针对纳米ZnO在制备以及使用的过程中极易发生团聚从而影响其抗菌性能这一缺点,设计实验使得纳米ZnO在溶胶凝胶过程中与多孔SiO2进行复合。通过扫描电子显微镜(Scanning electron microscope, SEM)以及透射电子显微镜(Transmission elect...针对纳米ZnO在制备以及使用的过程中极易发生团聚从而影响其抗菌性能这一缺点,设计实验使得纳米ZnO在溶胶凝胶过程中与多孔SiO2进行复合。通过扫描电子显微镜(Scanning electron microscope, SEM)以及透射电子显微镜(Transmission electron microscopy, TEM)等可以发现,ZnO很好地复合在多孔SiO2的骨架上并且分散得较为均匀。通过表面积测试(Brunner-emmet-teller measurement, BET)以及光致发光光谱(Photoluminescence spectrum,PL)的测试可以发现,复合材料的比表面积得到提高且光学性能加强。通过菌落计数法探究复合材料与单组分纳米ZnO的抗菌性能差异以及复合材料中纳米ZnO含量的变化导致的抗菌性能的变化。结论证明,当纳米ZnO与多孔SiO2进行复合之后,材料的抗菌性能得到了极大的提高,抑菌率超过了99%。展开更多
With the increasing of users and the demands which are transforming from the monotonous traditional service to network service,Multiple space environment web applications including browser-client,rich-client and mobil...With the increasing of users and the demands which are transforming from the monotonous traditional service to network service,Multiple space environment web applications including browser-client,rich-client and mobile-client applications have been developed by SEPC(Space Environment Prediction Center,NSSC,CAS)during the past few years.The architecture of Operational Space Environment Technology System(OSETS) that these applications rely on is described and the description of structural optimization of the architecture is provided.To demonstrate the evolution of the OSETS,three web application examples for e SpaceWx,Space Weather Situation Awareness Picture(SWSAP),Plug-and-Play SWx Analysis and Plotting Program(PPSWAP) are presented.展开更多
Pt and Ir coatings were produced by double glow plasma technology on the surface of Ti alloy substrates. The chemical compositions of the coatings were determined by X-ray diffraction and X-ray photoelectron spectrosc...Pt and Ir coatings were produced by double glow plasma technology on the surface of Ti alloy substrates. The chemical compositions of the coatings were determined by X-ray diffraction and X-ray photoelectron spectroscopy. The microstructure and morphology of the coatings were observed by scanning electron microscopy. The hardness and elastic modulus of the coatings were estimated by nanoindentation. The measurements of adhesive forces of the coatings were performed with scratch tester. The results indicated that the Pt and Ir coatings displayed the preferred (220) orientation due to the initial nuclei with preferred growth on the surface of the substrates. The interface between the Pt coating and substrate exhibited no evidence of delamination. The Ir coating was composed of irregular columnar grains with many nanovoids at the interface between the coating and substrate. The mean values of hardness for Pt and Ir coatings were 0.9 GPa and 9 GPa, respectively. The elastic modulus of Pt and Ir coatings were 178 GPa and 339 GPa, respectively. The adhesive forces of the Pt and Ir coatings were about 66.4 N and 55 N, respectively. The Pt and Ir coatings adhered well to the Ti alloy substrates.展开更多
In this paper,glass fibers were prepared by centrifugal-spinneret-blow(CSB) process.The molten glass got different flow rate from 390 kg/h to 270 kg/h by adjusting the electric current of platinum/10 rhodium alloy bus...In this paper,glass fibers were prepared by centrifugal-spinneret-blow(CSB) process.The molten glass got different flow rate from 390 kg/h to 270 kg/h by adjusting the electric current of platinum/10 rhodium alloy bushing.The diameter and microstructure of glass fibers have been investigated by scanning electron microscopy(SEM) and vertical optical microscope(VOM).The results indicated that the flow rate of molten glass was proportional to the diameter of glass fibers when the molten glass got main flow rate of 330 kg/h.The lower the flow rate was,the finer the average diameter was.展开更多
文摘针对纳米ZnO在制备以及使用的过程中极易发生团聚从而影响其抗菌性能这一缺点,设计实验使得纳米ZnO在溶胶凝胶过程中与多孔SiO2进行复合。通过扫描电子显微镜(Scanning electron microscope, SEM)以及透射电子显微镜(Transmission electron microscopy, TEM)等可以发现,ZnO很好地复合在多孔SiO2的骨架上并且分散得较为均匀。通过表面积测试(Brunner-emmet-teller measurement, BET)以及光致发光光谱(Photoluminescence spectrum,PL)的测试可以发现,复合材料的比表面积得到提高且光学性能加强。通过菌落计数法探究复合材料与单组分纳米ZnO的抗菌性能差异以及复合材料中纳米ZnO含量的变化导致的抗菌性能的变化。结论证明,当纳米ZnO与多孔SiO2进行复合之后,材料的抗菌性能得到了极大的提高,抑菌率超过了99%。
文摘With the increasing of users and the demands which are transforming from the monotonous traditional service to network service,Multiple space environment web applications including browser-client,rich-client and mobile-client applications have been developed by SEPC(Space Environment Prediction Center,NSSC,CAS)during the past few years.The architecture of Operational Space Environment Technology System(OSETS) that these applications rely on is described and the description of structural optimization of the architecture is provided.To demonstrate the evolution of the OSETS,three web application examples for e SpaceWx,Space Weather Situation Awareness Picture(SWSAP),Plug-and-Play SWx Analysis and Plotting Program(PPSWAP) are presented.
基金supported by the National Natural Science Foundation of China(50872055/E020703)Funding for Outstanding Doctoral Dissertation in NUAA(BCXJ1109)the Funding of Jiangsu Innovation Program for Graduate Education(CXLX11_0207)
文摘Pt and Ir coatings were produced by double glow plasma technology on the surface of Ti alloy substrates. The chemical compositions of the coatings were determined by X-ray diffraction and X-ray photoelectron spectroscopy. The microstructure and morphology of the coatings were observed by scanning electron microscopy. The hardness and elastic modulus of the coatings were estimated by nanoindentation. The measurements of adhesive forces of the coatings were performed with scratch tester. The results indicated that the Pt and Ir coatings displayed the preferred (220) orientation due to the initial nuclei with preferred growth on the surface of the substrates. The interface between the Pt coating and substrate exhibited no evidence of delamination. The Ir coating was composed of irregular columnar grains with many nanovoids at the interface between the coating and substrate. The mean values of hardness for Pt and Ir coatings were 0.9 GPa and 9 GPa, respectively. The elastic modulus of Pt and Ir coatings were 178 GPa and 339 GPa, respectively. The adhesive forces of the Pt and Ir coatings were about 66.4 N and 55 N, respectively. The Pt and Ir coatings adhered well to the Ti alloy substrates.
文摘In this paper,glass fibers were prepared by centrifugal-spinneret-blow(CSB) process.The molten glass got different flow rate from 390 kg/h to 270 kg/h by adjusting the electric current of platinum/10 rhodium alloy bushing.The diameter and microstructure of glass fibers have been investigated by scanning electron microscopy(SEM) and vertical optical microscope(VOM).The results indicated that the flow rate of molten glass was proportional to the diameter of glass fibers when the molten glass got main flow rate of 330 kg/h.The lower the flow rate was,the finer the average diameter was.
