In the field of deep space exploration,the rapid development of terahertz spectrometer has put forward higher requirements to the back-end chirp transform spectrometer(CTS)system.In order to simultaneously meet the me...In the field of deep space exploration,the rapid development of terahertz spectrometer has put forward higher requirements to the back-end chirp transform spectrometer(CTS)system.In order to simultaneously meet the measurement requirements of wide bandwidth and high accuracy spectral lines,we built a CTS system with an analysis bandwidth of 1 GHz and a frequency resolution of 100 kHz around the surface acoustic wave(SAW)chirp filter with a bandwidth of 1 GHz.In this paper,the relationship between the CTS nonlinear phase error shift model and the basic measurement parameters is studied,and the effect of CTS phase mismatch on the pulse compression waveform is analyzed by simulation.And the expander error optimization method is proposed for the problem that the large nonlinear error of the expander leads to the unbalanced response of the CTS system and the serious distortion of the compressed pulse waveform under large bandwidth.It is verified through simulation and experiment that the method is effective for reducing the root mean square error(RMSE)of the phase of the expander from 18.75°to 6.65°,reducing the in-band standard deviation of the CTS frequency resolution index from 8.43 kHz to 4.72 kHz,solving the problem of serious distortion of the compressed pulse waveform,and improving the uneven CTS response under large bandwidth.展开更多
Suspension roasting followed by magnetic separation is a promising method to upgrade oolitic hematite ore.An oolitic hematite ore was roasted using suspension roasting technology at different temperatures.The phase tr...Suspension roasting followed by magnetic separation is a promising method to upgrade oolitic hematite ore.An oolitic hematite ore was roasted using suspension roasting technology at different temperatures.The phase transformation for iron minerals was investigated by XRD and Mossbauer spectrum,and the characteristics of roasted product were analyzed by VSM and SEM-EDS.Results indicate that the magnetic concentrate is of 58.73% Fe with iron recovery of 83.96% at 650 °C.The hematite is rapidly transformed into magnetite during the roasting with transformation ratio of 92.75% at 650 °C.Roasting temperature has a significant influence on the phase transformation of hematite to magnetite.The transformation ratio increases with increased temperature.After roasting,the magnetic susceptibility is significantly improved,while iron ore microstructure is not altered significantly.展开更多
Siderite,as an abundant iron ore,has not been effectively utilized,with a low utilization rate.In this study,the in-situ kinetics and mechanism of siderite during suspension magnetization roasting(SMR)were investigate...Siderite,as an abundant iron ore,has not been effectively utilized,with a low utilization rate.In this study,the in-situ kinetics and mechanism of siderite during suspension magnetization roasting(SMR)were investigated to improve the selective conversion of siderite to magnetite and CO,enriching the theoretical system of green SMR using siderite as a reductant.According to the gas products analyses,the peak value of the reaction rate increased with increasing temperature,and its curves presented the feature of an early peak and long tail.The mechanism function of the siderite pyrolysis was the contraction sphere model(R_(3)):f(α)=3(1−α)2/3;E_(α)was 46.4653 kJ/mol;A was 0.5938 s^(−1);the kinetics equation was k=0.5938exp[−46.4653/(RT)].The in-situ HT-XRD results indicated that siderite was converted into magnetite and wüstite that exhibited a good crystallinity in SMR under a N_(2) atmosphere.At 620℃,the saturation magnetization(M_(s)),remanence magnetization(Mr),and coercivity(Hc)of the product peaked at 53.63×10^(-3)A·m^(2)/g,10.23×10^(-3)A·m^(2)/g,and 12.40×10^(3)A/m,respectively.Meanwhile,the initial particles with a smooth surface were transformed into particles with a porous and loose structure in the roasting process,which would contribute to reducing the grinding cost.展开更多
The effect of a high magnetic field up to 30T on phase transformation temperature and microstructure of Fe-based alloys has been reviewed. A high magnetic field accelerates ferrite transformation, changes the morpho...The effect of a high magnetic field up to 30T on phase transformation temperature and microstructure of Fe-based alloys has been reviewed. A high magnetic field accelerates ferrite transformation, changes the morphology of the transformed microstructures and increases the A3 and A1 temperature. In a magnetic field of 30T, the A1 temperature increases by about 37.1℃ for Fe-0.8C, the A3 temperature for pure Fe increases by about 33.1℃. The measured transformation temperature data are not consistent with calculation results using Weiss molecular field theory. Ferrite grains are elongated and aligned along the direction of magnetic field in Fe-0.4C and Fe-0.6C alloys by ferrite transformation, but elongated and aligned structure was not found in pure Fe, Fe-0.05C alloy and Fe-1.5Mn-0.11C-0.1V alloy.展开更多
