In our study we investigated a refractory copper-nickel sulfide ore separation by using a cyclonic-static micro-bubble flotation column (FCSMC). The process mineralogy of the main products was studied. Using a scannin...In our study we investigated a refractory copper-nickel sulfide ore separation by using a cyclonic-static micro-bubble flotation column (FCSMC). The process mineralogy of the main products was studied. Using a scanning electron microscope-energy dispersive system (SEM-EDS) and an X-ray spectrometer the mineral category and content of samples were analyzed. By using a mineral liberation analyzer (MLA) the mineral liberation characteristics were revealed. It is shown that in roughing feed the monomers liberation degree of nickel pyrite and chalcopyrite take up 84.11% and 88.82%, respectively. In tailings, the lost nickel pyrite and chalcopyrite are mainly monomers. Therefore, strengthening the micro-fine particle recovery capacity is the key to increase recovery.展开更多
The Cyclonic-Static Microbubble Flotation Column (FCSMC) is currently a widely used, novel type of flotation device. The self-absorbing microbubble generator is the core component of this device. The structure of the ...The Cyclonic-Static Microbubble Flotation Column (FCSMC) is currently a widely used, novel type of flotation device. The self-absorbing microbubble generator is the core component of this device. The structure of the microbubble generator directly influences flotation column performance by affecting bubble size and distribution as well as gas holdup in the column. However, the complicated flow inside the generator results in high R&D costs and difficulty in testing. Thus, the CFD software, FLUENT, was used to simulate the gas-liquid two-phase flow inside a self-absorbing microbubble generator. The effect of area ratio, a key structural parameter, was studied in detail. Critical flow-field parameters including velocity, turbulent kinetic energy, minimum static pressure and gas holdup were obtained. The simulation results demonstrate that the optimum area ratio is 3.展开更多
A packing-flotation column was proposed to optimize the flotation environment A research system was es- tablished using a 100 mm diameter cyclonic micro-bubble flotation column to study fluid properties. Dry-plate and...A packing-flotation column was proposed to optimize the flotation environment A research system was es- tablished using a 100 mm diameter cyclonic micro-bubble flotation column to study fluid properties. Dry-plate and wet- plate pressure drops were studied and the corresponding pressure drop equations developed. The results show that the dry-plate pressure drop of the packing cyclonic micro-bubble flotation column is 10–15 times less than that of the chemical tower, which is principally shown in its relatively small resistance coefficient, ξ ≈0.0207. The wet-plate pressure drop is 2–3 times higher than that of the chemical tower, which is largely caused by the separation materials and characteristics of the equipment. With flotation, the greater the pressure drop, the better the flotation environment.展开更多
Laboratory experiments have been conducted to study the flow field in a cyclone static micro-bubble flotation column. The method of Particle Image Velocimetry (PIV) was used. The flow field velocity distribution in bo...Laboratory experiments have been conducted to study the flow field in a cyclone static micro-bubble flotation column. The method of Particle Image Velocimetry (PIV) was used. The flow field velocity distribution in both cross section and longitudinal section within cyclonic zone was studied for different circulating volumes. The cross sectional vortex was also analyzed. The results show that in cross section as the circulating volume increases from 0.187 to 0.350 m 3 /h, the flow velocity ranges from 0 to 0.68 m/s. The flow field is mainly a non-vortex potential flow that forms a free vortex without outside energy input. In the cyclonic region the vortex deviates from the center of the flotation column because a single tangential opening introduces circulating fluid into the column. The tangential component of the velocity plays a defining role in the cross section. In the longitudinal section the velocity ranges from 0 to 0.08 m/s. The flow velocity increases as does the circulating volume. Advantageous mineral separation conditions arise from the combined effects of cyclonic flow in cross and longitudinal section.展开更多
