A series of sweeping detonation experiments were conducted to study the grain boundary effects during the primary spallation of high-purity copper cylinder.The free surface velocity profile of the shocked samples was ...A series of sweeping detonation experiments were conducted to study the grain boundary effects during the primary spallation of high-purity copper cylinder.The free surface velocity profile of the shocked samples was measured by Doppler pins systems.The soft-recovered samples were characterized by optical and electron backscatter diffraction microscopy,and the effects of microstructures like grain boundaries,and crystal orientation on spall behavior were investigated.The results indicated that the critical stress of deformation twinning in cylindrical copper increased.The nucleation sites of spallation damage were determined by the joint influence of the grain orientation(Taylor factor)and the angle between grain boundaries and radial impact-stress direction.Voids were prone to nucleating at the grain boundaries perpendicular to the radial impact-stress direction.Nevertheless,the number of voids nucleated at boundaries was relatively different from the results obtained from the plate impact experiment and plate sweeping detonation experiment,which is a result of the curvature that existed in the cylindrical copper and the obliquity of the impact-stress direction during sweeping detonation loading.展开更多
This study examines the effects of friction stir welding(FSW)and post-weld heat treatment(PWHT)on the grain boundary character distribution and corrosion resistance of cross sectional(top and bottom)regions of nickel-...This study examines the effects of friction stir welding(FSW)and post-weld heat treatment(PWHT)on the grain boundary character distribution and corrosion resistance of cross sectional(top and bottom)regions of nickel-and molybdenum-free high-nitrogen austenitic stainless steel(HNASS).FSW at 400 rpm and 30 mm/min resulted in finer grains(4.18μm)and higher coincident site lattice(CSL)boundaries(32.3%)at the top of the stir zone(SZ)due to dynamic recrystallization(DRX).PWHT at 900℃for 1 h led to grain coarsening(12.91μm the bottom SZ)but enhanced CSL boundaries from 24.6%to 30.2%,improving grain boundary stability.PWHT reduced the kernel average misorientation(KAM)by 14.9%in the SZ-top layer and 20.4%in the SZ-bottom layer,accompanied by a 25%decrease in hardness in the SZ-top layer and 26.7%in the SZ-bottom layer,indicating strain recovery and reduced dislocation density.Potentiodynamic polarization tests(PDP)showed a 18%increase in pitting potential and a 76%reduction in corrosion rate after PWHT.The improvement in corrosion resistance is attributed to the increase inΣ3 twin boundaries,which enhance grain boundary stability and reduce susceptibility to localized corrosion.These findings highlight the role of PWHT in refining the microstructure and strengthening corrosion resistance,making HNASS a promising material for demanding applications.展开更多
基金Projects(51871243,51574290)supported by the National Natural Science Foundation of ChinaProject(2019JJ40381)supported by the Natural Science Foundation of Hunan Province,ChinaProject supported by the Guangdong-Hong Kong-Macao Joint Laboratory for Neutron Scattering Science and Technology,China。
文摘A series of sweeping detonation experiments were conducted to study the grain boundary effects during the primary spallation of high-purity copper cylinder.The free surface velocity profile of the shocked samples was measured by Doppler pins systems.The soft-recovered samples were characterized by optical and electron backscatter diffraction microscopy,and the effects of microstructures like grain boundaries,and crystal orientation on spall behavior were investigated.The results indicated that the critical stress of deformation twinning in cylindrical copper increased.The nucleation sites of spallation damage were determined by the joint influence of the grain orientation(Taylor factor)and the angle between grain boundaries and radial impact-stress direction.Voids were prone to nucleating at the grain boundaries perpendicular to the radial impact-stress direction.Nevertheless,the number of voids nucleated at boundaries was relatively different from the results obtained from the plate impact experiment and plate sweeping detonation experiment,which is a result of the curvature that existed in the cylindrical copper and the obliquity of the impact-stress direction during sweeping detonation loading.
文摘This study examines the effects of friction stir welding(FSW)and post-weld heat treatment(PWHT)on the grain boundary character distribution and corrosion resistance of cross sectional(top and bottom)regions of nickel-and molybdenum-free high-nitrogen austenitic stainless steel(HNASS).FSW at 400 rpm and 30 mm/min resulted in finer grains(4.18μm)and higher coincident site lattice(CSL)boundaries(32.3%)at the top of the stir zone(SZ)due to dynamic recrystallization(DRX).PWHT at 900℃for 1 h led to grain coarsening(12.91μm the bottom SZ)but enhanced CSL boundaries from 24.6%to 30.2%,improving grain boundary stability.PWHT reduced the kernel average misorientation(KAM)by 14.9%in the SZ-top layer and 20.4%in the SZ-bottom layer,accompanied by a 25%decrease in hardness in the SZ-top layer and 26.7%in the SZ-bottom layer,indicating strain recovery and reduced dislocation density.Potentiodynamic polarization tests(PDP)showed a 18%increase in pitting potential and a 76%reduction in corrosion rate after PWHT.The improvement in corrosion resistance is attributed to the increase inΣ3 twin boundaries,which enhance grain boundary stability and reduce susceptibility to localized corrosion.These findings highlight the role of PWHT in refining the microstructure and strengthening corrosion resistance,making HNASS a promising material for demanding applications.