The effects of tensile temperatures ranging from 100 K to 900 K on the phase transition of hexagonal close-packed(HCP)zirconium were investigated by molecular dynamics simulations,which were combined with experimental...The effects of tensile temperatures ranging from 100 K to 900 K on the phase transition of hexagonal close-packed(HCP)zirconium were investigated by molecular dynamics simulations,which were combined with experimental observation under high resolution transmission electron microscopy.The results show that externally applied loading first induced the HCP to body-centered cubic(BCC)phase transition in the Pitsch-Schrader(PS)orientation relationship(OR).Then,the face-centered cubic(FCC)structure transformed from the BCC phase in the Bain path.However,the HCP-to-BCC transition was incomplete at 100 K and 300 K,resulting in a prismatic-type OR between the FCC and original HCP phase.Additionally,at the temperature ranging from 100 K to 600 K,the inverse BCC-to-HCP transition occurred locally following other variants of the PS OR,resulting in a basal-type relation between the newly generated HCP and FCC phases.A higher tensile temperature promoted the amount of FCC phase transforming into the BCC phase when the strain exceeded 45%.Besides,the crystal stretched at lower temperatures exhibits relatively higher strength but by the compromise of plasticity.This study reveals the deformation mechanisms in HCP-Zr at different temperatures,which may provide a better understanding of the deformation mechanism of zirconium alloys under different application environments.展开更多
A new process of WC-Co cemented carbide was developed by using nano-grained W（Co, C） composite powders as raw materials processed by high-energy ball milling. X-ray diffraetion（XRD）, differential thermal analysis ...A new process of WC-Co cemented carbide was developed by using nano-grained W（Co, C） composite powders as raw materials processed by high-energy ball milling. X-ray diffraetion（XRD）, differential thermal analysis （DTA）, thermo-gravimetrie （TG） analysis and coercive forces of the sintered samples were adopted to analyze the phase transformation and constitution, and the microstructures of sintered samples were characterized by scanning electron microscopy（SEM）. The results show that the as-milled powders are transformed into transitional phases W2C and η （Co3W3C or Co6W6C） during sintering, and finally transformed into WC and Co phases completely at 1 250℃ for 30 min, and a large number of fibrous WC grains with about 1.2μm in length and 100 nm in radial dimension are formed in the sintered body at 1 300 ℃.展开更多
The structure of a steel changes with temperature due to phase transformations. This phase change is generally companied by a variation in the specific volume which is exhibited as a departure from the behaviour of th...The structure of a steel changes with temperature due to phase transformations. This phase change is generally companied by a variation in the specific volume which is exhibited as a departure from the behaviour of the thermal expansion or contraction, at the temperature at which the change occurs. This behaviour can be detected as a change in the dimensions of a suitable test piece, and forms the operating principle of dilatometry. The dilatometric technique may be applicable to the investigation of the phase transformation kinetics if the relation between the fractions of phases, the temperature, the compositions of phases and the dilatation can be built up. Efforts have been made to analyze the dilatation during an isothermal transformation or to calculate the dilatation during the heating of plain carbon steels using the thermodynamic function. The existing models are, however, not directly applicable to the determination of the phase transformation kinetics from a dilatation curve. A detailed analysis has been made of the length change of a hypoeutectoid steel during a continuous cooling. A model has been developed in which the transient dilatation is calculated based on the fraction of the phases present. The model takes into account the redistribution of carbon and is applicable to the determination of the phase transformation kinetics from the dilatation data during a cooling of a hypo-eutectoid steel. The model was validated by comparing the model results with the experimental results of an interstitial free steel. Experiments have been done with an interstitial-free steel and a C-Mn steel. The model has been applied to the calculation of the transformation kinetics indicated by the dilatation curves. Excellent agreements between the model and the experiments have been obtained.展开更多
