共8页
On a self-made super-high shear strain rate rheometer, the rheological characteristics and apparent viscosity curves of a high-speed bearing grease were obtained under different working conditions. A new grease rheolo... On a self-made super-high shear strain rate rheometer, the rheological characteristics and apparent viscosity curves of a high-speed bearing grease were obtained under different working conditions. A new grease rheological model suited to a shear strain rate range of 0—3.5×10~6s^(-1) was presented. The results showed that the shear stress increased linearly at first and then increased nonlinearly with the increase in shear strain rate up to 1.5×10~6s^(-1), and finally the shear stress decreased slightly with the successive increase in shear strain rate. The shear stress increased with a decreasing rolling speed and an increasing contact pressure. The apparent viscosity decreased rapidly with the increase of shear strain rate at beginning and could approach the viscosity of the base oil if the shear strain rate surpassed 1.5×10~6s^(-1). The fits between the test data and the predicted values by the new model were fairly good. 展开更多
关键词 GREASE rheological characteristic rheological model high speed bearing high shear strain rate
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Study on the Dynamic Behavior of Tungsten Alloy at Strain Rates up to 5 000 s^(-1)
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作者 张宝■ 郑玉六 武海军 《Journal of Beijing Institute of Technology》 EI CAS 2004年第3期270-273,共4页
The dynamic stress-strain curves of 93% tungsten (W) alloy in the forged state at strain rates up to (5 000 s^(-1)) and in the temperature range from 223 K to 473 K were measured with the split Hopkinson pressure bar ... The dynamic stress-strain curves of 93% tungsten (W) alloy in the forged state at strain rates up to (5 000 s^(-1)) and in the temperature range from 223 K to 473 K were measured with the split Hopkinson pressure bar (SHPB) technique. Based on the above experimental data a dynamic constitutive equation considering the effects of strain rate, temperature and the special microstructure of such a kind of W-alloy was proposed. The numerical simulation for the experimental process with this constitutive equation was also carried out, the results show that the constitutive relationship constructed in this paper is very satisfactory for representing the dynamic responsive behavior of material.. 展开更多
关键词 tungsten alloy constitutive relationship high strain rate effect dynamic behavior of material
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Experimental Research on Early-Age Property of High-Performance Concrete Column by Embedded Sensors
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作者 贠英伟 张晓玲 +1 位作者 何朋立 王帅 《Journal of Southwest Jiaotong University(English Edition)》 2008年第3期242-246,共5页
This paper aims at monitoring the autogenous shrinkage (AS) of a high-performance concrete (HPC) column specimen using an embedded strain gauge just after concrete pouring. A real size specimen (40 cm×40 cm&... This paper aims at monitoring the autogenous shrinkage (AS) of a high-performance concrete (HPC) column specimen using an embedded strain gauge just after concrete pouring. A real size specimen (40 cm×40 cm×100cm) was made to simulate the structural members in construction site. The results show that the amount of HPC AS is comparable to that of drying shrinkage and even larger than it, so AS can not be omitted for HPC. By comparing the plain HPC and reinforced HPC specimens, the influences of reinforced bars on autogenous shrinkage and temperature distribution were obtained. 展开更多
