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一步合成PAN/Cu_3(BTC)_2薄膜及其可见光催化性能 被引量:1
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作者 李宗群 臧一鹏 +2 位作者 李姣 刘恋 吴丽 《蚌埠学院学报》 2015年第3期30-34,共5页
以Cu(Ac)2·H2O和均苯三甲酸(H3BTC)为原料,在不同浓度的聚丙烯腈(PAN)溶液中,一步超声合成了PAN/Cu3(BTC)2复合材料,并在石英玻璃基片上采用旋涂法制备了相应的薄膜。采用X-射线衍射(XRD)、扫描电镜(SEM)、傅里叶变换红外光谱(FT-... 以Cu(Ac)2·H2O和均苯三甲酸(H3BTC)为原料,在不同浓度的聚丙烯腈(PAN)溶液中,一步超声合成了PAN/Cu3(BTC)2复合材料,并在石英玻璃基片上采用旋涂法制备了相应的薄膜。采用X-射线衍射(XRD)、扫描电镜(SEM)、傅里叶变换红外光谱(FT-IR)、紫外-可见漫反射光谱(UV-vis)对薄膜进行表征。结果表明,采用超声法成功地合成了PAN/Cu3(BTC)2复合材料,Cu3(BTC)2纳米晶随着PAN浓度的增加,尺寸由30 nm逐步增大到100 nm。薄膜在可见光下对亚甲基蓝(MB)具有良好的脱色性能,加入不同的牺牲剂能够不同程度地提高薄膜光催化效率,不同的牺牲剂对提高材料的光催化效率,由大到小的顺序为:三乙胺>乙胺>H2O2>甲胺>三丁胺>苯胺。 展开更多
关键词 金属-有机骨架 超声合成 薄膜 光催化
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A spin-based magnetic scanning microscope for in-situ strain tuning of soft matter
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作者 丁哲 孙豫蒙 +8 位作者 王孟祺 余佩 郑宁冲 臧一鹏 王鹏飞 王亚 聂越峰 石发展 杜江峰 《Chinese Physics B》 SCIE EI CAS CSCD 2023年第5期102-107,共6页
We present a magnetic scanning microscope equipped with a nitrogen-vacancy(NV) center scanning probe that has the ability to mechanically tune the strain of soft matter in-situ. The construction of the microscope and ... We present a magnetic scanning microscope equipped with a nitrogen-vacancy(NV) center scanning probe that has the ability to mechanically tune the strain of soft matter in-situ. The construction of the microscope and a continuous straintuning sample holder are discussed. An optically detected magnetic resonance protocol utilized in the imaging is described.In order to show the reliability of this microscope, the strain conduction is estimated with finite element simulation, and xray diffraction is required for calibration when freestanding crystal films are under consideration. A magnetic imaging result is displayed to demonstrate the nano-scale imaging capability. The microscope presented in this work is helpful in studying strain-coupled magnetic physics such as magnetic phase transition under strain and strain-tuned cycloidal orientation tilting. 展开更多
关键词 nitrogen-vacancy(NV)center ANTIFERROMAGNETISM strain tuning soft matter
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