Boehmite was prepared under heat treatment in water vapour, and the phase transformation of gibbsite heat-treated at various temperatures was investigated. The sample was characterized by scanning electron microscopy(...Boehmite was prepared under heat treatment in water vapour, and the phase transformation of gibbsite heat-treated at various temperatures was investigated. The sample was characterized by scanning electron microscopy(SEM), X-ray diffraction (XRD), thermogravimetry and differential thermalanalysis (TG-DTA), fourier transform infrared (FTIR),and BET surface area.Effect of temperature on preparation was studied in the range of 155°–195°.With the increase in temperature, transformation of gibbsite into crystalline boehmites took place as indicated by the X-ray diffraction (XRD). The shape of the grains in the prepared sample was cube-like morphology.In water vapour gibbsite transform into boehmite by a dissolution - precipitation mechanism.展开更多
The room temperature phase diagram of Al-Zn-Cu system is the important basis for judging the phase constituents of the materials at the usage condition. New results about the room temperature phase diagram of the low ...The room temperature phase diagram of Al-Zn-Cu system is the important basis for judging the phase constituents of the materials at the usage condition. New results about the room temperature phase diagram of the low copper side in the Al-Zn-Cu systems have been shown in this study. Miscibility gap of fcc phase in the Al-Zn-Cu system has also been studied by experimental diffusion-couple method and thermodynamic calculation. Properties of this miscibility gap have been known. It is practically significant for the study on the aging behavior and for the control of the microstructure and properties of the Al alloys with Zn and Cu element.展开更多
In the present study,molecular dynamic simulation(MD)was used to investigate the plastic deformation process of the Fe-Mn alloys with different Mn contents.The influences of Mn contents ranging from 10%to 30%(at%)on t...In the present study,molecular dynamic simulation(MD)was used to investigate the plastic deformation process of the Fe-Mn alloys with different Mn contents.The influences of Mn contents ranging from 10%to 30%(at%)on the deformation behavior and the controlling mechanism of the Fe-base alloys were analyzed.The results show that phase transformations and{112}<111>_(BCC)deformation twinning occur in all Fe-Mn alloys but follow different deformation paths.In the Fe-10%Mn alloy the deformation twinning mechanism obeys the FCC-related path,the Fe-20%Mn alloy involves both the FCC-and HCP-related paths,and the deformation of the Fe-30%Mn alloy is dominated by the HCP-related twinning path.The addition of Mn can increase the stacking fault energy and retard the activation of slip systems as well as the formation of stacking faults.Thus,a higher content of Mn can delay the FCC®ε-martensite and the subsequentε-martensite®BCC phase transition at the intersection of twoε-martensitic bands.Therefore,the addition of Mn alloying element increases the yield strength and reduces the elastic modulus of the Fe-Mn alloys.The formation of deformation twins will contribute to the work-hardening effect and delay the necking and fracture of alloys.It is expected that the results in the present study will provide theoretical reference for the design and optimization of high-performance steels.展开更多
In-situ observations on α/γ phase transformation were made to study the effects of grain boundary microstructures on the formation of a new phase and the migration of α/γ interphase boundary in an iron4. 2%Cr allo...In-situ observations on α/γ phase transformation were made to study the effects of grain boundary microstructures on the formation of a new phase and the migration of α/γ interphase boundary in an iron4. 2%Cr alloy. It was found that triple junctions with more random boundaries could be the primary nucleation sites for a new phase, while triple junctions with low angle or low ∑ coincidence boundaries did not play any role as preferential sites. The migration of α/γ interphase boundary during heating over the transformation temperature range showed the two stage behaviour characterized by a stage with a migration velocity of 0. 33-0. 75 mm/s and secondly by a stage with 3. 7-7. 6 mm/s. It was also found that abnormal grain growth and a high density of ∑3 coincidence boundaries could occur in a phase with bcc structure after cycling of α/γ phase transformation. A new mechanism of nucleation and growth of a new phase in α/γ phase transformation is proposed on the basis of roles of plane-matching interphase boundaries, as previously discussed on the origin of anisotropy of grain growth due to the migration of {110} plane-matching boundaries in Fe-3z%Si alloy. The most recent theoretical work on the distribution of plane-matching boundaries in solids with different crystal structures was found to be useful for the understanding of nucleation and growth during α/γ phase transformation.展开更多