Today flotation column has become an acceptable means of froth flotation for a fairly broad range of applications, in particular the cleaning of sulfides. Even after having been used for several years in mineral proce...Today flotation column has become an acceptable means of froth flotation for a fairly broad range of applications, in particular the cleaning of sulfides. Even after having been used for several years in mineral processing plants, the full potential of the flotation column process is still not fully exploited. There is no prediction of process performance for the complete use of available control capabilities. The on-line estimation of grade usually requires a significant amount of work in maintenance and calibration of on-stream analyzers, in order to maintain good accuracy and high availability. These difficulties and the high cost of investment and maintenance of these devices have encouraged the approach of prediction of metal grade and recovery. In this paper, a new approach has been proposed for metallurgical performance prediction in flotation columns using Artificial Neural Network (ANN). Despite of the wide range of applications and flexibility of NNs, there is still no general framework or procedure through which the appropriate network for a specific task can be designed. Design and structural optimization of NNs is still strongly dependent upon the designer's experience. To mitigate this problem, a new method for the auto-design of NNs was used, based on Genetic Algorithm (GA). The new proposed method was evaluated by a case study in pilot plant flotation column at Sarcheshmeh copper plant. The chemical reagents dosage, froth height, air, wash water flow rates, gas holdup, Cu grade in the rougher feed, flotation column feed, column tail and final concentrate streams were used to the simulation by GANN. In this work, multi-layer NNs with Back Propagation (BP) algorithm with 8-17-10-2 and 8- 13-6-2 arrangements have been applied to predict the Cu and Mo grades and recoveries, respectively. The correlation coefficient (R) values for the testing sets for Cu and Mo grades were 0.93, 0.94 and for their recoveries were 0.93, 0.92, respectively. The results discussed in this paper indicate that the proposed model can be used to predict the Cu and Mo grades and recoveries with a reasonable error.展开更多
Level control in flotation columns is an important factor that influences the recovery and the grade of concentrate from the column. A flotation column is a nonlinear, multi-variable problem with changeable parameters...Level control in flotation columns is an important factor that influences the recovery and the grade of concentrate from the column. A flotation column is a nonlinear, multi-variable problem with changeable parameters that traditional methods have difficulty controlling. We have applied fuzzy control methods to the flotation column and tested the performance of the design by Matlab/Simulink simulation. The simulations show that level control in the flotation column becomes smoother and more rapid with the fuzzy controller. Compared to PID control methods the overshoot in valve position, the adjustment time, and the robustness of the controller are all improved. This indicates that it is suitable to model fuzzy controllers in applications for the study of automatic control of flotation column.展开更多
A new type of dissolved air released flotation column is developed to treat wastewater containing Cr（Ⅵ） based on advantages of both dissolved air floatation and column floatation. By using a column with a diameter ...A new type of dissolved air released flotation column is developed to treat wastewater containing Cr（Ⅵ） based on advantages of both dissolved air floatation and column floatation. By using a column with a diameter of 50 mm and a specially made dissolved air releaser, micro-bubbles inside the column can be formed. N2H4H2O was used as reductant, AlCl3 as flocculant, C12H25SO3Na（SDS） as surfactant in the experiment. The effects of pH of wastewater, pressure of dissolved air, ratio of return water, and concentration of flocculant and surfactant on the removal efficiency are studied. The results show that the efficiency of dissolved air released flotation column is much higher than that of other approaches after the operation parameters are optimized, with the reduction ratio of Cr（Ⅵ ） in wastewater reaching 98%. So this technique can be widely used in wastewater treatment展开更多
A new type of device,a dissolved-air flotation column,was developed for separation of oily wastewater. The unique design idea of the dissolved-air flotation column is the combined use of dissolved-air flotation and co...A new type of device,a dissolved-air flotation column,was developed for separation of oily wastewater. The unique design idea of the dissolved-air flotation column is the combined use of dissolved-air flotation and column flotation. The dissolved air release occurred within the column separation system. As a potential application the column was investigated for its performance in separating emulsified oil droplets in oily wastewater. A high separation efficiency was obtained in a series of tests. The aeration performance of the bubble generator used in the dissolved-air flotation column was also studied in particular.展开更多
