This paper discusses the influence of Sb/In ratio on the transport properties and crystal quality of the 200 nm InAs_(x)Sb_(1-x)thin film.The Sb content of InAs_(x)Sb_(1-x)thin film in all samples was verified by HRXR...This paper discusses the influence of Sb/In ratio on the transport properties and crystal quality of the 200 nm InAs_(x)Sb_(1-x)thin film.The Sb content of InAs_(x)Sb_(1-x)thin film in all samples was verified by HRXRD of the symmetrical 004 reflections and asymmetrical 115 reflections.The calculation results show that the Sb component was 0.6 in the InAs_(x)Sb_(1-x)thin film grown under the conditions of Sb/In ratio of 6 and As/In ratio of 3,which has the highest electron mobility(28560 cm^(2)/V·s)at 300 K.At the same time,the influence ofⅤ/Ⅲratio on the transport properties and crystal quality of Al_(0.2)In_(0.8)Sb/InAs_(x)Sb_(1-x)quantum well heterostructures also has been investigated.As a result,the Al_(0.2)In_(0.8)Sb/InAs_(0.4)Sb_(0.6)quantum well heterostructure with a channel thickness of 30 nm grown under the conditions of Sb/In ratio of 6 and As/In ratio of 3 has a maximum electron mobility of 28300 cm^(2)/V·s and a minimum RMS roughness of 0.68 nm.Through optimizing the growth conditions,our samples have higher electron mobility and smoother surface morphology.展开更多
To improve the microstructure and properties of the electron beam welded joints, the vacuum or furnace whole post weld heat treatment (FWPWHT) usually should be done on it. The electron beam local post weld heat treat...To improve the microstructure and properties of the electron beam welded joints, the vacuum or furnace whole post weld heat treatment (FWPWHT) usually should be done on it. The electron beam local post weld heat treatment (EBLPWHT) is a rather new heat treatment procedure that provides the advantages of high precision, flexibility and efficiency, energy saving and higher productivity. In this paper, the microstructure, mechanical properties, fracture toughness and fatigue properties of electron beam welded joints of 30CrMnSiNi2A steel in as-welded (AW) and EBLPWHT conditions have been investigated respectively. The results show that the microstructures of different zones of joints in as-welded condition are changed by EBLPWHT procedure, in which the welds from coarse needle martensite into lath-shaped martensite; the main structures of heat affected zones (HAZ) from lath-shaped martensite into lower bainite. The properties of welded joints can be improved by the EBLPWHT in some extent, especially the fracture toughness of the welds and the fatigue crack resistance of welded joints can be sufficiently improved. However, more appropriate heat treatment parameters of the EBLPWHT have to be studied in order to increase the mechanical properties of base metal near by the HAZ.展开更多
Prediction of weld bead geometry is always an interesting and challenging research topic as it involves understanding of complex multi input and multi output system. The weld bead geometry has a profound impact on the...Prediction of weld bead geometry is always an interesting and challenging research topic as it involves understanding of complex multi input and multi output system. The weld bead geometry has a profound impact on the load bearing capability of a weld joint, which in-turn decides the performance in real time service conditions. The present study introduces a novel approach of detecting a relationship between weld bead geometry and mechanical properties(e.g. tensile load) for the purpose of catering the best the process could offer. The significance of the proposed approach is demonstrated by a case of dissimilar aluminium alloy(AA2219 and AA5083) electron beam welds. A mathematical model of tensile braking load as a function of geometrical attributes of weld bead geometry is presented. The results of investigation suggests the effective thickness of weld-a geometric parameter of weld bead has the most significant influence on tensile breaking load of dissimilar weld joint. The observations on bead geometry and the mechanical properties(microhardness, ultimate tensile load and face bend angle) are correlated with detailed metallurgical analysis. The fusion zone of dissimilar electron beam weld has finer grain size with a moderate evaporation and segregation of alloying elements magnesium and copper respectively.The mechanical properties of weld joint are controlled by optimum bead geometry and HAZ softening in weaker AA5083 Al alloy.展开更多