The identification features of composite pseudocode phase modulation and carry frequency modulation signal include pseudocode and modulation frequency. In this paper,PWD is used to extract these features. First,the fe...The identification features of composite pseudocode phase modulation and carry frequency modulation signal include pseudocode and modulation frequency. In this paper,PWD is used to extract these features. First,the feature of pseudocode is extracted using the amplitude output of PWD and the correlation filter technology. Then the feature of frequency modulation is extracted by way of PWD analysis on the signal processed by anti-phase operation according to the extracted feature of pseudo code,i.e. position information of changed abruptly point of phase. The simulation result shows that both the features of frequency modulation and phase change position caused by the pseudocode phase modulation can be extracted effectively for SNR=3 dB.展开更多
This paper proposes a modified centralized shifted Rayleigh filter（MCSRF） algorithm for tracking boost phase of ballistic missile（BM） trajectory with a highly nonlinear dynamical model based on bearings-only.This ...This paper proposes a modified centralized shifted Rayleigh filter（MCSRF） algorithm for tracking boost phase of ballistic missile（BM） trajectory with a highly nonlinear dynamical model based on bearings-only.This paper contributes three folds.Firstly,the mathematical model of an MCSRF for multiple passive sensors is derived.Then,minimum entropy based onedimensional optimization search to adaptively adjust the probability of the different filters for real time state estimation is deployed.Finally,the unscented transform（UT） is introduced to resolve the asymmetric state estimation problem.Simulation results show that the proposed algorithm can consecutively track the BM precisely during the boost phase.In comparison with the unscented Kalman filter（UKF） algorithm,the proposed algorithm effectively reduces the tracking position and velocity root mean square（RMS） errors,which will make more sense for early precision interception.展开更多
The main methods of the second phase quantitative analysis in current material science researches are manual recognition and extracting by using software such as Image Tool and Nano Measurer. The weaknesses such as hi...The main methods of the second phase quantitative analysis in current material science researches are manual recognition and extracting by using software such as Image Tool and Nano Measurer. The weaknesses such as high labor intensity and low accuracy statistic results exist in these methods. In order to overcome the shortcomings of the current methods, the Ω phase in A1-Cu-Mg-Ag alloy is taken as the research object and an algorithm based on the digital image processing and pattern recognition is proposed and implemented to do the A1 alloy TEM （transmission electron microscope） digital images process and recognize and extract the information of the second phase in the result image automatically. The top-hat transformation of the mathematical morphology, as well as several imaging processing technologies has been used in the proposed algorithm. Thereinto, top-hat transformation is used for elimination of asymmetric illumination and doing Multi-layer filtering to segment Ω phase in the TEM image. The testing results are satisfied, which indicate that the Ω phase with unclear boundary or small size can be recognized by using this method. The omission of these two kinds of Ω phase can be avoided or significantly reduced. More Ω phases would be recognized （growing rate minimum to 2% and maximum to 400% in samples）, accuracy of recognition and statistics results would be greatly improved by using this method. And the manual error can be eliminated. The procedure recognizing and making quantitative analysis of information in this method is automatically completed by the software. It can process one image, including recognition and quantitative analysis in 30 min, but the manual method such as using Image Tool or Nano Measurer need 2 h or more. The labor intensity is effectively reduced and the working efficiency is greatly improved.展开更多
