针对高氮钢增材过程中氮损失及力学性能降低等问题,采用常规脉冲熔化极气保电弧(Pulsed Gas Metal Arc,P-GMA)及在脉冲电流峰值阶段叠加超音频脉冲电流的P-GMA对高氮钢进行电弧增材制造实验,分别制备不同工艺参数下的单道多层高氮钢直壁...针对高氮钢增材过程中氮损失及力学性能降低等问题,采用常规脉冲熔化极气保电弧(Pulsed Gas Metal Arc,P-GMA)及在脉冲电流峰值阶段叠加超音频脉冲电流的P-GMA对高氮钢进行电弧增材制造实验,分别制备不同工艺参数下的单道多层高氮钢直壁体,研究超音频脉冲电流叠加对高氮钢电弧增材制造凝固方式、显微组织演变及力学性能的影响规律。研究结果表明:由于高氮钢在电弧增材过程中存在氮损失现象,不同增材模式下高氮钢金属熔池的凝固模式均由单相奥氏体凝固(A模式)转变为铁素体为先析出相、奥氏体依附铁素体界面析出(FA模式);相比于常规P-GMA,叠加超音频脉冲电流后P-GMA产生的高频超声效应能够提高氮元素的扩散,促进奥氏体相变,限制铁素体枝晶生长;经过对比分析,超音频脉冲电流对铁素体树枝晶Y轴方向的影响大于Z轴方向,对Y轴方向力学性能的影响也大于Z轴方向,当频率为60 kHz时Y轴方向抗拉强度提高了9.9%,屈服强度提高了15.9%。展开更多
针对高氮钢增材制造熔滴过渡过程中氮元素逸出及飞溅问题,进行超音频脉冲熔化极气体保护(Ultrasonic Frequency Pulsed Gas Metal Arc,UFP-GMA)增材制造熔滴过渡试验,研究不同超音频脉冲电流叠加模式和脉冲电流频率对高氮钢熔滴过渡稳...针对高氮钢增材制造熔滴过渡过程中氮元素逸出及飞溅问题,进行超音频脉冲熔化极气体保护(Ultrasonic Frequency Pulsed Gas Metal Arc,UFP-GMA)增材制造熔滴过渡试验,研究不同超音频脉冲电流叠加模式和脉冲电流频率对高氮钢熔滴过渡稳定性的影响,获取能够实现高氮钢增材稳定熔滴过渡的工艺参数。试验结果表明:在脉冲熔化极气体保护(Pulsed Gas Metal Arc,P-GMA)增材工艺条件下可以实现一脉一滴过渡,但是过渡稳定性较差,飞溅明显;在P-GMA基值阶段或基值和峰值阶段都叠加超音频脉冲电流均不利于熔滴过渡,容易出现短路、熔滴爆炸等问题;在P-GMA峰值阶段叠加低频(20 kHz)脉冲电流时,对熔滴过渡影响较弱,叠加中频(40~60 kHz)脉冲电流能抑制高氮钢熔滴过渡中大颗粒飞溅生成,提高熔滴过渡稳定性,但是当频率超过60 kHz时在过渡中会形成许多小飞溅。展开更多
Let X=Σ_(i=1)^(n)a_(i)ξ_(i)be a Rademacher sum with Var(X)=1 and Z be a standard normal random variable.This paper concerns the upper bound of|P(X≤x)−P(Z≤x)|for any x∈R.Using the symmetric properties and R softwa...Let X=Σ_(i=1)^(n)a_(i)ξ_(i)be a Rademacher sum with Var(X)=1 and Z be a standard normal random variable.This paper concerns the upper bound of|P(X≤x)−P(Z≤x)|for any x∈R.Using the symmetric properties and R software,this paper gets the following improved Berry-Esseen type bound under some conditions,|P(X≤x)−P(Z≤x)|≤P(Z∈(0,a1)),∀x∈R,which is one of the modified conjecture proposed by Nathan K.and Ohad K.展开更多
采用高效液相色谱法建立10批次不同产地马蹄金指纹图谱,并进行聚类分析。称取0.5 g马蹄金,以70%乙醇为溶剂,加热回流提取样品溶液,使用CACELLPAK-C_(18)色谱柱,流动相为乙腈-0.2%(体积比)磷酸水溶液,梯度洗脱,流量为1.0 m L/min,检测器...采用高效液相色谱法建立10批次不同产地马蹄金指纹图谱,并进行聚类分析。称取0.5 g马蹄金,以70%乙醇为溶剂,加热回流提取样品溶液,使用CACELLPAK-C_(18)色谱柱,流动相为乙腈-0.2%(体积比)磷酸水溶液,梯度洗脱,流量为1.0 m L/min,检测器波长为254 nm,建立马蹄金指纹图谱。10批次马蹄金相似度为0.97~0.99,相对保留时间测定结果的相对标准偏差(RSD)小于1.0%。通过共有模式筛选出8个共有特征峰,其中指认主要1个共有峰为芦丁。方法的重复性、稳定性测试的色谱峰面积RSD均小于1.0%,芦丁的样品加标回收率为98.78%~101.56%,RSD为1.0%(n=6),符合指纹图谱检测要求。运用SPSS 19.0软件进行聚类分析,马蹄金样品分为两大类。该方法具有良好的重复性和稳定性,结合相似度评价和聚类分析,可以评价不同产地马蹄金质量,为马蹄金的质量控制提供参考及对其产地的初步鉴别。展开更多
Objective： To study the anti-fatigue effects of salidroside in mice. Methods： Totally 120 normal male Kunming mice were randomized into 5 groups （4 salidroside intervention groups and the control group） based on b...Objective： To study the anti-fatigue effects of salidroside in mice. Methods： Totally 120 normal male Kunming mice were randomized into 5 groups （4 salidroside intervention groups and the control group） based on body weight. The control group was given distilled water and the 4 intervention groups were given various doses of salidroside （60, 180, 360, 720 mg/kg） for 15 consecutive days, respectively. The levels of lactate, serum urea nitrogen, muscle and liver glycogen, the longest swimming time and hemoglobin were