Tests were carried out on 8 self-compacting reinforced concrete(SCC) beams and 4 normal reinforced concrete beams. The effects of mode of consolidation,load level,reinforcing ratio and structural type on long term beh...Tests were carried out on 8 self-compacting reinforced concrete(SCC) beams and 4 normal reinforced concrete beams. The effects of mode of consolidation,load level,reinforcing ratio and structural type on long term behavior of SCC were investigated. Under the same environmental conditions,the shrinkage-time curve of self-compacting concrete beam is very similar to that of normal concrete beam. For both self-compacting reinforced concrete beams and normal reinforced concrete beams,the rate of shrinkage at early stages is higher,the shrinkage strain at 2 months is about 60% of the maximum value at one year. The shrinkage strain of self-compacting reinforced concrete beam after one year is about 450×10-6. Creep deflection of self-compacting reinforced concrete beam decreases as the tensile reinforcing ratio increases. The deflection creep coefficient of self-compacting reinforced concrete beam after one and a half year is about 1.6,which is very close to that of normal reinforced concrete beams cast with vibration. Extra cautions considering shrinkage and creep behavior are not needed for the use of SCC in engineering practices.展开更多
A pulse generator with a voltage rise time of~1.5 ns and voltage amplitude variable from 30 kV to 200 kV was designed for generating runaway electron beams in atmospheric pressure air with different interelectrode ga...A pulse generator with a voltage rise time of~1.5 ns and voltage amplitude variable from 30 kV to 200 kV was designed for generating runaway electron beams in atmospheric pressure air with different interelectrode gaps.The influence of the voltage amplitude and gap length on the generation was studied.In the gas diode geometry under study,the gap voltage at which the generation of a runaway electron beam begins was determined.Decreasing the voltage pulse amplitude does not increase the beam current pulse width measured with a time resolution of~0.1 ns.It is shown that the escape of beam electrons to the downstream of the foil is sync in time with the voltage drop across the gap,and that the delay of beam current generation increases gradually from 1.1 ns to 2.6 ns as the voltage pulse amplitude across the gap decreases from~100 kV to 40 kV.展开更多
In this paper,subnanosecond-pulse and one-nanosecond-pulse generators are used to study the breakdowns in highly overvolted gaps in atmospheric pressure air.With different cathodes,we measured the applied voltage and ...In this paper,subnanosecond-pulse and one-nanosecond-pulse generators are used to study the breakdowns in highly overvolted gaps in atmospheric pressure air.With different cathodes,we measured the applied voltage and discharge current to investigate the dynamic characteristics in the subnanosecond breakdown during the generation of a supershort avalanche electron beam.Especially,characteristics of dynamic displacement current are presented in the current paper,which is detected between the ionization wave front and a plane anode.It is shown that during a subnanosecond voltage rise time,the amplitude of the dynamic displacement current can be higher than 4 kA.It is demonstrated that the breakdown in the air gap is assisted by ionization processes between the ionization wave front and a plane anode.展开更多
Electron beam lithography(EBL) is a key technology in the fabrication of nanoscale silicon optical waveguide. The influence of exposure dose, the main process parameter of EBL, on the structure profile of poly-methyl ...Electron beam lithography(EBL) is a key technology in the fabrication of nanoscale silicon optical waveguide. The influence of exposure dose, the main process parameter of EBL, on the structure profile of poly-methyl methacrylate(PMMA) after development was studied using a silicon on insulator(SOI) wafer with 220 nm top silicon as the substrate. The relationship between exposure dose and structure pattern width after development was analyzed according to the measurement results. The optimum exposure dose of 220 μC/cm^(2) was found to obtain a final structure consistent with the designed mask value through subsequent processes. At the same time, according to the image segmentation curve tracking technology, the contour extraction process of the dose test results was carried out, and the relationship among mask design value, exposure dose and two-dimensional roughness of boundary contour was analyzed, which can provide reference for the subsequent electron beam lithography of the same substrate material.展开更多
The high-temperature oxidation resistance behavior of 7% (mass fraction) Y203-ZrO2 thermal barrier coatings (TBCs) irradiated by high-intensity pulsed ion beam (HIPIB) was investigated under the cyclic oxidation...The high-temperature oxidation resistance behavior of 7% (mass fraction) Y203-ZrO2 thermal barrier coatings (TBCs) irradiated by high-intensity pulsed ion beam (HIPIB) was investigated under the cyclic oxidation condition of 1 050 ℃ and 1 h. The columnar grains in the TBCs disappear after the HIPIB irradiation at ion current densities of 100-200 A/cm^2 and the irradiated surface becomes smooth and densified after remelting and ablation due to the HIPIB irradiation. The thermally grown oxide (TGO) layer thickness of the irradiated TBCs is smaller than that of the original TBCs. After 15 cycles, the mass gains of the original TBCs and those irradiated by ion current densities of 100 and 200 A/cm^2 due to the oxidation are found to be 0.8-0.9, 0.6-0.7, and 0.3-0.4 mg/cm^2, respectively. The inward diffusion of oxygen through the irradiated TBCs is significantly impeded by the densified top layer formed due to irradiation, which is the main reason for the improved overall oxidation resistance of the irradiated TBCs.展开更多