Physical upgrading of graphite is typically achieved with many stages of grinding and flotation to produce a concentrate with approximately 95% carbon grade.An innovative grinding and column flotation process has been...Physical upgrading of graphite is typically achieved with many stages of grinding and flotation to produce a concentrate with approximately 95% carbon grade.An innovative grinding and column flotation process has been developed for efficient graphite upgrading to substantially simplify the process flowsheet and reduce operating costs.In this process,a high-pressure grinding roller(HPGR) and a stirred mill were employed as primary comminution techniques and a nanobubble flotation column as a key separation process.The results obtained with a crystalline flake graphite sample with a carbon grade of 11.15% show that the novel process can produce a concentrate with 94.82% carbon grade and 97.89% recovery from an open circuit of one rougher and two cleaner flotation stages.Scanning electron microscope(SEM)microphotographs indicate that HPGR offers the advantage of more effective protection of graphite flakes during crushing.Grinding test results show that stirred mill could not only protect graphite flakes but also promote the efficient liberation of graphite.Compared with the traditional flotation process,nanobubble flotation can effectively recover ultrafine graphite.The new process possesses a number of important advantages over the traditional method,including substantially higher graphite recovery,greatly simplified process flowsheet,better protection of flake size,reduced reagent consumption and process costs,etc.展开更多
The cyclonic static micro-bubble column flotation (FCSMC) is an effective separation device for fine particle treatment. The high mineralization rate and short flotation time of this equipment can be attributed to its...The cyclonic static micro-bubble column flotation (FCSMC) is an effective separation device for fine particle treatment. The high mineralization rate and short flotation time of this equipment can be attributed to its unique cyclonic force field. It also has been observed that the presence of a cyclonic force field leads to a lower bottom separation size limit and a reduction of unselective entrainment. The collection zone of the column is considered to consist of two parts,a column separation zone and a cyclonic zone. Total recovery of the collection zone was developed. For our study,we analyzed the particle movement in the cyclonic zone. Particle residence time equations for the cyclonic zone were de-rived by force analysis. Results obtained in this study provide a theoretical foundation for the design and scale-up of the FCSMC.展开更多
Flotation performance of a de-slimed（-150＋53μm）Jordanian siliceous phosphate was evaluated in a batch laboratory flotation column 100 cm high and 5 cm inside diameter.The collector used during anionic flotation wa...Flotation performance of a de-slimed（-150＋53μm）Jordanian siliceous phosphate was evaluated in a batch laboratory flotation column 100 cm high and 5 cm inside diameter.The collector used during anionic flotation was sodium oleate while an amine acetate（AEROMINE 3100C）was used for cationic flotation.Flotation comparison at different collector dosage,superficial gas velocity,and frother concentration showed that the maximum difference in performance between cationic and anionic flotation was obtained with these flotation parameters：30×10^（-6）（mg/L）frother concentration,250 g/t collector concentration,and 3.4 cm/s superficial gas velocity.At these operating conditions amine （cationic）flotation gave 7%higher flotation recovery,a 6%cleaner concentrate grade,and was 6%more efficient at removing silica.展开更多
We address problems in the development of large-scale flotation columns that use short cylinders. As a starting point, we investigated the packing medium to identify a highly efficient internal packing for the flotati...We address problems in the development of large-scale flotation columns that use short cylinders. As a starting point, we investigated the packing medium to identify a highly efficient internal packing for the flotation column. The chosen packing was a honeycomb structure with an aperture diameter of 80 mm, a web thickness of 0.80 mm, a film height of 1000 mm, packed into a 400 mm diameter space, which completely filled the vessel at optimal cost. The column consisted of a modular ring of single-hole hexagonal honeycomb tube packing made from atactic polyproplene (PP-R). The packing was tested in a cyclonic, static micro-bubble flotation column. Computational fluid dynamic modeling was used to analyze the flotation fluid in a honeycomb tube packed flotation column. Our results show that the fluid axial movement was maximized and that the transverse fluid velocities were zero in the vicinity of axial flow. Using the honeycomb tube packing for copper sulfide flotation we observed that the average concentration in the product was increased to 25.41%, from an average feed concentration of 0.729%, with an average recovery of 92.92%. The demands of on-site industrial production were met.展开更多
