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Choice of reference surfaces for machined surface roughness in milling of SiC_p/Al composites 被引量:4
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作者 王阳俊 黄海波 +1 位作者 陈立国 孙立宁 《Journal of Central South University》 SCIE EI CAS 2014年第11期4150-4156,共7页
In order to choose the appropriate reference surface on the machined surface roughness of Si Cp/Al composites, the cutting experiments of Si Cp/Al composites were carried out, and the machined surface topography was m... In order to choose the appropriate reference surface on the machined surface roughness of Si Cp/Al composites, the cutting experiments of Si Cp/Al composites were carried out, and the machined surface topography was measured by OLS3000 Confocal laser scanning microscope. The 3D measured data of machined surface topography were analyzed by the area power spectrum density. The result shows that the texture of machined surface topography in milling of Si Cp/Al composites is almost isotropic. This is the reason that the values of Rq at different locations on the same machined surface are obviously different. Through the comparison of performance of different filtering methods, the robust least squares reference surface can be used to extract the surface roughness of SiC p/Al composites effectively. 展开更多
关键词 SiCp/al composites surface topography milling filtering method power spectrum density
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Wear mechanism for spray deposited Al-Si/SiC_p composites under dry sliding condition 被引量:6
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作者 滕杰 李华培 陈刚 《Journal of Central South University》 SCIE EI CAS CSCD 2015年第8期2875-2882,共8页
Al-Si/15%SiCp(volume fraction) composites with different silicon contents were fabricated by spray deposition technique, and typical microstructures of these composites were studied by optical microscopy(OM). Dry slid... Al-Si/15%SiCp(volume fraction) composites with different silicon contents were fabricated by spray deposition technique, and typical microstructures of these composites were studied by optical microscopy(OM). Dry sliding wear tests were carried out using a block-on-ring wear machine to investigate the effect of applied load range of 10-220 N on the wear and friction behavior of these composites sliding against SAE 52100 grade bearing steel. Scanning electron microscopy(SEM) and energy-dispersive X-ray microanalysis(EDAX) were utilized to examine the morphologies of the worn surfaces in order to observe the wear characteristics and investigate the wear mechanism. The results show that the wear behavior of these composites is dependent on the silicon content in the matrix alloy and the applied load. Al-Si/15%SiCp composites with higher silicon content exhibit better wear resistance in the applied load range. Under lower loads, the major wear mechanisms are oxidation wear and abrasive wear for all tested composites. Under higher loads, severe adhesive wear becomes the main wear mechanisms for Al-7Si/15%SiCp and Al-13Si/15%SiCp composites, while Al-20Si/15%SiCp presents a compound wear mechanism, consisting of oxidation, abrasive wear and adhesion wear. 展开更多
关键词 dry sliding wear wear mechanism al-Si/SiC_p composites spray deposition
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Research on the Characters of the Cutting Force in Vibration Cutting Particle Reinforced Metal Matrix Composites SiC_p/Al 被引量:3
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作者 LIU Chuan-shao 1, ZHAO Bo 1,2, GAO Guo-fu 1, JIAO F eng 1 (1. Department of Mechanical Engineering, Jiaozuo Institute of Techno logy, Henan 454000, China 2. Institute of Mechanical Engineering, Shanghai Jiaotong University, Shanghai 200030, China) 《厦门大学学报(自然科学版)》 CAS CSCD 北大核心 2002年第S1期74-75,共2页
