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氧化还原引发体系下双层自交联丙烯酸核壳乳液的合成
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作者 亓子怡 程相林 +2 位作者 唐雅馨 洪涛 高明奇 《高分子材料科学与工程》 北大核心 2025年第1期10-18,共9页
以苯乙烯(St)、甲基丙烯酸甲酯(MMA)为硬单体,丙烯酸丁酯(BA)为软单体,乙烯基三甲氧基硅烷(A-171)和双丙酮丙烯酰胺(DAAM)分别为核层和壳层的交联单体,合成了室温自交联改性核壳结构丙烯酸酯乳液,探究了引发体系的选择与用量、交联单体... 以苯乙烯(St)、甲基丙烯酸甲酯(MMA)为硬单体,丙烯酸丁酯(BA)为软单体,乙烯基三甲氧基硅烷(A-171)和双丙酮丙烯酰胺(DAAM)分别为核层和壳层的交联单体,合成了室温自交联改性核壳结构丙烯酸酯乳液,探究了引发体系的选择与用量、交联单体种类和添加量对乳液聚合的影响。通过衰减全反射傅里叶变换红外光谱证明交联单体成功交联,通过Zeta电位分析、透射电镜对乳液进行表征,证明成功合成了均一的核壳乳液。结果证明,以半连续种子乳液聚合法聚合,引发剂KPS和NaHSO_(3)质量比为2:1、引发剂用量为0.4%、核层自交联单体乙烯基三甲氧基硅烷(A-171)和壳层自交联单体双丙酮丙烯酰胺(DAAM+ADH)的质量分数分别为3%和2%,乳液的稳定性、耐水性和成膜性良好,转化率在90%以上,吸水率为6.87%,钙离子稳定性合格。与非核壳无交联单体乳液进行对比,热重分析表明热分解温度提高了41℃,缓解了传统水性丙烯酸酯乳液涂层耐水性差、耐溶剂性差、“热粘冷脆”的问题。 展开更多
关键词 核壳乳液 氧化还原引发体系 核壳双层交联 水性油墨连接料
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Point cloud-based environment reconstruction and ray tracing simulations for railway tunnel channels
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作者 ziyi qi Ruisi He +6 位作者 Mi Yang Xuejian Zhang Bo Ai Weiming Li Shaopeng Wang Wenpu Sun Lizhe Li 《High-Speed Railway》 2023年第4期241-247,共7页
Radio propagation environment plays a critical role in the performance of wireless communication systems,and understanding channel characteristics is vital for ensuring reliable communication links and optimizing syst... Radio propagation environment plays a critical role in the performance of wireless communication systems,and understanding channel characteristics is vital for ensuring reliable communication links and optimizing system performance.Ray tracing is an effective method to investigate propagation characteristics in a complex environment,and how to quickly and accurately obtain environmental information needs to be solved.This paper presents dynamic environment reconstruction and ray tracing simulation in railway tunnel environment based on Simultaneous Localization and Mapping(SLAM)algorithm and Poisson reconstruction algorithm.Accurate channel parameters are obtained and analyzed based on ray tracing simulation.Both straight and curved tunnels are considered and investigated,and the results show the channel characteristics in complex railway tunnel environments. 展开更多
关键词 Railway communication TUNNELS Ray tracing Environment reconstruction Wireless channel
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