High nitrogen stainless steel(HNS) is a nickel free austenitic stainless steel that is used as a structural component in defence applications for manufacturing battle tanks as a replacement of the existing armour grad...High nitrogen stainless steel(HNS) is a nickel free austenitic stainless steel that is used as a structural component in defence applications for manufacturing battle tanks as a replacement of the existing armour grade steel owing to its low cost, excellent mechanical properties and better corrosion resistance.Conventional fusion welding causes problems like nitrogen desorption, solidification cracking in weld zone, liquation cracking in heat affected zone, nitrogen induced porosity and poor mechanical properties.The above problems can be overcome by proper selection and procedure of joining process. In the present work, an attempt has been made to correlate the microstructural changes with mechanical properties of fusion and solid state welds of high nitrogen steel. Shielded metal arc welding(SMAW), gas tungsten arc welding(GTAW), electron beam welding(EBW) and friction stir welding(FSW) processes were used in the present work. Optical microscopy, scanning electron microscopy and electron backscatter diffraction were used to characterize microstructural changes. Hardness, tensile and bend tests were performed to evaluate the mechanical properties of welds. The results of the present investigation established that fully austenitic dendritic structure was found in welds of SMAW. Reverted austenite pools in the martensite matrix in weld zone and unmixed zones near the fusion boundary were observed in GTA welds. Discontinuous ferrite network in austenite matrix was observed in electron beam welds.Fine recrystallized austenite grain structure was observed in the nugget zone of friction stir welds.Improved mechanical properties are obtained in friction stir welds when compared to fusion welds. This is attributed to the refined microstructure consisting of equiaxed and homogenous austenite grains.展开更多
The one-dimensional photonic crystals of Ag/SiO_(2) system are studied to investigate the photonic band gaps (PBG). The samples were prepared by the ultra-high vacuum electron beam evaporation. The clear band gaps wer...The one-dimensional photonic crystals of Ag/SiO_(2) system are studied to investigate the photonic band gaps (PBG). The samples were prepared by the ultra-high vacuum electron beam evaporation. The clear band gaps were observed. Satisfactory agreement between experimental and calculated results was obtained without fitting. The thickness of SiO_(2 )film has influence on the photonic band gap, as well as it awfully affects the transmittance of Ag. More layers can get clearer PBG.展开更多
Based on the basic operating principal and the technology characteristic of electron beam physical vapor deposition(EBPVD) technique, EBPVD was used to prepare the micro-layer composites. The effect on the substrate p...Based on the basic operating principal and the technology characteristic of electron beam physical vapor deposition(EBPVD) technique, EBPVD was used to prepare the micro-layer composites. The effect on the substrate preheating temperature was taken into accounts and the finite element analysis package ANSYS was used to simulate the internal stress field and the potential displacement changing tendency. The results show that one of the most important quality factors on the judgment of micro-layer composites is the adhesion between the substrate and the deposition layers as well as among the different deposition layers. Besides the existance of temperature gradient through the thickness of layers, the main reason for the internal stress in micro-layer composites is the mismatch of various properties of the layer and the substrate of different thermal expansions and crystal lattice types. With the increase of substrate preheating temperature, the inter-laminar shear stress also takes on a tendency of increase but the axial residual stress decrease.展开更多
基金Supported by the Natural Science Basic Research Program of Shaanxi Province(2023-JC-QN-0758)Shaanxi University of Science and Technology Research Launch Project(2020BJ-26)Doctoral Research Initializing Fund of Hebei University of Science and Technology,China(1181476).