关键词 high-performance concrete Autogenous shrinkage Embedded strain gauge temperature distribution
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抽穗开花期高温对杂交稻结实率和产量影响研究
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作者 方文英 陈佳麒 +9 位作者 楚岱蔚 丁梦佳 姚平 金益民 罗天子 沈兴连 莫红华 黄玉英 郑孝孝 朱德峰 《浙江农业科学》 2025年第1期30-34,共5页
针对2022年余杭区出现异常高温,分析该区4个镇街气象站的温度资料,研究高温对单季杂交稻甬优1540、甬优12、春优590、春优161、江两优7901等品种结实率及产量影响。结果表明:2022年日最高温度高于35℃的高温日数为65 d,较常年同期偏多34... 针对2022年余杭区出现异常高温,分析该区4个镇街气象站的温度资料,研究高温对单季杂交稻甬优1540、甬优12、春优590、春优161、江两优7901等品种结实率及产量影响。结果表明:2022年日最高温度高于35℃的高温日数为65 d,较常年同期偏多34 d;40℃以上的高温日数达32 d。在单季杂交稻集中抽穗开花期间的8月10日至8月23日,除1 d为36.7℃外,其余均高于38.0℃。杂交稻因抽穗开花期不同,遇到高温的结实率较常温下降13.9~43.3百分点。抽穗开花期遇到高温,结实率波动较大,且随总粒数变大结实率下降幅度增大。单季杂交稻抽穗开花期遇到38.0~41.0℃的异常高温,较常温结实率下降,导致产量下降28.8%~53.8%。单季杂交稻抽穗开花期遇到异常高温造成产量下降的主要原因为结实率下降。 展开更多
关键词 杂交稻 高温 抽穗开花 结实率 产量
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红曲霉对高温大曲的扰动及制曲工艺探究
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作者 张柱 黄钧 +9 位作者 周荣清 张宿义 秦辉 董异 王超 王小军 雷梓伦 唐秋香 万营东 张毅 《食品与发酵工业》 北大核心 2025年第2期275-284,共10页
以高温大曲为对象,应用多种检测技术探讨了传统(T)与架式(J)工艺及Monascus分离株间扰动对高温大曲理化性质和代谢组分贡献的差异。结果表明,架式工艺提高了发酵力及醇类的丰富度和含量,降低了酯化力,分离株扰动提高了曲的总挥发性和酯... 以高温大曲为对象,应用多种检测技术探讨了传统(T)与架式(J)工艺及Monascus分离株间扰动对高温大曲理化性质和代谢组分贡献的差异。结果表明,架式工艺提高了发酵力及醇类的丰富度和含量,降低了酯化力,分离株扰动提高了曲的总挥发性和酯类成分的含量,改变了组成轮廓。其贡献特点因发酵方式而异,扰动显著提高了传统工艺曲的理化性质和代谢组分的含量,且H26使四甲基吡嗪的含量高达0.38 mg/kg。分离株增大了曲中Saccharopolyspora及Bacillus和Thermoactinomyces等功能菌的丰度。探讨功能菌与理化性质和代谢成分相关性的结果表明,细菌与挥发性成分主要是负相关的,而Kroppenstedtia、Thermoactinomyces等5个属与多种非挥发组分正相关。应用KEGG注释酶的表达解析了代谢途径的特征,架式工艺曲的代谢途径中EC:2.6.1.1的丰度高表达提高了苯乙醇的含量,传统工艺曲则是相关代谢途径中EC:1.4.1.3及EC:1.4.1.4和EC:6.3.4.14的高丰度表达,提高了四甲基吡嗪和酯类组分的含量。由此可见,发酵方式和酱香型大曲内源性分离株的专一性显著影响扰动作用的特点。研究结果为构建目标代谢的生物扰动技术具有重要的借鉴作用。 展开更多
关键词 高温大曲 分离株扰动 代谢组分 传统工艺 架式工艺 相关性 代谢途径
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微泡沫对高温高盐油藏稠油的降黏促进作用
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作者 黄志学 王业飞 +2 位作者 张富民 邵文博 丁名臣 《石油化工》 北大核心 2025年第3期372-378,共7页
针对高温高盐油藏微泡沫稳定性弱的问题,优选出一种以聚丙烯酰胺类聚合物SAV10为稳泡剂、表面活性剂芥酸酰胺丙基甜菜碱和十二烷基二甲基甜菜碱为发泡剂的耐高温高盐的发泡体系,该发泡体系在6800 r/min的转速下搅拌1 min可形成微泡沫,... 针对高温高盐油藏微泡沫稳定性弱的问题,优选出一种以聚丙烯酰胺类聚合物SAV10为稳泡剂、表面活性剂芥酸酰胺丙基甜菜碱和十二烷基二甲基甜菜碱为发泡剂的耐高温高盐的发泡体系,该发泡体系在6800 r/min的转速下搅拌1 min可形成微泡沫,对比了发泡体系和微泡沫的稠油乳化降黏效果和水包油乳液的稳定性。实验结果表明,微泡沫的乳化降黏效果优于发泡体系。优选出的发泡体系的发泡率可达420%;在90℃下发泡体系老化60 d的黏度保持率大于88%;所制备的微泡沫的析液半衰期为1161 s,表现出良好的稳定性。采用矿化度为218.1 g/L的矿化水制备泡沫体系和微泡沫时,在90℃、稠油和矿化水的质量比为30∶70,50∶50,70∶30时,发泡体系和微泡沫均可乳化稠油,发泡体系的降黏率大于89%,析水率大于80%;微泡沫的降黏率大于95%,析水率虽偏低,但仍大于60%。 展开更多
关键词 微泡沫 降黏率 析水率 高温高盐油藏 发泡率 析液半衰期
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(W+TiB+TiC)/TA15复合材料的动态力学性能及绝热剪切行为
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作者 孙守伟 马逸飞 任宇 《兵器装备工程学报》 北大核心 2025年第2期244-250,共7页
钛基复合材料(TMC)在涉及冲击载荷服役条件的武器装备领域具有广阔的应用前景。为揭示新型“难熔金属+陶瓷”杂化增强TMC的高应变率加载响应特性及失效行为,通过原位合成反应成功制备了(W+TiB+TiC)/TA15杂化增强TMC,并利用材料万能试验... 钛基复合材料(TMC)在涉及冲击载荷服役条件的武器装备领域具有广阔的应用前景。为揭示新型“难熔金属+陶瓷”杂化增强TMC的高应变率加载响应特性及失效行为,通过原位合成反应成功制备了(W+TiB+TiC)/TA15杂化增强TMC,并利用材料万能试验机和分离式Hopkinson压杆测试了该TMC在0.001~4 000/s应变率范围内的室温压缩力学性能,同时对高应变率加载后TMC的微观组织进行了系统表征。结果表明:准静态及动态压缩时,杂化增强TMC的强度和塑性均高于作为基体的均质TA15合金;4 000/s应变率时,TMC的平均流变应力、均匀塑性应变和冲击吸收能分别达到1632 MPa、27%和449 J/cm^(3),较均质TA15合金分别提高了9.8%、8.0%和20.7%;杂化增强相团簇的存在显著影响TMC中绝热剪切带(ABS)的扩展和交互作用行为,导致ASB更容易发生偏转、分叉和汇聚,有效耗散了高应变率加载过程中的冲击能量,使TMC表现出了更优异的动态力学性能。 展开更多
关键词 钛基复合材料 杂化增强相 原位合成 力学行为 高应变率 绝热剪切带
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