Code acquisition is the kernel operation for signal synchronization in the spread-spectrum receiver.To reduce the computational complexity and latency of code acquisition,this paper proposes an efficient scheme employ...Code acquisition is the kernel operation for signal synchronization in the spread-spectrum receiver.To reduce the computational complexity and latency of code acquisition,this paper proposes an efficient scheme employing sparse Fourier transform(SFT)and the relevant hardware architecture for field programmable gate array(FPGA)and application-specific integrated circuit(ASIC)implementation.Efforts are made at both the algorithmic level and the implementation level to enable merged searching of code phase and Doppler frequency without incurring massive hardware expenditure.Compared with the existing code acquisition approaches,it is shown from theoretical analysis and experimental results that the proposed design can shorten processing latency and reduce hardware complexity without degrading the acquisition probability.展开更多
文摘In the field of deep space exploration,the rapid development of terahertz spectrometer has put forward higher requirements to the back-end chirp transform spectrometer(CTS)system.In order to simultaneously meet the measurement requirements of wide bandwidth and high accuracy spectral lines,we built a CTS system with an analysis bandwidth of 1 GHz and a frequency resolution of 100 kHz around the surface acoustic wave(SAW)chirp filter with a bandwidth of 1 GHz.In this paper,the relationship between the CTS nonlinear phase error shift model and the basic measurement parameters is studied,and the effect of CTS phase mismatch on the pulse compression waveform is analyzed by simulation.And the expander error optimization method is proposed for the problem that the large nonlinear error of the expander leads to the unbalanced response of the CTS system and the serious distortion of the compressed pulse waveform under large bandwidth.It is verified through simulation and experiment that the method is effective for reducing the root mean square error(RMSE)of the phase of the expander from 18.75°to 6.65°,reducing the in-band standard deviation of the CTS frequency resolution index from 8.43 kHz to 4.72 kHz,solving the problem of serious distortion of the compressed pulse waveform,and improving the uneven CTS response under large bandwidth.
基金Project([2011]01-69-07)supported by the China Geological Survey Project
文摘Suspension roasting followed by magnetic separation is a promising method to upgrade oolitic hematite ore.An oolitic hematite ore was roasted using suspension roasting technology at different temperatures.The phase transformation for iron minerals was investigated by XRD and Mossbauer spectrum,and the characteristics of roasted product were analyzed by VSM and SEM-EDS.Results indicate that the magnetic concentrate is of 58.73% Fe with iron recovery of 83.96% at 650 °C.The hematite is rapidly transformed into magnetite during the roasting with transformation ratio of 92.75% at 650 °C.Roasting temperature has a significant influence on the phase transformation of hematite to magnetite.The transformation ratio increases with increased temperature.After roasting,the magnetic susceptibility is significantly improved,while iron ore microstructure is not altered significantly.
基金Projects(51874071,52022019,51734005)supported by the National Natural Science Foundation of ChinaProject(161045)supported by the Fok Ying Tung Education Foundation for Yong Teachers in the Higher Education Institutions of China。
文摘Siderite,as an abundant iron ore,has not been effectively utilized,with a low utilization rate.In this study,the in-situ kinetics and mechanism of siderite during suspension magnetization roasting(SMR)were investigated to improve the selective conversion of siderite to magnetite and CO,enriching the theoretical system of green SMR using siderite as a reductant.According to the gas products analyses,the peak value of the reaction rate increased with increasing temperature,and its curves presented the feature of an early peak and long tail.The mechanism function of the siderite pyrolysis was the contraction sphere model(R_(3)):f(α)=3(1−α)2/3;E_(α)was 46.4653 kJ/mol;A was 0.5938 s^(−1);the kinetics equation was k=0.5938exp[−46.4653/(RT)].The in-situ HT-XRD results indicated that siderite was converted into magnetite and wüstite that exhibited a good crystallinity in SMR under a N_(2) atmosphere.At 620℃,the saturation magnetization(M_(s)),remanence magnetization(Mr),and coercivity(Hc)of the product peaked at 53.63×10^(-3)A·m^(2)/g,10.23×10^(-3)A·m^(2)/g,and 12.40×10^(3)A/m,respectively.Meanwhile,the initial particles with a smooth surface were transformed into particles with a porous and loose structure in the roasting process,which would contribute to reducing the grinding cost.