A low grade graphite ore from eastern India was beneficiated by flotation to improve its quality. The ore was composed of 87.80%ash and 8.59%fixed carbon. Primary coarse wet grinding （d80：186 μm） followed by rough...A low grade graphite ore from eastern India was beneficiated by flotation to improve its quality. The ore was composed of 87.80%ash and 8.59%fixed carbon. Primary coarse wet grinding （d80：186 μm） followed by rougher flotation in Denver flotation cell using diesel as collector and pine oil as frother yielded a rougher concentrate. Regrinding （d80：144 μm） of this rougher concentrate was opted for further libera-tion of graphite. It was followed by cleaning in laboratory flotation column. This combined process of relatively coarse primary grinding followed by regrinding and cleaning in flotation column resulted in final concentrate of 7.44% yield with 89.65% fixed carbon and 6.00% ash. This approach of two-stage grinding to recover the flake graphite at the coarsest possible grind can help to minimize grinding energy costs. A conceptual flow sheet which is cost effective was developed based on this methodology.展开更多
The cyclonic-static microbubble flotation column has dual effects including the cyclonic separation and floatation separation with the characteristics of the small lower limit of the effective separation size, short s...The cyclonic-static microbubble flotation column has dual effects including the cyclonic separation and floatation separation with the characteristics of the small lower limit of the effective separation size, short separation time, large handling capacity, and low operation cost. It shows significant advantages in the oily wastewater treatment field, especially the polymer flooding oily wastewater treatment aspect. In this paper, the cyclonic separation function mechanism of the cyclonic-static microbubble flotation column was studied, the impact of the parameters including the feeding rate, aeration rate, circulating pressure, and underflow split ratio on the cyclonic separation efficiency was investigated, and the cyclonic separation efficiency model was established as well. In addition, by applying the Doppler Laser Velocimeter (LDV) and Fluent simulation software, the test and simulation to the single-phase flow velocity field of the cyclonic separation section of the cyclonic-static microbubble flotation column were carried out, and the velocity distribution rule of the cyclonic separation section was analyzed under the singlephase flow conditions.展开更多
Low grade dumped limestone sample having high silica of 8.1%, 36.8% CaO, and 3% Al2O3 has been studied with the aim to reduce the silica level to below 3% for its utilization in iron making. Beneficiation study of the...Low grade dumped limestone sample having high silica of 8.1%, 36.8% CaO, and 3% Al2O3 has been studied with the aim to reduce the silica level to below 3% for its utilization in iron making. Beneficiation study of the sample was initiated with desliming of the feed sample of -100 μm to remove the siliceous ultrafine particles and to improve the feed quality. Flotation study was carried out by column flotation technique varying the collector dosage, superficial air flow velocity and froth depth to assess their effect on silica reduction and CaO recovery. It was observed that increased collector dosage and superficial air velocity increases the recovery of CaO, and increase in the froth depth reduces the mass flow and silica content in the concentrate. The best result was found at 1.25 cm/sec superficial air velocity, 25 cm froth depth, 1.25 kgpt collector dosage and concentrate assayed 47.3% CaO, 2.8% silica with 72% CaO recovery.展开更多
Hydrodynamic cavitaion venturi tube technique is used for pico and nano bubble generations in coal column flotation. In order to determine the optimal design of hydrodynamic cavitation venture tube for pico and nano b...Hydrodynamic cavitaion venturi tube technique is used for pico and nano bubble generations in coal column flotation. In order to determine the optimal design of hydrodynamic cavitation venture tube for pico and nano bubble generation, a four-factor three-level Central Composite Design of Experimental was conducted for investigating four important design parameters of cavitation venturi tube governing the median size and the volume of pico and nano bubbles. The test results showed that maximum volume of pico and nano bubbles, 65–75%, and minimum mean pico and nano bubble size,150–240 nm, were achieved at the medium ratio of the diameter of outlet of the venturi-tube and diameter of throat(3–4), medium outlet angle(11–13°), high inlet angle(26–27°) and high ratio of the length of the throat and the diameter of throat(2.3–3). Study the effects of the producing pico and nano bubbles on fine coal flotation was performed in a 5 cm diameter 260 cm height flotation column. The optimal percentage of pico and nano bubbles was about 70%, which produced maximum combustible material recovery of 86% with clean coal ash content of 11.7%.展开更多