文摘This paper discusses the influence of Sb/In ratio on the transport properties and crystal quality of the 200 nm InAs_(x)Sb_(1-x)thin film.The Sb content of InAs_(x)Sb_(1-x)thin film in all samples was verified by HRXRD of the symmetrical 004 reflections and asymmetrical 115 reflections.The calculation results show that the Sb component was 0.6 in the InAs_(x)Sb_(1-x)thin film grown under the conditions of Sb/In ratio of 6 and As/In ratio of 3,which has the highest electron mobility(28560 cm^(2)/V·s)at 300 K.At the same time,the influence ofⅤ/Ⅲratio on the transport properties and crystal quality of Al_(0.2)In_(0.8)Sb/InAs_(x)Sb_(1-x)quantum well heterostructures also has been investigated.As a result,the Al_(0.2)In_(0.8)Sb/InAs_(0.4)Sb_(0.6)quantum well heterostructure with a channel thickness of 30 nm grown under the conditions of Sb/In ratio of 6 and As/In ratio of 3 has a maximum electron mobility of 28300 cm^(2)/V·s and a minimum RMS roughness of 0.68 nm.Through optimizing the growth conditions,our samples have higher electron mobility and smoother surface morphology.
文摘To improve the microstructure and properties of the electron beam welded joints, the vacuum or furnace whole post weld heat treatment (FWPWHT) usually should be done on it. The electron beam local post weld heat treatment (EBLPWHT) is a rather new heat treatment procedure that provides the advantages of high precision, flexibility and efficiency, energy saving and higher productivity. In this paper, the microstructure, mechanical properties, fracture toughness and fatigue properties of electron beam welded joints of 30CrMnSiNi2A steel in as-welded (AW) and EBLPWHT conditions have been investigated respectively. The results show that the microstructures of different zones of joints in as-welded condition are changed by EBLPWHT procedure, in which the welds from coarse needle martensite into lath-shaped martensite; the main structures of heat affected zones (HAZ) from lath-shaped martensite into lower bainite. The properties of welded joints can be improved by the EBLPWHT in some extent, especially the fracture toughness of the welds and the fatigue crack resistance of welded joints can be sufficiently improved. However, more appropriate heat treatment parameters of the EBLPWHT have to be studied in order to increase the mechanical properties of base metal near by the HAZ.
基金financial support from Defence Research and Development Organisation(DRDO)
文摘Prediction of weld bead geometry is always an interesting and challenging research topic as it involves understanding of complex multi input and multi output system. The weld bead geometry has a profound impact on the load bearing capability of a weld joint, which in-turn decides the performance in real time service conditions. The present study introduces a novel approach of detecting a relationship between weld bead geometry and mechanical properties(e.g. tensile load) for the purpose of catering the best the process could offer. The significance of the proposed approach is demonstrated by a case of dissimilar aluminium alloy(AA2219 and AA5083) electron beam welds. A mathematical model of tensile braking load as a function of geometrical attributes of weld bead geometry is presented. The results of investigation suggests the effective thickness of weld-a geometric parameter of weld bead has the most significant influence on tensile breaking load of dissimilar weld joint. The observations on bead geometry and the mechanical properties(microhardness, ultimate tensile load and face bend angle) are correlated with detailed metallurgical analysis. The fusion zone of dissimilar electron beam weld has finer grain size with a moderate evaporation and segregation of alloying elements magnesium and copper respectively.The mechanical properties of weld joint are controlled by optimum bead geometry and HAZ softening in weaker AA5083 Al alloy.