In this paper, turning experiments of machining particle reinforced metal matri x composites(PRMMCs) SiC p/Al with PCD tools have been carried out. The cutting force characteristics in ultrasonic vibration turning com... In this paper, turning experiments of machining particle reinforced metal matri x composites(PRMMCs) SiC p/Al with PCD tools have been carried out. The cutting force characteristics in ultrasonic vibration turning compared with that in com mon turning were studied. Through the single factor experiments and multiple fac tor orthogonal experiments, the influences of three kinds of cutting conditions such as cutting velocity, amount of feed and cutting depth on cutting force were analyzed in detail. Meanwhile, according to the experimental data, the empirica l formula of main cutting force in ultrasonic vibration turning was conclude d. According to the test results, the cutting force is direct proportion to cutt ing depth basically according to the relation between cutting force and other fa ctors, which is similar to that of common cutting, so is the feed rate, but the influence is not so big. The influence of cutting speed is larger than that of f eed rate on cutting force because the efficient cutting time increases in vibrat ion cycle with the increase of cutting speed, which causes cutting force to incr ease. The research results indicate: (1) Ultrasonic vibration turning possesses much lower main cutting force than that in common turning when adopting smaller cutting parameters. If using larger cutting parameters, the difference will inco nspicuous. (2) There are remarkable differences of cutting force-cutting veloci ty characteristics in ultrasonic vibration turning from that in common turning m ainly because built-up edge does not emerge in ultrasonic turning unlike common turning in corresponding velocity range. (3) In ultrasonic vibration cutting, t he influence of cutting velocity on cutting force is most obvious among thre e cutting parameters and the influence of feed is smallest. So adopting lower cu tting velocity and larger cutting depth not only can reduce cutting force effect ively but also can ensure cutting efficiency. (4) The conclusions are useful in precision and super precision manufacturing thin-wall pieces. 展开更多
关键词 composite SiC p/al PCD tool ultrasonic vibrati on turning cutting force
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Research on the Surface Micro-configuration in Vibration Cutting Particle Reinforced Metallic Matrix Composites SiC_p/Al
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作者 ZHAO Bo 1,2, LIU Chuan-shao 2, ZHU Xun-sheng 1, XU Ke-wei 1 (1. Institute of Mechanical Engineering, Shanghai Jiaotong U niversity, Shanghai 200030, China 2. Department of Mechanical Engineering, Jiaozuo Institute of Technology, Hena n 454000, China) 《厦门大学学报(自然科学版)》 CAS CSCD 北大核心 2002年第S1期71-72,共2页
The cutting performance of particulate reinforced me tallic matrix composites(PRMMCs) SiC p/Al in ultrasonic vibration cutting and c ommon cutting with carbide tools and PCD tools was researched in the paper. Mic rost... The cutting performance of particulate reinforced me tallic matrix composites(PRMMCs) SiC p/Al in ultrasonic vibration cutting and c ommon cutting with carbide tools and PCD tools was researched in the paper. Mic rostructure of machined surface was described, the relation between cutting para meters and surface roughness was presented, and characteristic of the surface re mained stress was also presented. Furthermore, wear regularity and abrasion resi stance ability of tools in ultrasonic vibration cutting and common cutting o f PRMMCs were discussed in detail. The test results show: (1) The surface config urations are obviously different when using different tools to