The unique structural and physical properties of boron carbide, which make it suitable for a wide range of applications,demands the development of low-cost and green synthesis method. In the present work, the commonly...The unique structural and physical properties of boron carbide, which make it suitable for a wide range of applications,demands the development of low-cost and green synthesis method. In the present work, the commonly available leaves of aloe vera are hydrothermally treated to form the carbon precursor for the synthesis of boron carbide. The morphological characterization reveals the porous nature of the precursor turning into a tubular structure upon boron carbide formation.The structural characterization by x-ray diffraction and other spectroscopic techniques such as Fourier transform infrared,Raman, photoluminescence and uv-visible near-infrared spectroscopy confirm the formation of boron carbide. The thermogravimetric analysis of the sample is found to exhibit good thermal stability above 500 °C. When the sample is annealed to 600 °C, boron carbide with phase purity is obtained, which is confirmed through XRD and FTIR analyses. The optical emission properties of the sample are studied through CIE plot and power spectrum. Compared with other natural precursors for boron carbide, the aloe vera is found to give a good yield above 50%.展开更多
天空地监测技术的迅速发展使得可免费获取的地形数据越来越多,而不同地形数据的精度和现势性制约着水文科学的创新和发展。收集目前可免费获取的数字高程模型,基于分辨率、现势性、覆盖范围等属性筛选出SRTM、ASTER2 GDEM和ALOS World 3...天空地监测技术的迅速发展使得可免费获取的地形数据越来越多,而不同地形数据的精度和现势性制约着水文科学的创新和发展。收集目前可免费获取的数字高程模型,基于分辨率、现势性、覆盖范围等属性筛选出SRTM、ASTER2 GDEM和ALOS World 3D三类数据源为研究对象,针对不同地形地貌区,计算分析与水文密切相关的DEM衍生特征的精度,进而提出不同数字高程模型在水文应用中的适用范围。经分析:各DEM在地势起伏大的区域,地形宏观描述基本一致;地势起伏小的区域,Aster2 DEM与其他三种DEM存在差异;在中小河流洪水预报的经验模型中,根据资料情况利用任何一种数字高程模型提取流域参数均可,不作为影响模型精度的重要指标。在地势起伏大的地区,除SRTM外各DEM对水系形态的描述精度较高;地势起伏小的地区,除ALOS world 3D能准确描述河口区域水系结构关系外,其余DEM均不能准确描述河口区域水系形态;分布式水文模型的产汇流分析、水文通视性分析等建议使用ALOS world 3D。展开更多
从0.6 m Quick Bird、2.5 m ALOS、10.0 m ALOS遥感影像中分别提取崩岗的特征数据,分析遥感影像的分辨率对崩岗数据精度的影响。结果表明:从0.6 m Quick Bird能容易地提取崩岗数据,且重现性较好,从2.5 m ALOS能提取崩岗数据,但重现性不...从0.6 m Quick Bird、2.5 m ALOS、10.0 m ALOS遥感影像中分别提取崩岗的特征数据,分析遥感影像的分辨率对崩岗数据精度的影响。结果表明:从0.6 m Quick Bird能容易地提取崩岗数据,且重现性较好,从2.5 m ALOS能提取崩岗数据,但重现性不强,从10.0 m ALOS无法提取崩岗。从0.6 m Quick Bird和2.5 m ALOS提取的崩岗,数量基本一致,但位置不一致、边界不重合、形状差别很大,从2.5m ALOS提取的崩岗周长平均减少20.83%,占58.33%的崩岗面积减少了,平均减少19.78%。因此,可断定0.6 m Quick Bird能反映崩岗的实际情况,2.5 m ALOS能较好地反映崩岗的实际情况,10.0 m ALOS完全不能提取崩岗数据。但高精度遥感影像的获取比较困难,且价格较贵。展开更多
基金support from UGC-SAP (DRS, Phase Ⅲ) with Sanction order No. F.510/3/DRS-Ⅲ/2015(SAPI)UGC-MRP with F. No. 43-539/2014 (SR)FD Diary No.3668
文摘The unique structural and physical properties of boron carbide, which make it suitable for a wide range of applications,demands the development of low-cost and green synthesis method. In the present work, the commonly available leaves of aloe vera are hydrothermally treated to form the carbon precursor for the synthesis of boron carbide. The morphological characterization reveals the porous nature of the precursor turning into a tubular structure upon boron carbide formation.The structural characterization by x-ray diffraction and other spectroscopic techniques such as Fourier transform infrared,Raman, photoluminescence and uv-visible near-infrared spectroscopy confirm the formation of boron carbide. The thermogravimetric analysis of the sample is found to exhibit good thermal stability above 500 °C. When the sample is annealed to 600 °C, boron carbide with phase purity is obtained, which is confirmed through XRD and FTIR analyses. The optical emission properties of the sample are studied through CIE plot and power spectrum. Compared with other natural precursors for boron carbide, the aloe vera is found to give a good yield above 50%.
文摘天空地监测技术的迅速发展使得可免费获取的地形数据越来越多,而不同地形数据的精度和现势性制约着水文科学的创新和发展。收集目前可免费获取的数字高程模型,基于分辨率、现势性、覆盖范围等属性筛选出SRTM、ASTER2 GDEM和ALOS World 3D三类数据源为研究对象,针对不同地形地貌区,计算分析与水文密切相关的DEM衍生特征的精度,进而提出不同数字高程模型在水文应用中的适用范围。经分析:各DEM在地势起伏大的区域,地形宏观描述基本一致;地势起伏小的区域,Aster2 DEM与其他三种DEM存在差异;在中小河流洪水预报的经验模型中,根据资料情况利用任何一种数字高程模型提取流域参数均可,不作为影响模型精度的重要指标。在地势起伏大的地区,除SRTM外各DEM对水系形态的描述精度较高;地势起伏小的地区,除ALOS world 3D能准确描述河口区域水系结构关系外,其余DEM均不能准确描述河口区域水系形态;分布式水文模型的产汇流分析、水文通视性分析等建议使用ALOS world 3D。
文摘从0.6 m Quick Bird、2.5 m ALOS、10.0 m ALOS遥感影像中分别提取崩岗的特征数据,分析遥感影像的分辨率对崩岗数据精度的影响。结果表明:从0.6 m Quick Bird能容易地提取崩岗数据,且重现性较好,从2.5 m ALOS能提取崩岗数据,但重现性不强,从10.0 m ALOS无法提取崩岗。从0.6 m Quick Bird和2.5 m ALOS提取的崩岗,数量基本一致,但位置不一致、边界不重合、形状差别很大,从2.5m ALOS提取的崩岗周长平均减少20.83%,占58.33%的崩岗面积减少了,平均减少19.78%。因此,可断定0.6 m Quick Bird能反映崩岗的实际情况,2.5 m ALOS能较好地反映崩岗的实际情况,10.0 m ALOS完全不能提取崩岗数据。但高精度遥感影像的获取比较困难,且价格较贵。