文摘The effect of a high magnetic field up to 30T on phase transformation temperature and microstructure of Fe-based alloys has been reviewed. A high magnetic field accelerates ferrite transformation, changes the morphology of the transformed microstructures and increases the A3 and A1 temperature. In a magnetic field of 30T, the A1 temperature increases by about 37.1℃ for Fe-0.8C, the A3 temperature for pure Fe increases by about 33.1℃. The measured transformation temperature data are not consistent with calculation results using Weiss molecular field theory. Ferrite grains are elongated and aligned along the direction of magnetic field in Fe-0.4C and Fe-0.6C alloys by ferrite transformation, but elongated and aligned structure was not found in pure Fe, Fe-0.05C alloy and Fe-1.5Mn-0.11C-0.1V alloy.
基金Projects(51901248,51828102)supported by the National Natural Science Foundation of ChinaProject(2018JJ3649)supported by the Natural Science Foundation of Hunan Province,ChinaProject(2019CX026)supported by the Innovation-driven Plan in Central South University,China。
文摘The effects of tensile temperatures ranging from 100 K to 900 K on the phase transition of hexagonal close-packed(HCP)zirconium were investigated by molecular dynamics simulations,which were combined with experimental observation under high resolution transmission electron microscopy.The results show that externally applied loading first induced the HCP to body-centered cubic(BCC)phase transition in the Pitsch-Schrader(PS)orientation relationship(OR).Then,the face-centered cubic(FCC)structure transformed from the BCC phase in the Bain path.However,the HCP-to-BCC transition was incomplete at 100 K and 300 K,resulting in a prismatic-type OR between the FCC and original HCP phase.Additionally,at the temperature ranging from 100 K to 600 K,the inverse BCC-to-HCP transition occurred locally following other variants of the PS OR,resulting in a basal-type relation between the newly generated HCP and FCC phases.A higher tensile temperature promoted the amount of FCC phase transforming into the BCC phase when the strain exceeded 45%.Besides,the crystal stretched at lower temperatures exhibits relatively higher strength but by the compromise of plasticity.This study reveals the deformation mechanisms in HCP-Zr at different temperatures,which may provide a better understanding of the deformation mechanism of zirconium alloys under different application environments.
基金Project (50474049) supported by the National Natural Science Foundation of China
文摘A new process of WC-Co cemented carbide was developed by using nano-grained W（Co, C） composite powders as raw materials processed by high-energy ball milling. X-ray diffraetion（XRD）, differential thermal analysis （DTA）, thermo-gravimetrie （TG） analysis and coercive forces of the sintered samples were adopted to analyze the phase transformation and constitution, and the microstructures of sintered samples were characterized by scanning electron microscopy（SEM）. The results show that the as-milled powders are transformed into transitional phases W2C and η （Co3W3C or Co6W6C） during sintering, and finally transformed into WC and Co phases completely at 1 250℃ for 30 min, and a large number of fibrous WC grains with about 1.2μm in length and 100 nm in radial dimension are formed in the sintered body at 1 300 ℃.