machine such PRMM Cs. The surface machined with carbide tools looks luminous and orderly and there are seldom surface defects on it. The reason is that the soft basal body is apt to flow during cutting, therefore a layer of Al matrix film covers machined sur face. On the contrary, the surface machined with PCD tools looks lackluster. But the profile of machined surface is very clear. Superfine grooves, pits and blac k reinforce particulates can be seen easily without obvious Al film. (2) Because of unstable cutting process in common cutting, the surface is easy to produce s ome defects such as burrs, built-up edges and so on so that the quality of surf ace becomes very poor. Vibration cutting can reduce the influence of tearing, pl astic deformation and built-up edge in cutting and can restrain flutter so as t o make cutting process more stable. Therefore, surface roughness of vibration cu tting is better than that of common cutting. (3) There is an optimum value of fe ed rate in vibration cutting of PRMMCs due to the influence of material characte ristics. Whether feed rate is more than or less than this optimum value, surface roughness will increase. (4) According to analyzing the wear rate of tools in v ibration cutting PRMMCs, it can be concluded that abrasion resistance of tools w ill be improved remarkably when vibration cutting composites have a lower pe rcentage of reinforce particulate. If the percentage of reinforce particulate is higher, the influence on abrasion resistance of carbide tool in vibration cut ting will not be obvious. The research result indicates that vibration cutting effect has a close relation with material characteristics. 展开更多
关键词 PCD tools composite SiC p/al surface micro-c onfiguration tool wear
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Rolling of Al-SiC_p Composites
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作者 Rajesh Purohit Anil Kumar Das Rakesh Sagar 《厦门大学学报(自然科学版)》 CAS CSCD 北大核心 2002年第S1期103-105,共3页
Aluminum based metal matrix composites are offering o utstanding properties in a number of automotive and aircraft components and body structures. The major advantages of these composite materials are their high st re... Aluminum based metal matrix composites are offering o utstanding properties in a number of automotive and aircraft components and body structures. The major advantages of these composite materials are their high st rength to weight ratio, high stiffness, high hardness, wear resistance, low coef ficient of thermal expansion, superior dimensional stability and versatility to designer. In addition to these their isotropic properties, good forming characte ristics, easy availability of cheaper reinforcements along with the availability of comparatively low cost, high volume production methods have made them a prom ising material for future growth. Weight reduction is a major goal of automotive innovations. Lighter vehicles/ ai rcraft means less fuel consumption, reduced emissions, and improved performance. Components made from highly loaded aluminium matrix composites are attractive r elative to iron based materials because of their low density, high stiffness (eq uivalent to nodular iron) and better heat transfer characteristics. The basic co st of materials is higher with these advanced composites; however, manufacturing the part to near net shape may offset basic material costs. A good aluminium based material design can improves safety. The aluminium-based composites can give cars better acceleration and braking, improved handling, ex cellent durability, and ease of repair. Tha aluminum-based composite performs a s well or better in crash than conventional steel-structured cars because of th eir larger volume, which can absorb more crash energy. Another excellent advanta ge of Al-SiC p composite in auto design is better stability and response, and reduced noise, vibration/harshness (NHV). These advantages stem from reduced veh icle weight combined with high structural stiffness and also lead to improved st ability and turning response. In the present work Al-SiC p composite plates of 10 to 12 mm thickness w ere cast using sand casting as well as die casting process. The plates were furt her machined to 3 to 4 mm thicknesses. The machined plates were subjected to col d as well hot rolling. The cold rolling of Al-3 wt.