基金Projects 2008BAB31B01 supported by the National Key Technology R&D Program in the 11th Five-Year Plan of China50834006 by the National Natural Science Foundation of China
文摘In our study we investigated a refractory copper-nickel sulfide ore separation by using a cyclonic-static micro-bubble flotation column (FCSMC). The process mineralogy of the main products was studied. Using a scanning electron microscope-energy dispersive system (SEM-EDS) and an X-ray spectrometer the mineral category and content of samples were analyzed. By using a mineral liberation analyzer (MLA) the mineral liberation characteristics were revealed. It is shown that in roughing feed the monomers liberation degree of nickel pyrite and chalcopyrite take up 84.11% and 88.82%, respectively. In tailings, the lost nickel pyrite and chalcopyrite are mainly monomers. Therefore, strengthening the micro-fine particle recovery capacity is the key to increase recovery.
基金Financial supports for this work provided by the National High Technology Research and Development Program of China (No.2008BAB31B02) is gratefully acknowledged
文摘The Cyclonic-Static Microbubble Flotation Column (FCSMC) is currently a widely used, novel type of flotation device. The self-absorbing microbubble generator is the core component of this device. The structure of the microbubble generator directly influences flotation column performance by affecting bubble size and distribution as well as gas holdup in the column. However, the complicated flow inside the generator results in high R&D costs and difficulty in testing. Thus, the CFD software, FLUENT, was used to simulate the gas-liquid two-phase flow inside a self-absorbing microbubble generator. The effect of area ratio, a key structural parameter, was studied in detail. Critical flow-field parameters including velocity, turbulent kinetic energy, minimum static pressure and gas holdup were obtained. The simulation results demonstrate that the optimum area ratio is 3.
基金Project 50425414 supported by the National Outstanding Youth Science Foundation of China
文摘A packing-flotation column was proposed to optimize the flotation environment A research system was es- tablished using a 100 mm diameter cyclonic micro-bubble flotation column to study fluid properties. Dry-plate and wet- plate pressure drops were studied and the corresponding pressure drop equations developed. The results show that the dry-plate pressure drop of the packing cyclonic micro-bubble flotation column is 10–15 times less than that of the chemical tower, which is principally shown in its relatively small resistance coefficient, ξ ≈0.0207. The wet-plate pressure drop is 2–3 times higher than that of the chemical tower, which is largely caused by the separation materials and characteristics of the equipment. With flotation, the greater the pressure drop, the better the flotation environment.
基金the State Key Basic Research Program of China (No. 2012CB214905)Key Program of National Natural Science Foundation of China (No. 500834006)the National Natural Science Foundation of China (No. 50974119) for financial support
文摘Laboratory experiments have been conducted to study the flow field in a cyclone static micro-bubble flotation column. The method of Particle Image Velocimetry (PIV) was used. The flow field velocity distribution in both cross section and longitudinal section within cyclonic zone was studied for different circulating volumes. The cross sectional vortex was also analyzed. The results show that in cross section as the circulating volume increases from 0.187 to 0.350 m 3 /h, the flow velocity ranges from 0 to 0.68 m/s. The flow field is mainly a non-vortex potential flow that forms a free vortex without outside energy input. In the cyclonic region the vortex deviates from the center of the flotation column because a single tangential opening introduces circulating fluid into the column. The tangential component of the velocity plays a defining role in the cross section. In the longitudinal section the velocity ranges from 0 to 0.08 m/s. The flow velocity increases as does the circulating volume. Advantageous mineral separation conditions arise from the combined effects of cyclonic flow in cross and longitudinal section.