文摘The structure of a steel changes with temperature due to phase transformations. This phase change is generally companied by a variation in the specific volume which is exhibited as a departure from the behaviour of the thermal expansion or contraction, at the temperature at which the change occurs. This behaviour can be detected as a change in the dimensions of a suitable test piece, and forms the operating principle of dilatometry. The dilatometric technique may be applicable to the investigation of the phase transformation kinetics if the relation between the fractions of phases, the temperature, the compositions of phases and the dilatation can be built up. Efforts have been made to analyze the dilatation during an isothermal transformation or to calculate the dilatation during the heating of plain carbon steels using the thermodynamic function. The existing models are, however, not directly applicable to the determination of the phase transformation kinetics from a dilatation curve. A detailed analysis has been made of the length change of a hypoeutectoid steel during a continuous cooling. A model has been developed in which the transient dilatation is calculated based on the fraction of the phases present. The model takes into account the redistribution of carbon and is applicable to the determination of the phase transformation kinetics from the dilatation data during a cooling of a hypo-eutectoid steel. The model was validated by comparing the model results with the experimental results of an interstitial free steel. Experiments have been done with an interstitial-free steel and a C-Mn steel. The model has been applied to the calculation of the transformation kinetics indicated by the dilatation curves. Excellent agreements between the model and the experiments have been obtained.
文摘Boehmite was prepared under heat treatment in water vapour, and the phase transformation of gibbsite heat-treated at various temperatures was investigated. The sample was characterized by scanning electron microscopy(SEM), X-ray diffraction (XRD), thermogravimetry and differential thermalanalysis (TG-DTA), fourier transform infrared (FTIR),and BET surface area.Effect of temperature on preparation was studied in the range of 155°–195°.With the increase in temperature, transformation of gibbsite into crystalline boehmites took place as indicated by the X-ray diffraction (XRD). The shape of the grains in the prepared sample was cube-like morphology.In water vapour gibbsite transform into boehmite by a dissolution - precipitation mechanism.
文摘The room temperature phase diagram of Al-Zn-Cu system is the important basis for judging the phase constituents of the materials at the usage condition. New results about the room temperature phase diagram of the low copper side in the Al-Zn-Cu systems have been shown in this study. Miscibility gap of fcc phase in the Al-Zn-Cu system has also been studied by experimental diffusion-couple method and thermodynamic calculation. Properties of this miscibility gap have been known. It is practically significant for the study on the aging behavior and for the control of the microstructure and properties of the Al alloys with Zn and Cu element.
基金Project(51901248)supported by the National Natural Science Foundation of ChinaProject(2023JJ40742)supported by the Natural Science Foundation of Hunan Province,China。
文摘In the present study,molecular dynamic simulation(MD)was used to investigate the plastic deformation process of the Fe-Mn alloys with different Mn contents.The influences of Mn contents ranging from 10%to 30%(at%)on the deformation behavior and the controlling mechanism of the Fe-base alloys were analyzed.The results show that phase transformations and{112}<111>_(BCC)deformation twinning occur in all Fe-Mn alloys but follow different deformation paths.In the Fe-10%Mn alloy the deformation twinning mechanism obeys the FCC-related path,the Fe-20%Mn alloy involves both the FCC-and HCP-related paths,and the deformation of the Fe-30%Mn alloy is dominated by the HCP-related twinning path.The addition of Mn can increase the stacking fault energy and retard the activation of slip systems as well as the formation of stacking faults.Thus,a higher content of Mn can delay the FCC®ε-martensite and the subsequentε-martensite®BCC phase transition at the intersection of twoε-martensitic bands.Therefore,the addition of Mn alloying element increases the yield strength and reduces the elastic modulus of the Fe-Mn alloys.The formation of deformation twins will contribute to the work-hardening effect and delay the necking and fracture of alloys.It is expected that the results in the present study will provide theoretical reference for the design and optimization of high-performance steels.
文摘In-situ observations on α/γ phase transformation were made to study the effects of grain boundary microstructures on the formation of a new phase and the migration of α/γ interphase boundary in an iron4. 2%Cr alloy. It was found that triple junctions with more random boundaries could be the primary nucleation sites for a new phase, while triple junctions with low angle or low ∑ coincidence boundaries did not play any role as preferential sites. The migration of α/γ interphase boundary during heating over the transformation temperature range showed the two stage behaviour characterized by a stage with a migration velocity of 0. 33-0. 75 mm/s and secondly by a stage with 3. 7-7. 6 mm/s. It was also found that abnormal grain growth and a high density of ∑3 coincidence boundaries could occur in a phase with bcc structure after cycling of α/γ phase transformation. A new mechanism of nucleation and growth of a new phase in α/γ phase transformation is proposed on the basis of roles of plane-matching interphase boundaries, as previously discussed on the origin of anisotropy of grain growth due to the migration of {110} plane-matching boundaries in Fe-3z%Si alloy. The most recent theoretical work on the distribution of plane-matching boundaries in solids with different crystal structures was found to be useful for the understanding of nucleation and growth during α/γ phase transformation.