% SiC composite plates was done on 2 high experimental cold rolling mill at Indian Oil Corporation Ltd., R esearch and Development centre, Faridabad. For hot rolling, the Al-5 weight % SiC p composite plates were heat treated at 500 ℃ temperature and Al-15 weight % SiC p composite plates were heat treate d at 550 ℃ temperature for 20 minutes. The plates were hot rolled on 2 high ro lling mill of one ton capacity at IIT Delhi. The maximum percentage reduction ob tained after hot rolling of Al-5 weight % SiC p composite and Al- 15 weight % SiC p composite plates for 10 passes was 11 % and 6 % respectively. During col d rolling of Al-SiC p composites cracks (particle fracture) were observed due to the low ductility of Al-SiC p composties at room temperature. The various m echanical properties such as tensile strength, hardness and wear resistance were measured for the rolled and un-rolled Al-SiC p composite plates. The tensile strength of un-rolled and rolled Al-5wt.% SiC p composites are shown in Tab. 1. Table shows that the tensile strength decreases after rolling. This may be du e to the damage of the bonding between aluminum and silicon carbide particulates . The Rockwell hardness values of Al-5 wt.% SiC p composites measured before a nd after hot rolling are shown in Tab.2. The hardness was found to decrease afte r hot rolling, which may be due to the annealing of composites during heating. T he Rockwell hardness values of Al-3 wt.% SiC p composites before and after cold rolling are shown in Tab.3. The Table shows that the Rockwell hardness of Al-SiC p compostes increases after cold rolling due to the workhardening effec t. The wear resistance of rolled and un-rolled Al-SiC p composites were teste d on reciprocating ball on flat wear testing machine. The wear resistance of Al -SiC p composites decreases after hot rolling due to decrease in hardness 展开更多
关键词 SIC Rolling of al-SiC_p composites al
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TiC-TiB_(2)/Al-xSi-4.5Cu复合材料的制备与性能
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作者 梁艳峰 刘逍恂 +1 位作者 夏峰 郭巧琴 《热加工工艺》 北大核心 2025年第9期92-97,共6页
根据TiB_(2)与TiC原位粒子的形成温区,设计粒子的原位反应路径,在铸造Al-xSi-4.5Cu(x=7,2,18,wt%)合金熔体内成功制备TiB_(2)与TiC双相粒子。借助OM、SEM、EDS等方法观察所制备的复合材料微观组织,并测试其维氏硬度,探究基体合金中Si含... 根据TiB_(2)与TiC原位粒子的形成温区,设计粒子的原位反应路径,在铸造Al-xSi-4.5Cu(x=7,2,18,wt%)合金熔体内成功制备TiB_(2)与TiC双相粒子。借助OM、SEM、EDS等方法观察所制备的复合材料微观组织,并测试其维氏硬度,探究基体合金中Si含量对原位TiB_(2)与TiC粒子分布及复合材料硬度的影响。结果表明:3种Si含量的复合材料均可以通过原位自生法获得微纳米尺度的TiB_(2)与TiC双相粒子,但随着Si含量增加,原位粒子在Si相附近团聚加剧;当Si含量为12wt%时,复合材料硬度达到极值,为173.56 HV;当Si含量增加到18wt%时,TiC粒子发生失稳分解,导致了复合材料硬度下降。 展开更多
关键词 al-SI-CU合金 al基复合材料 TIC TiB_(2) 原位自生法
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Al/Ni-WC复合涂层高温抗氧化性能与扩散分析
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作者 李德元 孙继博 +2 位作者 李光全 张楠楠 祝成 《沈阳工业大学学报》 北大核心 2025年第2期197-204,共8页