基金the support of the Department of Research and Development of Sarcheshmeh copper plants for this research
文摘Today flotation column has become an acceptable means of froth flotation for a fairly broad range of applications, in particular the cleaning of sulfides. Even after having been used for several years in mineral processing plants, the full potential of the flotation column process is still not fully exploited. There is no prediction of process performance for the complete use of available control capabilities. The on-line estimation of grade usually requires a significant amount of work in maintenance and calibration of on-stream analyzers, in order to maintain good accuracy and high availability. These difficulties and the high cost of investment and maintenance of these devices have encouraged the approach of prediction of metal grade and recovery. In this paper, a new approach has been proposed for metallurgical performance prediction in flotation columns using Artificial Neural Network (ANN). Despite of the wide range of applications and flexibility of NNs, there is still no general framework or procedure through which the appropriate network for a specific task can be designed. Design and structural optimization of NNs is still strongly dependent upon the designer's experience. To mitigate this problem, a new method for the auto-design of NNs was used, based on Genetic Algorithm (GA). The new proposed method was evaluated by a case study in pilot plant flotation column at Sarcheshmeh copper plant. The chemical reagents dosage, froth height, air, wash water flow rates, gas holdup, Cu grade in the rougher feed, flotation column feed, column tail and final concentrate streams were used to the simulation by GANN. In this work, multi-layer NNs with Back Propagation (BP) algorithm with 8-17-10-2 and 8- 13-6-2 arrangements have been applied to predict the Cu and Mo grades and recoveries, respectively. The correlation coefficient (R) values for the testing sets for Cu and Mo grades were 0.93, 0.94 and for their recoveries were 0.93, 0.92, respectively. The results discussed in this paper indicate that the proposed model can be used to predict the Cu and Mo grades and recoveries with a reasonable error.
基金support from the Fundamental Research Funds for the Central Universitiesthe National Key Technology R & D Program in the 11th Five Year Plan of China (No. 2008BAB31B03)
文摘Level control in flotation columns is an important factor that influences the recovery and the grade of concentrate from the column. A flotation column is a nonlinear, multi-variable problem with changeable parameters that traditional methods have difficulty controlling. We have applied fuzzy control methods to the flotation column and tested the performance of the design by Matlab/Simulink simulation. The simulations show that level control in the flotation column becomes smoother and more rapid with the fuzzy controller. Compared to PID control methods the overshoot in valve position, the adjustment time, and the robustness of the controller are all improved. This indicates that it is suitable to model fuzzy controllers in applications for the study of automatic control of flotation column.
基金Projects 50425414 supported by National Fund for Distinguished Young Scholars and B200403 by Science and Technology Fund of China University ofMining &Technology
文摘A new type of dissolved air released flotation column is developed to treat wastewater containing Cr（Ⅵ） based on advantages of both dissolved air floatation and column floatation. By using a column with a diameter of 50 mm and a specially made dissolved air releaser, micro-bubbles inside the column can be formed. N2H4H2O was used as reductant, AlCl3 as flocculant, C12H25SO3Na（SDS） as surfactant in the experiment. The effects of pH of wastewater, pressure of dissolved air, ratio of return water, and concentration of flocculant and surfactant on the removal efficiency are studied. The results show that the efficiency of dissolved air released flotation column is much higher than that of other approaches after the operation parameters are optimized, with the reduction ratio of Cr（Ⅵ ） in wastewater reaching 98%. So this technique can be widely used in wastewater treatment
基金Projects 50425414 supported by thte National Fund for Distinguished Young Scholars2006A019 by the Science and Technology Fund of China University of Mining &Technology
文摘A new type of device,a dissolved-air flotation column,was developed for separation of oily wastewater. The unique design idea of the dissolved-air flotation column is the combined use of dissolved-air flotation and column flotation. The dissolved air release occurred within the column separation system. As a potential application the column was investigated for its performance in separating emulsified oil droplets in oily wastewater. A high separation efficiency was obtained in a series of tests. The aeration performance of the bubble generator used in the dissolved-air flotation column was also studied in particular.