基金Project(50278097) supported by the National Natural Science Foundation of China
文摘Tests were carried out on 8 self-compacting reinforced concrete(SCC) beams and 4 normal reinforced concrete beams. The effects of mode of consolidation,load level,reinforcing ratio and structural type on long term behavior of SCC were investigated. Under the same environmental conditions,the shrinkage-time curve of self-compacting concrete beam is very similar to that of normal concrete beam. For both self-compacting reinforced concrete beams and normal reinforced concrete beams,the rate of shrinkage at early stages is higher,the shrinkage strain at 2 months is about 60% of the maximum value at one year. The shrinkage strain of self-compacting reinforced concrete beam after one year is about 450×10-6. Creep deflection of self-compacting reinforced concrete beam decreases as the tensile reinforcing ratio increases. The deflection creep coefficient of self-compacting reinforced concrete beam after one and a half year is about 1.6,which is very close to that of normal reinforced concrete beams cast with vibration. Extra cautions considering shrinkage and creep behavior are not needed for the use of SCC in engineering practices.
基金Project supported by Russian Foundation for Basic Research (12-08-91150-GFEN_a), National Natural Science Foundation of China (51222701, 51207154, 51211120183), National Basic Research Program of China (973 Program) (20llCB209402), Opening Project of State Key Laboratory of Electrical Insulation and Power Equipment in Xi'an Jiaotong University (EIPEI2204), Chinese Academy of Sciences Visiting Professorship for Senior International Scientists (2012TtG0021).
文摘A pulse generator with a voltage rise time of~1.5 ns and voltage amplitude variable from 30 kV to 200 kV was designed for generating runaway electron beams in atmospheric pressure air with different interelectrode gaps.The influence of the voltage amplitude and gap length on the generation was studied.In the gas diode geometry under study,the gap voltage at which the generation of a runaway electron beam begins was determined.Decreasing the voltage pulse amplitude does not increase the beam current pulse width measured with a time resolution of~0.1 ns.It is shown that the escape of beam electrons to the downstream of the foil is sync in time with the voltage drop across the gap,and that the delay of beam current generation increases gradually from 1.1 ns to 2.6 ns as the voltage pulse amplitude across the gap decreases from~100 kV to 40 kV.
基金Project supported by Russian Foundation for Basic Research (12-08-91150-FOEH_a and 12-08-00105-a), National Natural Science Foundation of China (51222701, 51207154, 51211120183), and the Chinese Academy of Sciences Visiting Professorship for Senior International Scientists (2012T1G0021).
文摘In this paper,subnanosecond-pulse and one-nanosecond-pulse generators are used to study the breakdowns in highly overvolted gaps in atmospheric pressure air.With different cathodes,we measured the applied voltage and discharge current to investigate the dynamic characteristics in the subnanosecond breakdown during the generation of a supershort avalanche electron beam.Especially,characteristics of dynamic displacement current are presented in the current paper,which is detected between the ionization wave front and a plane anode.It is shown that during a subnanosecond voltage rise time,the amplitude of the dynamic displacement current can be higher than 4 kA.It is demonstrated that the breakdown in the air gap is assisted by ionization processes between the ionization wave front and a plane anode.
基金Project(52175445) supported by the National Natural Science Foundation of ChinaProject(ZZYJKT2020-09) supported by the State Key Laboratory of High Performance Complex Manufacturing (Central South University),China+1 种基金Projects(2020JJ4247, 2022JJ30743) supported by the Natural Foundation of Hunan Province,ChinaProject(1053320190337) supported by the Fundamental Research Funds for the Central University,China。
文摘Electron beam lithography(EBL) is a key technology in the fabrication of nanoscale silicon optical waveguide. The influence of exposure dose, the main process parameter of EBL, on the structure profile of poly-methyl methacrylate(PMMA) after development was studied using a silicon on insulator(SOI) wafer with 220 nm top silicon as the substrate. The relationship between exposure dose and structure pattern width after development was analyzed according to the measurement results. The optimum exposure dose of 220 μC/cm^(2) was found to obtain a final structure consistent with the designed mask value through subsequent processes. At the same time, according to the image segmentation curve tracking technology, the contour extraction process of the dose test results was carried out, and the relationship among mask design value, exposure dose and two-dimensional roughness of boundary contour was analyzed, which can provide reference for the subsequent electron beam lithography of the same substrate material.