【目的】碳钢因其较差的抗氧化性能,在高温工况下的使用受到了严格限制。Ni-Al金属间化合物由于具有较高的熔点和较好的高温抗氧化性能,在实际工业领域应用众多。针对含有Ni-Al金属间化合物的涂层,研究其高温抗氧化涂层的进一步应用,提... 【目的】碳钢因其较差的抗氧化性能,在高温工况下的使用受到了严格限制。Ni-Al金属间化合物由于具有较高的熔点和较好的高温抗氧化性能,在实际工业领域应用众多。针对含有Ni-Al金属间化合物的涂层,研究其高温抗氧化涂层的进一步应用,提高碳钢的高温使用寿命,拟在碳钢表面制备Ni-Al反应改性涂层。【方法】采用超音速火焰喷涂在碳钢基体上制备Ni-WC涂层,随后在其上利用电弧喷涂制备Al涂层,在800℃不同时间扩散处理下使得涂层内的Ni-Al发生反应,以得到金属间化合物并增强其高温抗氧化性能。通过记录氧化增重曲线测试涂层的高温抗氧化性能。【结果】在高温氧化过程中Al/Ni-WC复合涂层在Al/Ni界面处原位生成了富铝的Ni-Al金属间化合物。Al/Ni-WC涂层经800℃扩散处理过程中,首先形成富Al的NiAl 3,且其表面Al原子与大气中的氧原子反应形成了Al_(2)O_(3)。随着反应时间的延长,在Al/Ni界面形成的NiAl 3相转变为抗高温氧化能力更优异的Ni_(2)Al_(3)相,两种Ni-Al金属间化合物本身具有高熔点和高温抗氧化性能,且在Al/Ni-WC复合涂层表面形成的Al_(2)O_(3)减缓了氧原子的扩散过程。Al/Ni-WC复合涂层试件的扩散层厚度随着扩散处理时间的延长呈现类似线性增长趋势。经800℃扩散处理后,Al/Ni-WC涂层中NiAl 3层的增厚速率较快,且在加热10 h后原位反应生成了更厚的Ni_(2)Al_(3)层。经800℃扩散处理20 h后,经过原位反应得到了比NiAl 3层稍厚一些的Ni_(2)Al_(3)层。由于Ni_(2)Al_(3)层熔点更高且更稳定,因而经过800℃扩散处理后的Al/Ni-WC涂层具有更好的高温抗氧化能力。经900℃/50 h扩散处理后的Al/Ni-WC涂层经循环氧化后存在陶瓷相Al_(2)O_(3)、WC和NiAl相,在陶瓷相和NiAl相的共同作用下呈现较好的高温抗氧化性能。测得不同扩散时间下Al/Ni-WC涂层的扩散层厚度,得到了Ni和Al之间的扩散关系式,其扩散反应动力指数为0.79045,复合涂层对碳钢基体的保护作用明显提高。【结论】在氧化过程中形成的Ni-Al金属间化合物、Al_(2)O_(3)膜与涂层中原有WC相的共同作用下碳钢基体的高温抗氧化性能得到了明显提升。通过氧化增重实验可知,在Ni层中增加陶瓷相以后,金属-陶瓷复合涂层的高温抗氧化能力明显优于碳钢基体,因而对碳钢基体的保护效果更好。 展开更多
关键词 电弧喷涂 超音速火焰喷涂 碳钢 原位生成 al/Ni-WC复合涂层 al/Ni界面 高温抗氧化性能 Ni-al金属间化合物
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脉冲激光-超声复合辅助车削SiCp/Al的切屑形成演变过程分析
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作者 林洁琼 解略 +2 位作者 于行 谷岩 周晓勤 《表面技术》 北大核心 2025年第8期167-179,共13页
目的 SiCp/Al复合材料与传统的金属材料相比具有高硬度、高抗弯强度以及热膨胀系数低等优异的物理性能,但其加工过程困难。旨在揭示脉冲激光-超声复合辅助车削SiCp/Al复合材料的切屑形成机理。方法 建立理论模型来确定最小未变形切屑厚... 目的 SiCp/Al复合材料与传统的金属材料相比具有高硬度、高抗弯强度以及热膨胀系数低等优异的物理性能,但其加工过程困难。旨在揭示脉冲激光-超声复合辅助车削SiCp/Al复合材料的切屑形成机理。方法 建立理论模型来确定最小未变形切屑厚度,进而揭示脉冲激光-超声复合辅助车削SiCp/Al切屑形成的临界条件。并比较常规车削、脉冲激光辅助车削和脉冲激光-超声复合辅助车削的切屑形态,探究脉冲激光功率对切屑形成机理的影响。结果 研究表明,当脉冲激光作用于材料表面时,会产生热软化效应。这种效应使材料更易去除,并减少了切屑自由表面颗粒的破损程度。此外,在超声振动的辅助下,切屑连续性得到进一步改善。通过对加工后工件表面形貌测试发现,脉冲激光-超声复合辅助加工的表面粗糙度最小,为0.388μm,与常规加工相比降低了70.8%;脉冲激光-超声复合辅助加工的亚表面变形层厚度最小,为37.28μm。结论 通过深入分析复合车削切屑的形成及其对表面质量的影响,为优化SiCp/Al复合材料的表面质量提供了有力的理论支撑和实用的加工方法。 展开更多
关键词 脉冲激光-超声复合辅助车削 SICP/al 切屑形成机理 表面质量
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SiC_(p)/Al复合材料高效低损伤加工技术研究进展
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作者 赵重阳 韩基山 +2 位作者 王毅 赵波 唐进元 《工具技术》 北大核心 2025年第3期1-19,共19页
铝基碳化硅(SiC_(p)/Al)复合材料在实际加工中存在加工效率低、刀具磨损严重和表面完整性差等问题,上述问题限制着SiC_(p)/Al在工程领域的应用。为实现SiC_(p)/Al的高效低损伤加工,本文从工艺参数的选择、界面冷却润滑、刀具选用及优化... 铝基碳化硅(SiC_(p)/Al)复合材料在实际加工中存在加工效率低、刀具磨损严重和表面完整性差等问题,上述问题限制着SiC_(p)/Al在工程领域的应用。为实现SiC_(p)/Al的高效低损伤加工,本文从工艺参数的选择、界面冷却润滑、刀具选用及优化的角度出发,总结了传统机械加工的研究现状。从激光加工、电火花加工、超声辅助加工、磨料水射流加工、激光加热辅助加工以及电化学射流加工的研究现状出发,详述了各种加工方法的特点以及现阶段存在的突出问题。并从切削力、刀具磨损、材料去除形式、表面和亚表面损伤方面出发,论述了加工参数对表面完整性的影响规律。在总结现有加工方法研究现状的基础上,指出了多能场复合加工是改善SiC_(p)/Al切削性能、降低刀具磨损及表面损伤、提高加工精度和表面完整性的有效途径,也是未来的发展趋势。 展开更多
关键词 SiC_(p)/al复合材料 表面完整性 材料去除形式 刀具磨损 多能场复合加工
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Al纳米颗粒掺杂对Sn基复合焊点组织与性能影响的研究
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作者 孙磊 王静 +2 位作者 王文昊 姜加伟 张亮 《热加工工艺》 北大核心 2025年第15期182-186,共5页
研究了微量Al纳米颗粒(0~0.5wt%)掺杂对三维封装技术中芯片堆叠互连Sn基焊点的界面组织、润湿性能以及剪切强度的影响。结果表明,掺杂微量的Al纳米颗粒可以显著抑制Sn基复合焊点界面层金属间化合物的生长。当Al颗粒掺杂量为0.3wt%时,Sn... 研究了微量Al纳米颗粒(0~0.5wt%)掺杂对三维封装技术中芯片堆叠互连Sn基焊点的界面组织、润湿性能以及剪切强度的影响。结果表明,掺杂微量的Al纳米颗粒可以显著抑制Sn基复合焊点界面层金属间化合物的生长。当Al颗粒掺杂量为0.3wt%时,Sn/Cu焊点界面层厚度由最初始的3.00μm下降到2.28μm。当Al纳米颗粒掺杂量超过0.3wt%时,复合焊点界面层厚度却出现增厚的趋势。此外,随着微量Al颗粒的掺杂,钎料的熔点未出现明显变化,Sn基钎料的润湿角得到降低。当Al纳米颗粒的掺杂量为0.3wt%时,Sn基钎料的润湿角由未掺杂的16.8°下降到13.4°,降幅20.2%。Sn-0.3Al复合焊点的剪切性能则达到了最大值16.9 MPa,增幅24.3%。继续增加Al纳米颗粒掺杂量,复合焊点的润湿性能和剪切强度逐渐下降。 展开更多
关键词 Sn基复合焊点 al纳米颗粒 界面组织 润湿角 剪切强度
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退火温度对依据LSDR原理轧制的Mg/Al层合板界面结构的影响
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作者 冯光 郜豪杰 +1 位作者 刘洪涛 于百灵 《热加工工艺》 北大核心 2025年第12期34-38,共5页
基于点阵强变形轧制(lattice severe deformation rolling,LSDR)原理制备了Mg/Al层合板,研究了200~400℃退火温度下界面扩散层厚度、成分以及形态特征,并进行了拉伸试验。结果表明:随退火温度升高,扩散层厚度逐渐增大。当退火温度为300... 基于点阵强变形轧制(lattice severe deformation rolling,LSDR)原理制备了Mg/Al层合板,研究了200~400℃退火温度下界面扩散层厚度、成分以及形态特征,并进行了拉伸试验。结果表明:随退火温度升高,扩散层厚度逐渐增大。当退火温度为300℃时,界面由明显的两层组成,靠近镁合金一侧为Mg_(17)Al_(12)相,靠近铝合金一侧为Mg_(2)Al_(3)相,且随温度升高,Mg_(2)Al_(3)相比Mg_(17)Al_(12)相生长速度快;界面沿轧向(rolling direction,RD)和横向(transverse direction,TD)均连续分布。Mg/Al层合板沿RD和TD的抗拉强度以及伸长率随退火温度升高均呈先增大后减小规律,300℃退火时获得最优的力学性能,沿RD和TD抗拉强度最大值分别为242 MPa和247 MPa,同时伸长率超过14%,相较未经退火的板材有显著提高。研究结果为探究LSDR原理制备高质量Mg/Al层合板提供了试验参考。 展开更多