determined before and after swimming test. Results： Different doses of salidroside significantly lengthened the swimming time and increased the contents of hemoglobin and muscle and liver glycogen, while reducing that of lactate in blood significantly compared with control group, especially in the 180 mg/kg salidroside group. Conclusion： Salidroside has noticeable anti-fatigue effect on mice. These effects were dose-dependent, and the strongest effect on most biomarkers was seen with an intermediate dose.展开更多
文摘针对高氮钢增材过程中氮损失及力学性能降低等问题,采用常规脉冲熔化极气保电弧(Pulsed Gas Metal Arc,P-GMA)及在脉冲电流峰值阶段叠加超音频脉冲电流的P-GMA对高氮钢进行电弧增材制造实验,分别制备不同工艺参数下的单道多层高氮钢直壁体,研究超音频脉冲电流叠加对高氮钢电弧增材制造凝固方式、显微组织演变及力学性能的影响规律。研究结果表明:由于高氮钢在电弧增材过程中存在氮损失现象,不同增材模式下高氮钢金属熔池的凝固模式均由单相奥氏体凝固(A模式)转变为铁素体为先析出相、奥氏体依附铁素体界面析出(FA模式);相比于常规P-GMA,叠加超音频脉冲电流后P-GMA产生的高频超声效应能够提高氮元素的扩散,促进奥氏体相变,限制铁素体枝晶生长;经过对比分析,超音频脉冲电流对铁素体树枝晶Y轴方向的影响大于Z轴方向,对Y轴方向力学性能的影响也大于Z轴方向,当频率为60 kHz时Y轴方向抗拉强度提高了9.9%,屈服强度提高了15.9%。
文摘针对高氮钢增材制造熔滴过渡过程中氮元素逸出及飞溅问题,进行超音频脉冲熔化极气体保护(Ultrasonic Frequency Pulsed Gas Metal Arc,UFP-GMA)增材制造熔滴过渡试验,研究不同超音频脉冲电流叠加模式和脉冲电流频率对高氮钢熔滴过渡稳定性的影响,获取能够实现高氮钢增材稳定熔滴过渡的工艺参数。试验结果表明:在脉冲熔化极气体保护(Pulsed Gas Metal Arc,P-GMA)增材工艺条件下可以实现一脉一滴过渡,但是过渡稳定性较差,飞溅明显;在P-GMA基值阶段或基值和峰值阶段都叠加超音频脉冲电流均不利于熔滴过渡,容易出现短路、熔滴爆炸等问题;在P-GMA峰值阶段叠加低频(20 kHz)脉冲电流时,对熔滴过渡影响较弱,叠加中频(40~60 kHz)脉冲电流能抑制高氮钢熔滴过渡中大颗粒飞溅生成,提高熔滴过渡稳定性,但是当频率超过60 kHz时在过渡中会形成许多小飞溅。
基金supported by the National Natural Science Foundation of China(Grant No.11861029)the Hainan Provincial Natural Science Foundation of China(Grants Nos.122MS056,124MS056).
文摘Let X=Σ_(i=1)^(n)a_(i)ξ_(i)be a Rademacher sum with Var(X)=1 and Z be a standard normal random variable.This paper concerns the upper bound of|P(X≤x)−P(Z≤x)|for any x∈R.Using the symmetric properties and R software,this paper gets the following improved Berry-Esseen type bound under some conditions,|P(X≤x)−P(Z≤x)|≤P(Z∈(0,a1)),∀x∈R,which is one of the modified conjecture proposed by Nathan K.and Ohad K.
基金the Foundation of the Gym Sport Bureau of Shanghai (04JT017)
文摘Objective： To study the anti-fatigue effects of salidroside in mice. Methods： Totally 120 normal male Kunming mice were randomized into 5 groups （4 salidroside intervention groups and the control group） based on body weight. The control group was given distilled water and the 4 intervention groups were given various doses of salidroside （60, 180, 360, 720 mg/kg） for 15 consecutive days, respectively. The levels of lactate, serum urea nitrogen, muscle and liver glycogen, the longest swimming time and hemoglobin were determined before and after swimming test. Results： Different doses of salidroside significantly lengthened the swimming time and increased the contents of hemoglobin and muscle and liver glycogen, while reducing that of lactate in blood significantly compared with control group, especially in the 180 mg/kg salidroside group. Conclusion： Salidroside has noticeable anti-fatigue effect on mice. These effects were dose-dependent, and the strongest effect on most biomarkers was seen with an intermediate dose.