基金Projects supported by The 2nd Stage of Brain Korea and Korea Research Foundation
文摘The high-temperature oxidation resistance behavior of 7% (mass fraction) Y203-ZrO2 thermal barrier coatings (TBCs) irradiated by high-intensity pulsed ion beam (HIPIB) was investigated under the cyclic oxidation condition of 1 050 ℃ and 1 h. The columnar grains in the TBCs disappear after the HIPIB irradiation at ion current densities of 100-200 A/cm^2 and the irradiated surface becomes smooth and densified after remelting and ablation due to the HIPIB irradiation. The thermally grown oxide (TGO) layer thickness of the irradiated TBCs is smaller than that of the original TBCs. After 15 cycles, the mass gains of the original TBCs and those irradiated by ion current densities of 100 and 200 A/cm^2 due to the oxidation are found to be 0.8-0.9, 0.6-0.7, and 0.3-0.4 mg/cm^2, respectively. The inward diffusion of oxygen through the irradiated TBCs is significantly impeded by the densified top layer formed due to irradiation, which is the main reason for the improved overall oxidation resistance of the irradiated TBCs.
文摘High nitrogen stainless steel(HNS) is a nickel free austenitic stainless steel that is used as a structural component in defence applications for manufacturing battle tanks as a replacement of the existing armour grade steel owing to its low cost, excellent mechanical properties and better corrosion resistance.Conventional fusion welding causes problems like nitrogen desorption, solidification cracking in weld zone, liquation cracking in heat affected zone, nitrogen induced porosity and poor mechanical properties.The above problems can be overcome by proper selection and procedure of joining process. In the present work, an attempt has been made to correlate the microstructural changes with mechanical properties of fusion and solid state welds of high nitrogen steel. Shielded metal arc welding(SMAW), gas tungsten arc welding(GTAW), electron beam welding(EBW) and friction stir welding(FSW) processes were used in the present work. Optical microscopy, scanning electron microscopy and electron backscatter diffraction were used to characterize microstructural changes. Hardness, tensile and bend tests were performed to evaluate the mechanical properties of welds. The results of the present investigation established that fully austenitic dendritic structure was found in welds of SMAW. Reverted austenite pools in the martensite matrix in weld zone and unmixed zones near the fusion boundary were observed in GTA welds. Discontinuous ferrite network in austenite matrix was observed in electron beam welds.Fine recrystallized austenite grain structure was observed in the nugget zone of friction stir welds.Improved mechanical properties are obtained in friction stir welds when compared to fusion welds. This is attributed to the refined microstructure consisting of equiaxed and homogenous austenite grains.
基金Supported by the National High Technology Development Program of China(Grant No.2003AA32720)Shanghai Nanotechnology Promotion Center(0352nm016, 0359nm204,0252nm084)+2 种基金Science and Technology Council of Shanghai(03dz11009)Fore-research of basic research project(2001CCA02800)the special Foundation for State Major Basic Research Programmeof China(Grant No.001CB610408)
文摘The one-dimensional photonic crystals of Ag/SiO_(2) system are studied to investigate the photonic band gaps (PBG). The samples were prepared by the ultra-high vacuum electron beam evaporation. The clear band gaps were observed. Satisfactory agreement between experimental and calculated results was obtained without fitting. The thickness of SiO_(2 )film has influence on the photonic band gap, as well as it awfully affects the transmittance of Ag. More layers can get clearer PBG.
基金Project(50304007) supported by the National Natural Science Foundation of China
文摘Based on the basic operating principal and the technology characteristic of electron beam physical vapor deposition(EBPVD) technique, EBPVD was used to prepare the micro-layer composites. The effect on the substrate preheating temperature was taken into accounts and the finite element analysis package ANSYS was used to simulate the internal stress field and the potential displacement changing tendency. The results show that one of the most important quality factors on the judgment of micro-layer composites is the adhesion between the substrate and the deposition layers as well as among the different deposition layers. Besides the existance of temperature gradient through the thickness of layers, the main reason for the internal stress in micro-layer composites is the mismatch of various properties of the layer and the substrate of different thermal expansions and crystal lattice types. With the increase of substrate preheating temperature, the inter-laminar shear stress also takes on a tendency of increase but the axial residual stress decrease.