文摘The identification features of composite pseudocode phase modulation and carry frequency modulation signal include pseudocode and modulation frequency. In this paper,PWD is used to extract these features. First,the feature of pseudocode is extracted using the amplitude output of PWD and the correlation filter technology. Then the feature of frequency modulation is extracted by way of PWD analysis on the signal processed by anti-phase operation according to the extracted feature of pseudo code,i.e. position information of changed abruptly point of phase. The simulation result shows that both the features of frequency modulation and phase change position caused by the pseudocode phase modulation can be extracted effectively for SNR=3 dB.
基金supported by the Aerospace Science and Technology Innovation Foundation (CASC0202-3)
文摘This paper proposes a modified centralized shifted Rayleigh filter（MCSRF） algorithm for tracking boost phase of ballistic missile（BM） trajectory with a highly nonlinear dynamical model based on bearings-only.This paper contributes three folds.Firstly,the mathematical model of an MCSRF for multiple passive sensors is derived.Then,minimum entropy based onedimensional optimization search to adaptively adjust the probability of the different filters for real time state estimation is deployed.Finally,the unscented transform（UT） is introduced to resolve the asymmetric state estimation problem.Simulation results show that the proposed algorithm can consecutively track the BM precisely during the boost phase.In comparison with the unscented Kalman filter（UKF） algorithm,the proposed algorithm effectively reduces the tracking position and velocity root mean square（RMS） errors,which will make more sense for early precision interception.
基金Project(51171209)supported by the National Natural Science Foundation of China
文摘The main methods of the second phase quantitative analysis in current material science researches are manual recognition and extracting by using software such as Image Tool and Nano Measurer. The weaknesses such as high labor intensity and low accuracy statistic results exist in these methods. In order to overcome the shortcomings of the current methods, the Ω phase in A1-Cu-Mg-Ag alloy is taken as the research object and an algorithm based on the digital image processing and pattern recognition is proposed and implemented to do the A1 alloy TEM （transmission electron microscope） digital images process and recognize and extract the information of the second phase in the result image automatically. The top-hat transformation of the mathematical morphology, as well as several imaging processing technologies has been used in the proposed algorithm. Thereinto, top-hat transformation is used for elimination of asymmetric illumination and doing Multi-layer filtering to segment Ω phase in the TEM image. The testing results are satisfied, which indicate that the Ω phase with unclear boundary or small size can be recognized by using this method. The omission of these two kinds of Ω phase can be avoided or significantly reduced. More Ω phases would be recognized （growing rate minimum to 2% and maximum to 400% in samples）, accuracy of recognition and statistics results would be greatly improved by using this method. And the manual error can be eliminated. The procedure recognizing and making quantitative analysis of information in this method is automatically completed by the software. It can process one image, including recognition and quantitative analysis in 30 min, but the manual method such as using Image Tool or Nano Measurer need 2 h or more. The labor intensity is effectively reduced and the working efficiency is greatly improved.
基金supported by the National Natural Science Foundation of China(61801503).
文摘Code acquisition is the kernel operation for signal synchronization in the spread-spectrum receiver.To reduce the computational complexity and latency of code acquisition,this paper proposes an efficient scheme employing sparse Fourier transform(SFT)and the relevant hardware architecture for field programmable gate array(FPGA)and application-specific integrated circuit(ASIC)implementation.Efforts are made at both the algorithmic level and the implementation level to enable merged searching of code phase and Doppler frequency without incurring massive hardware expenditure.Compared with the existing code acquisition approaches,it is shown from theoretical analysis and experimental results that the proposed design can shorten processing latency and reduce hardware complexity without degrading the acquisition probability.