基金supported by the Fundamental Research Funds for the Central Universities (No. 2019XKQYMS45)。
文摘Physical upgrading of graphite is typically achieved with many stages of grinding and flotation to produce a concentrate with approximately 95% carbon grade.An innovative grinding and column flotation process has been developed for efficient graphite upgrading to substantially simplify the process flowsheet and reduce operating costs.In this process,a high-pressure grinding roller(HPGR) and a stirred mill were employed as primary comminution techniques and a nanobubble flotation column as a key separation process.The results obtained with a crystalline flake graphite sample with a carbon grade of 11.15% show that the novel process can produce a concentrate with 94.82% carbon grade and 97.89% recovery from an open circuit of one rougher and two cleaner flotation stages.Scanning electron microscope(SEM)microphotographs indicate that HPGR offers the advantage of more effective protection of graphite flakes during crushing.Grinding test results show that stirred mill could not only protect graphite flakes but also promote the efficient liberation of graphite.Compared with the traditional flotation process,nanobubble flotation can effectively recover ultrafine graphite.The new process possesses a number of important advantages over the traditional method,including substantially higher graphite recovery,greatly simplified process flowsheet,better protection of flake size,reduced reagent consumption and process costs,etc.
基金Project 50425414 supported by the National Outstanding Youth Science Foundation of China
文摘The cyclonic static micro-bubble column flotation (FCSMC) is an effective separation device for fine particle treatment. The high mineralization rate and short flotation time of this equipment can be attributed to its unique cyclonic force field. It also has been observed that the presence of a cyclonic force field leads to a lower bottom separation size limit and a reduction of unselective entrainment. The collection zone of the column is considered to consist of two parts,a column separation zone and a cyclonic zone. Total recovery of the collection zone was developed. For our study,we analyzed the particle movement in the cyclonic zone. Particle residence time equations for the cyclonic zone were de-rived by force analysis. Results obtained in this study provide a theoretical foundation for the design and scale-up of the FCSMC.
基金done during the first author's Fulbright fellowship at the Center for Advanced Separation (CAST)/Virginia Technical Institute and State University-USA. Salah would like to thank all the people who work at CAST for their friendship and support during his stay in Blacksburg, VA.
文摘Flotation performance of a de-slimed（-150＋53μm）Jordanian siliceous phosphate was evaluated in a batch laboratory flotation column 100 cm high and 5 cm inside diameter.The collector used during anionic flotation was sodium oleate while an amine acetate（AEROMINE 3100C）was used for cationic flotation.Flotation comparison at different collector dosage,superficial gas velocity,and frother concentration showed that the maximum difference in performance between cationic and anionic flotation was obtained with these flotation parameters：30×10^（-6）（mg/L）frother concentration,250 g/t collector concentration,and 3.4 cm/s superficial gas velocity.At these operating conditions amine （cationic）flotation gave 7%higher flotation recovery,a 6%cleaner concentrate grade,and was 6%more efficient at removing silica.
基金Project 2007AA05Z339 supported by the National High-Tech Research and Development Program of China
文摘We address problems in the development of large-scale flotation columns that use short cylinders. As a starting point, we investigated the packing medium to identify a highly efficient internal packing for the flotation column. The chosen packing was a honeycomb structure with an aperture diameter of 80 mm, a web thickness of 0.80 mm, a film height of 1000 mm, packed into a 400 mm diameter space, which completely filled the vessel at optimal cost. The column consisted of a modular ring of single-hole hexagonal honeycomb tube packing made from atactic polyproplene (PP-R). The packing was tested in a cyclonic, static micro-bubble flotation column. Computational fluid dynamic modeling was used to analyze the flotation fluid in a honeycomb tube packed flotation column. Our results show that the fluid axial movement was maximized and that the transverse fluid velocities were zero in the vicinity of axial flow. Using the honeycomb tube packing for copper sulfide flotation we observed that the average concentration in the product was increased to 25.41%, from an average feed concentration of 0.729%, with an average recovery of 92.92%. The demands of on-site industrial production were met.