关键词 LSDR Mg/al层合板 退火温度 界面 扩散层
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温度对Al-Sn-Bi-Pb复合粉末水反应特性的影响
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作者 周星 闫超宇 +1 位作者 陈珊姗 黄蕾 《固体火箭技术》 北大核心 2025年第3期390-396,共7页
铝(Al)粉表面存在的惰性氧化膜,极大降低了Al/H2O反应速率,限制了其在高活性金属燃料中的应用。为提高Al/H2O反应速率和反应效率,采用低熔点元素(Sn、Bi、Pb)对Al进行活化并制备了Al-Sn-Bi-Pb复合粉末,利用水反应测试装置研究了温度(25... 铝(Al)粉表面存在的惰性氧化膜,极大降低了Al/H2O反应速率,限制了其在高活性金属燃料中的应用。为提高Al/H2O反应速率和反应效率,采用低熔点元素(Sn、Bi、Pb)对Al进行活化并制备了Al-Sn-Bi-Pb复合粉末,利用水反应测试装置研究了温度(25~70℃)对Al-Sn-Bi-Pb复合粉末水反应特性的影响,并利用XRD和SEM对水反应产物物相组成和微观组织结构进行了分析。结果表明,Sn、Bi、Pb的加入提高了复合粉末的密度,促进了Al粉的燃烧,提高了Al粉的燃烧效率。随着温度升高,平均反应速率加快,在70℃时最高可达4 936 mL·g^(-1)·min^(-1);25℃时,Al-Sn-Bi-Pb复合粉末燃烧产物主要为蜂巢状花瓣结构的AlOOH和短棒状结构的Al(OH)_(3),70℃时则主要为蜂巢状花瓣结构AlOOH。蜂巢花瓣状结构的形成与H2的形成有直接关系,同时这些孔洞的存在又为水分子的进入提供了通道,促进了反应的发生。 展开更多
关键词 al-Sn-Bi-Pb复合粉末 水反应特性 微观结构 温度
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中高体积分数SiC_p/Al复合材料的力学性能及强化机制 被引量:2
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作者 崔岩 廖家杰 +1 位作者 曹雷刚 杨越 《材料工程》 EI CAS CSCD 北大核心 2024年第4期110-119,共10页
采用热等静压粉末冶金工艺,以2024和6061铝合金为基体,分别制备体积分数为35%,45%,55%的中高体积分数SiC_(p)/Al复合材料。探究基体合金与SiC体积分数对复合材料力学性能的影响。结果表明:相同体积分数时,以2024铝合金为基体的复合材料... 采用热等静压粉末冶金工艺,以2024和6061铝合金为基体,分别制备体积分数为35%,45%,55%的中高体积分数SiC_(p)/Al复合材料。探究基体合金与SiC体积分数对复合材料力学性能的影响。结果表明:相同体积分数时,以2024铝合金为基体的复合材料具有更高的弯曲强度和弹性模量;但以6061铝合金为基体的复合材料则呈现出了更高的断裂应变。随着体积分数的增加,两类复合材料力学性能的变化规律相同,弯曲强度呈先增大后减小的趋势,当体积分数为45%时达到峰值,分别为656.54 MPa和548.00 MPa;弹性模量呈持续上升趋势,当体积分数为55%时分别达到202 GPa和188 GPa。基体合金差异对力学性能的影响在体积分数较低时更为明显,提高体积分数将会弱化这种差异。结合理论公式计算发现,对于微米级的增强体颗粒,Orowan机制带来的强化效应极小,可忽略不计;其他各类强化机制的强化效果将随着增强体体积分数的增加呈现不同程度的提高;几何必须位错强化和热错配强化对材料屈服强度的贡献始终占据主导地位。 展开更多
关键词 SIC_P/al复合材料 体积分数 力学性能 强化机制
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Reactive Processing and Mechanical Properties of Al/SiC_P Composite 被引量:4
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作者 CHEN Kang-hua GE Jian-guo +1 位作者 LIU Hong-wei LIU Yun-zhong 《Journal of Central South University》 SCIE EI CAS 2000年第1期1-3,共3页
The reactive process for Al/SiC P composite was studied. SiC particles were in situ coated by the exothermal reaction of SiC Ti powder compact in Al melt bath, and easily incorporated into Al melt. The detailed study ... The reactive process for Al/SiC P composite was studied. SiC particles were in situ coated by the exothermal reaction of SiC Ti powder compact in Al melt bath, and easily incorporated into Al melt. The detailed study was carried out to understand the microstructures of the reacted SiC particles. During the reaction and consequent mixing, the successive processes include in situ coating on the reacted SiC particles, coat dissolution and SiC P splitting. The tensile mechanical properties of 6013Al/SiC P composite processed by the present technology showed that the reacted SiC P considerably reinforced the 6013 matrix. 展开更多
关键词 al/SiC_P compositE REACTIVE processing in SITU coating MECHANICal properties
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基于NaGdF_(4)∶Er^(3+)/Yb^(3+)/Al^(3+)的复合薄膜上转换发光与光热性能 被引量:2
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作者 邵泽杰 周海芳 +1 位作者 郑瑞锦 程树英 《发光学报》 北大核心 2025年第1期89-97,共9页
稀土掺杂的上转换纳米材料在光热传感、生物医学等领域有着广泛的应用前景,但其存在导热性差、测温灵敏度与上转换发光(UCL)强度低的问题,而添加单壁碳纳米管(SWCNT)、贵金属与光子晶体(PCs)是提高其UCL强度与光热性能的有效手段。本文... 稀土掺杂的上转换纳米材料在光热传感、生物医学等领域有着广泛的应用前景,但其存在导热性差、测温灵敏度与上转换发光(UCL)强度低的问题,而添加单壁碳纳米管(SWCNT)、贵金属与光子晶体(PCs)是提高其UCL强度与光热性能的有效手段。本文使用溶剂热法合成了NaGdF_(4)∶Er^(3+)/Yb^(3+)/Al^(3+)纳米晶体(UCNPs),通过对比上转换层(UC)、SWCNT/UC、Ag/SWCNT/UC与PCs/Ag/SWCNT/UC的光热性能,研究不同膜层对UCNPs的光热性能影响。结果表明,PCs/Ag/SWCNT/UC具有优异的性能,其红绿光强度分别为UC的3.48倍与4.24倍,其光热转换效率达到33.79%,是UC的1.49倍;并且光学测温绝对灵敏度SA在353 K时达到3.14×10^(-3) K^(-1),相对灵敏度SR在273 K时达到1.87×10^(-2) K^(-1)。本研究为提高光热传感器性能提供了一种有效的策略。 展开更多
关键词 复合薄膜 NaGdF_(4)∶Er^(3+)/Yb^(3+)/al^(3+)纳米晶 光热性能 测温灵敏度
