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利用安捷伦SampliQ SCX固相萃取柱和液相色谱/串联质谱联用检测猪肉中的β_2-激动剂
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作者 Chenhao Zhai jianzhong li Yue Song 《食品安全质量检测学报》 CAS 2011年第2期108-111,共4页
本应用报告开发并验证了一种同时检测四种β2-激动剂残留物的方法,包括特布他林、沙丁胺醇、克仑特罗和福莫特罗。分析物经过液-液萃取(LLE)和固相萃取(SPE)纯化后,由正离子多反应监测模式下的液相色谱耦合电喷雾串联质谱(LC-ESI-MS/MS... 本应用报告开发并验证了一种同时检测四种β2-激动剂残留物的方法,包括特布他林、沙丁胺醇、克仑特罗和福莫特罗。分析物经过液-液萃取(LLE)和固相萃取(SPE)纯化后,由正离子多反应监测模式下的液相色谱耦合电喷雾串联质谱(LC-ESI-MS/MS)进行定量。该方法为检测猪肉中四种β2-激动剂提供了亚ng/g水平的检测限(LOD),以及0.25至5ng/g的动态校准范围。总回收率为78%至101%,相对标准偏差(RSD)为1.8%至7.2%。 展开更多
关键词 激动剂 固相萃取 安捷伦 猪肉 肉类 克仑特罗 残留物 沙丁胺醇 特布他林 SampliQ SCX 部件号 离心分离 SPE 监测模式
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Effect of dynamic loading conditions on the dynamic performance of MP1 energy-absorbing rockbolts:Insight from laboratory drop test 被引量:3
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作者 Jinfu Lou Fuqiang Gao +2 位作者 jianzhong li Guiyang Yuan Mostafa Sharifzadeh 《International Journal of Mining Science and Technology》 SCIE EI CAS CSCD 2023年第2期215-231,共17页
Energy-absorbing rockbolts have been widely adopted in burst-prone excavation support, and their serviceability is closely related to the frequency and magnitude of seismic events. In this research, the splittube drop... Energy-absorbing rockbolts have been widely adopted in burst-prone excavation support, and their serviceability is closely related to the frequency and magnitude of seismic events. In this research, the splittube drop test with varying impact energy was conducted to reproduce the dynamic performance of MP1rockbolts under a wide range of seismic event magnitudes. The test results showed that the impact process could be subdivided into four distinct stages, i.e. mobilization, strain hardening, plastic flow(ductile), and rebound stage, of which strain hardening and plastic flow are the primary energy absorbing stages. As the impact energy per drop increases from 8.1 to 46.7 k J, the strain rate of the shank varies between 1.20 and 2.70 s^(-1), and the average impact load is between 240 and 270kN, which may be considered as constant. The MP1 rockbolt has a cumulative maximum energy absorption(CMEA) of 31.9–40.0 k J/m, with an average of 35.0 k J/m, and the elongation rate is 11.4%–14.7%, with an average of 12.7%, both of which are negatively correlated with the impact energy per drop. Regression analysis shows that energy absorption and shank elongation, as well as momentum input and impact duration,conform to the linear relationship. The complete dynamic capacity envelope of MP1 rockbolts is proposed, which reflects the dynamic bearing capacity, elongation, and distinct stages. This study is helpful to better understand the dynamic characteristics of energy-absorbing rockbolts and assist design engineers in robust reinforcement systems design to mitigate rockburst damage in seismically active underground excavations. 展开更多
关键词 Energy-absorbing rockbolt Dynamic performance Drop test Residual elastic energy(REE) Energy absorption rate(EAR) Dynamic capacity envelope
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洋流干扰下无人船限制水域直线跟踪安全视距制导
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作者 彭周华 李建众 +1 位作者 韩冰 古楠 《哈尔滨工程大学学报(英文版)》 CSCD 2023年第3期602-613,共12页
The collision-free straight-line following of an unmanned surface vehicle(USV)moving in a constrained water region subject to stationary and moving obstacles is addressed in this paper.USV systems are normally subject... The collision-free straight-line following of an unmanned surface vehicle(USV)moving in a constrained water region subject to stationary and moving obstacles is addressed in this paper.USV systems are normally subjected to surge velocity constraints,yaw rate constraints,and unknown ocean currents.Herein,a safety-certificated line-of-sight(LOS)guidance method is proposed to achieve a constrained straight-line following task.First,an antidisturbance LOS guidance law is designed based on the LOS guidance scheme and an extended state observer.Furthermore,collision avoidance with waterway boundaries and stationary/moving obstacles is encoded in control barrier functions,utilizing which the safety constraints are transformed into input constraints.Finally,safety-certificated guidance signals are obtained by solving a quadratic programming problem subject to input constraints.Using the proposed safety-certified LOS guidance method,the USV can accomplish a straight-line following task with guaranteed input-to-state safety.Simulation results substantiate the efficacy of the proposed safety-certificated LOS guidance method for the straight-line following of USVs moving in a constrained water region subject to unknown ocean currents. 展开更多
关键词 Line-of-sight guidance Constrained water region Unmanned surface vehicle Control barrier function Extended state observer
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