文摘A low grade graphite ore from eastern India was beneficiated by flotation to improve its quality. The ore was composed of 87.80%ash and 8.59%fixed carbon. Primary coarse wet grinding （d80：186 μm） followed by rougher flotation in Denver flotation cell using diesel as collector and pine oil as frother yielded a rougher concentrate. Regrinding （d80：144 μm） of this rougher concentrate was opted for further libera-tion of graphite. It was followed by cleaning in laboratory flotation column. This combined process of relatively coarse primary grinding followed by regrinding and cleaning in flotation column resulted in final concentrate of 7.44% yield with 89.65% fixed carbon and 6.00% ash. This approach of two-stage grinding to recover the flake graphite at the coarsest possible grind can help to minimize grinding energy costs. A conceptual flow sheet which is cost effective was developed based on this methodology.
基金the National Natural Science Foundation of China (No. 50974119) for the financial support for this project
文摘The cyclonic-static microbubble flotation column has dual effects including the cyclonic separation and floatation separation with the characteristics of the small lower limit of the effective separation size, short separation time, large handling capacity, and low operation cost. It shows significant advantages in the oily wastewater treatment field, especially the polymer flooding oily wastewater treatment aspect. In this paper, the cyclonic separation function mechanism of the cyclonic-static microbubble flotation column was studied, the impact of the parameters including the feeding rate, aeration rate, circulating pressure, and underflow split ratio on the cyclonic separation efficiency was investigated, and the cyclonic separation efficiency model was established as well. In addition, by applying the Doppler Laser Velocimeter (LDV) and Fluent simulation software, the test and simulation to the single-phase flow velocity field of the cyclonic separation section of the cyclonic-static microbubble flotation column were carried out, and the velocity distribution rule of the cyclonic separation section was analyzed under the singlephase flow conditions.
文摘Low grade dumped limestone sample having high silica of 8.1%, 36.8% CaO, and 3% Al2O3 has been studied with the aim to reduce the silica level to below 3% for its utilization in iron making. Beneficiation study of the sample was initiated with desliming of the feed sample of -100 μm to remove the siliceous ultrafine particles and to improve the feed quality. Flotation study was carried out by column flotation technique varying the collector dosage, superficial air flow velocity and froth depth to assess their effect on silica reduction and CaO recovery. It was observed that increased collector dosage and superficial air velocity increases the recovery of CaO, and increase in the froth depth reduces the mass flow and silica content in the concentrate. The best result was found at 1.25 cm/sec superficial air velocity, 25 cm froth depth, 1.25 kgpt collector dosage and concentrate assayed 47.3% CaO, 2.8% silica with 72% CaO recovery.
基金West Virginia State Coal and Energy Research Bureau(WVCERB)the Department of Mining Engineering,West Virginia University
文摘Hydrodynamic cavitaion venturi tube technique is used for pico and nano bubble generations in coal column flotation. In order to determine the optimal design of hydrodynamic cavitation venture tube for pico and nano bubble generation, a four-factor three-level Central Composite Design of Experimental was conducted for investigating four important design parameters of cavitation venturi tube governing the median size and the volume of pico and nano bubbles. The test results showed that maximum volume of pico and nano bubbles, 65–75%, and minimum mean pico and nano bubble size,150–240 nm, were achieved at the medium ratio of the diameter of outlet of the venturi-tube and diameter of throat(3–4), medium outlet angle(11–13°), high inlet angle(26–27°) and high ratio of the length of the throat and the diameter of throat(2.3–3). Study the effects of the producing pico and nano bubbles on fine coal flotation was performed in a 5 cm diameter 260 cm height flotation column. The optimal percentage of pico and nano bubbles was about 70%, which produced maximum combustible material recovery of 86% with clean coal ash content of 11.7%.