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Preparation and characterization of different surface modified SiCp reinforced Al-matrix composites 被引量:11
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作者 LÜ Pin-hui WANG Xiao-feng +2 位作者 DONG Cui-ge PENG Chao-qun WANG Ri-chu 《Journal of Central South University》 SCIE EI CAS CSCD 2020年第9期2567-2577,共11页
The effects of SiCp surface modifications(Cu coating,Ni coating and Ni/Cu coating)on the microstructures and mechanical properties of Al matrix composites were investigated.Surface modification of SiC particles with C... The effects of SiCp surface modifications(Cu coating,Ni coating and Ni/Cu coating)on the microstructures and mechanical properties of Al matrix composites were investigated.Surface modification of SiC particles with Cu,Ni and Cu/Ni,respectively,was carried out by electroless plating method.SiCp/Al composites were prepared by hot pressed sintering followed by hot extrusion.The results show that the surface modification of SiC particles plays an effective role,which is relative to the type of surface coating,and the interfacial bonding become stronger in the following order:untreated SiCp<Ni(Cu)-coated SiCp<Ni/Cu-coated SiCp.The Ni/Cu-coated SiCp/Al composites exhibit the best comprehensive mechanical properties,with ultimate tensile strength(σUTS)and fracture strain(εf)of 389 MPa and 6.3%,respectively.Compared with that of untreated-SiCp/Al composites,theσUTS andεf are enhanced by 19.3%and 57.5%. 展开更多
关键词 SiCp/al composite surface modification electroless plating mechanical properties interfacial bonding
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Effect of hot extrusion on microstructure and tribological behavior of Al_(2)O_(3p) reinforced 7075 aluminum-matrix composites 被引量:4
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作者 LEI Yu-shun YAN Hong +4 位作者 WEI Zhi-fan XIONG Jun-jie ZHANG Peng-xiang WAN Jian-ping WANG Zhi-lu 《Journal of Central South University》 SCIE EI CAS CSCD 2021年第8期2269-2284,共16页
The effects of hot extrusion and addition of Al_(2)O_(3p) on both microstructure and tribological behavior of 7075 composites were investigated via optical microscopy(OM),scanning electron microscopy(SEM),energy dispe... The effects of hot extrusion and addition of Al_(2)O_(3p) on both microstructure and tribological behavior of 7075 composites were investigated via optical microscopy(OM),scanning electron microscopy(SEM),energy dispersive spectrometry(EDS),and transmission electron microscopy(TEM).The experimental consequences reveal that the optimal addition of Al_(2)O_(3p) was 2 wt%.After hot extrusion,the Mg(Zn,Cu,Al)2 phases partially dissolve into the matrix and generate many uniformly distributed aging precipitation particles,the Al_(7)Cu_(2)Fe phases are squeezed and broken,and the Al_(2)O_(3p) become uniform distribution.The microhardness of as-extruded 2 wt%Al_(2)O_(3p)/7075 composites reaches HV 170.34,increased by 41.5%than as-cast composites.The wear rate of as-extruded 2 wt%Al_(2)O_(3p)/7075 composites is further lower than that of as-cast composites under the same condition.SEM-EDS analyses reveal that the reinforced wear resistance of composites can put down to the protective effect of the Al_(2)O_(3p) reinforced transition layer.After hot extrusion,the transition layer becomes stable,which determines the reinforced wear resistance of the as-extruded composites. 展开更多
关键词 7075 alloy al2O3P composites hot extrusion MICROSTRUCTURE tribological behavior
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Mo2BC增强Al基复合材料摩擦学性能研究
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作者 祝林 王帅 +5 位作者 游龙 刘娟 逄显娟 陆焕焕 宋晨飞 张永振 《材料导报》 北大核心 2025年第9期158-163,共6页
