An active set truncated-Newton algorithm (ASTNA) is proposed to solve the large-scale bound constrained sub-problems. The global convergence of the algorithm is obtained and two groups of numerical experiments are mad...An active set truncated-Newton algorithm (ASTNA) is proposed to solve the large-scale bound constrained sub-problems. The global convergence of the algorithm is obtained and two groups of numerical experiments are made for the various large-scale problems of varying size. The comparison results between ASTNA and the subspace limited memory quasi-Newton algorithm and between the modified augmented Lagrange multiplier methods combined with ASTNA and the modified barrier function method show the stability and effectiveness of ASTNA for simultaneous optimization of distillation column.展开更多
Bismuth-doped tin dioxide （BTO） nanometer powders were prepared by the wet chemical method using tin tetrachloride （SnCl4）, bismuth nitrate [Bi（NO3） 3 ] and ammonia as raw materials. Non-bridge hydroxides and ca...Bismuth-doped tin dioxide （BTO） nanometer powders were prepared by the wet chemical method using tin tetrachloride （SnCl4）, bismuth nitrate [Bi（NO3） 3 ] and ammonia as raw materials. Non-bridge hydroxides and capillary force between particles were found to be key factors causing hard aggregation of BTO through analyzing the formation mechanism of hard aggregation. The hard aggregation of BTO was eliminated effectively when the Bi-Sn precursor （BSP） was treated with post processing including dispersing with ultrasonic wave, refluxing and distilling with addition of n-butanol and benzene （DRD） and drying by microwave. Characterized with X-ray diffraction （XRD） and transmission electron microscopy （TEM）, BTO spherical particles with tetragonal phase structure are well crystallized, dispersed easily and the average size was less than 10 nm.展开更多
基金Project (2002CB312200) supported by the National Key Basic Research and Development Program of China Project(03JJY3109) supported by the Natural Science Foundation of Hunan Province
文摘An active set truncated-Newton algorithm (ASTNA) is proposed to solve the large-scale bound constrained sub-problems. The global convergence of the algorithm is obtained and two groups of numerical experiments are made for the various large-scale problems of varying size. The comparison results between ASTNA and the subspace limited memory quasi-Newton algorithm and between the modified augmented Lagrange multiplier methods combined with ASTNA and the modified barrier function method show the stability and effectiveness of ASTNA for simultaneous optimization of distillation column.
文摘Bismuth-doped tin dioxide （BTO） nanometer powders were prepared by the wet chemical method using tin tetrachloride （SnCl4）, bismuth nitrate [Bi（NO3） 3 ] and ammonia as raw materials. Non-bridge hydroxides and capillary force between particles were found to be key factors causing hard aggregation of BTO through analyzing the formation mechanism of hard aggregation. The hard aggregation of BTO was eliminated effectively when the Bi-Sn precursor （BSP） was treated with post processing including dispersing with ultrasonic wave, refluxing and distilling with addition of n-butanol and benzene （DRD） and drying by microwave. Characterized with X-ray diffraction （XRD） and transmission electron microscopy （TEM）, BTO spherical particles with tetragonal phase structure are well crystallized, dispersed easily and the average size was less than 10 nm.