采用真空热压烧结制备了不同Mo_(2)BC含量的Al基复合材料,并进一步分析了Mo_(2)BC含量对Al基复合材料摩擦学性能的影响。研究表明:随着Al基体中Mo_(2)BC陶瓷颗粒含量的增加,材料体系的硬度得到了明显的提升,这是因为高硬度的Mo_(2)BC陶... 采用真空热压烧结制备了不同Mo_(2)BC含量的Al基复合材料,并进一步分析了Mo_(2)BC含量对Al基复合材料摩擦学性能的影响。研究表明:随着Al基体中Mo_(2)BC陶瓷颗粒含量的增加,材料体系的硬度得到了明显的提升,这是因为高硬度的Mo_(2)BC陶瓷颗粒在复合材料中能够表现出显著的钉扎效应,使得基体在受力过程中产生的塑性变形能够得到抑制。当Mo_(2)BC陶瓷颗粒的质量分数提高到30%时,复合材料的硬度较纯Al提升了约130%,其硬度值高达72.5HV_(0.2)。此外,随着Mo_(2)BC陶瓷颗粒含量的增加,复合材料的摩擦磨损性能得到了明显的改善。对于纯Al和添加Mo_(2)BC质量分数为10%的Al基复合材料,当其与GCr15轴承钢进行配副时,磨损机制主要表现为二体磨粒磨损和黏着磨损,此时材料基体具有较高的磨损率(1.43×10^(-4)mm^(3)·N^(-1)·m^(-1))和摩擦系数(0.84)。随着添加的Mo_(2)BC陶瓷颗粒质量分数逐渐增加至30%,复合材料的磨损率降低至2.35×10^(-3)mm^(3)·N^(-1)·m^(-1),摩擦系数降至0.56,表现出一定的减摩润滑特性。这是由于Mo_(2)BC的添加能够使材料体系摩擦表面通过摩擦氧化作用生成具有润滑性能的摩擦氧化物层,有效抑制了二体磨粒磨损和黏着磨损,起到了一定的抗磨减摩效应。 展开更多
关键词 铝基复合材料 粉末冶金 摩擦学行为 磨损机制
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Synthesis of nano-to micrometer-sized B_(4)C particle-reinforced aluminum matrix composites via powder metallurgy and subsequent heat treatment 被引量:6
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作者 LIU Rui-feng WANG Wen-xian CHEN Hong-sheng 《Journal of Central South University》 SCIE EI CAS CSCD 2021年第8期2295-2306,共12页
B4C/6061Al composites reinforced with nano-to micrometer-sized B4C particles were fabricated via powder metallurgy route consisting of spark plasma sintering(SPS)and hot extrusion and rolling(HER),followed by T6 treat... B4C/6061Al composites reinforced with nano-to micrometer-sized B4C particles were fabricated via powder metallurgy route consisting of spark plasma sintering(SPS)and hot extrusion and rolling(HER),followed by T6 treatment.The microstructural evolution and mechanical properties were investigated.Results showed that the status of B4C particles changed from a network after SPS to a dispersion distribution after HER.The substructured grains reached 66.5%owing to the pinning effect of nano-sized B4C,and the grain size was refined from 3.12μm to 1.56μm after HER.After T6 treatment,dispersed Mg_(2)Si precipitated phases formed,and the grain size increased to 1.87μm.Fine recrystallized grains around micro-sized B4C were smaller than those in the areas with uniform distribution of nano-sized B4C and Mg_(2)Si.The stress distributions of as-rolled and heated composites were similar,considering that the T6 heat treatment was only effective in eliminating the first internal stress.The Vickers,microhardness,and tensile strength of as-SPSed composites were greatly improved from HV 55.45,0.86 GPa,and 180 MPa to HV 77.51,1.08 GPa,and 310 MPa,respectively.Despite the precipitation strengthening,the corresponding values of as-heated composites decreased to HV 70.82,0.85 GPa,and 230 MPa owing to grain coarsening. 展开更多
关键词 nano-to micrometer-size B_(4)C/6061 al composites T6 heat treatment
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Al含量对TiZrNbMoAl_(x)难熔高熵合金薄膜高温抗氧化的影响 被引量:1
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作者 王林青 蒲春林 +1 位作者 张艳 王军军 《表面技术》 北大核心 2025年第1期53-61,73,共10页
目的探讨Al含量对TiZrNbMoAl_(x)难熔高熵合金(Refractory High-entropy Alloys,RHEAs)薄膜结构和高温抗氧化性能的影响,并讨论TiZrNbMoAl_(x)RHEAs薄膜的氧化机理。方法利用双靶磁控共溅射技术,以90°扇形的Ti、Zr、Nb、Mo靶拼接... 目的探讨Al含量对TiZrNbMoAl_(x)难熔高熵合金(Refractory High-entropy Alloys,RHEAs)薄膜结构和高温抗氧化性能的影响,并讨论TiZrNbMoAl_(x)RHEAs薄膜的氧化机理。方法利用双靶磁控共溅射技术,以90°扇形的Ti、Zr、Nb、Mo靶拼接而成的靶材和Al靶材作为溅射靶材,通过调节Al靶溅射功率,制备不同Al含量(原子数分数0%、14%、18%、24%、28%)的TiZrNbMoAl_(x)RHEAs薄膜,并将这些薄膜置于600℃大气环境中进行氧化试验。采用场发射扫描电子显微镜(FESEM)、能量色散光谱仪(EDS)、X射线衍射仪(XRD)和X射线光电子能谱仪(XPS)等,对氧化前后薄膜的物相组成和微观结构进行分析。对比不同Al含量的TiZrNbMoAl_(x)RHEAs薄膜的抗氧化性能,并分析其氧化机理。结果薄膜的微观结构和高温抗氧化性能与Al含量密切相关。不含Al时,薄膜呈现出(110)择优取向的BCC单相固溶体结构;Al原子数分数为14%~24%时,薄膜表现为无定形相结构;Al含量较高(原子数分数为28%)时,薄膜中出现了AlZr_(3)二次相。在600℃环境退火后,Al氧化生成了Al_(2)O_(3),这有效提升了TiZrNbMoAl_(x)RHEAs薄膜的抗氧化性能。然而,过量的Al含量(原子数分数为28%)会导致应力集中并产生裂纹,降低薄膜的高温抗氧化性能。结论Al含量对TiZrNbMoAl_(x)RHEAs薄膜的高温抗氧化性能具有重要影响,适量的Al含量可改善TiZrNbMoAl_(x)RHEAs薄膜的抗氧化性能。 展开更多
关键词 难熔高熵合金薄膜 高温抗氧化性能 al含量 相组成 微观结构
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