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黄姜皂甙元清洁生产工艺 被引量:3
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作者 程军 冯求宝 +2 位作者 王颜 周文举 谭远友 《武汉科技学院学报》 2005年第6期49-52,共4页
以黄姜为原料,研究提取皂甙元的清洁生产工艺。本工艺采用溶剂把黄姜中的皂甙与淀粉、纤维素等成分分离,然后再将皂甙水解、过滤、中和、脱水、提取、重结晶,从而得到高纯度的皂甙元。研究表明:用4#溶剂提取皂甙效果较好;溶剂的回收率可... 以黄姜为原料,研究提取皂甙元的清洁生产工艺。本工艺采用溶剂把黄姜中的皂甙与淀粉、纤维素等成分分离,然后再将皂甙水解、过滤、中和、脱水、提取、重结晶,从而得到高纯度的皂甙元。研究表明:用4#溶剂提取皂甙效果较好;溶剂的回收率可达98%以上;水解的酸浓度为[H+]=0.5mol/l较好、水解的压力为0.7-0.8Mpa较适合、水解时间为6h。在这些条件下,皂甙元的得率可以达到95%以上。本工艺产生的生产废水不到传统工艺的10%,酸的用量约为传统工艺的10%,皂甙元的得率有所提高,生产周期也大大缩短了,资源的综合利用率明显提高。 展开更多
关键词 黄姜 薯蓣皂甙元 水解 提取工艺
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Preliminary Study of Thermal Treatment of Coke Wastewater Sludge Using Plasma Torch 被引量:1
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作者 李铭书 李胜利 +2 位作者 孙德茂 刘欣 冯求宝 《Plasma Science and Technology》 SCIE EI CAS CSCD 2016年第10期1020-1026,共7页
Thermal plasma was applied for the treatment of coke wastewater sludge derived from the steel industry in order to investigate the feasibility of the safe treatment and energy recovery of the sludge. A 30 kW plasma to... Thermal plasma was applied for the treatment of coke wastewater sludge derived from the steel industry in order to investigate the feasibility of the safe treatment and energy recovery of the sludge. A 30 kW plasma torch system was applied to study the vitrification and gas production of coke wastewater sludge. Toxicity leaching results indicated that the sludge treated via the thermal plasma process converted into a vitrified slag which resisted the leaching of heavy metals. CO2 was utilized as working gas to study the production and heat energy of the syngas. The heating value of the gas products by thermal plasma achieved 8.43 k J/L, indicating the further utilization of the gas products. Considering the utilization of the syngas and recovery heat from the gas products, the estimated treatment cost of coke wastewater sludge via plasma torch was about 0.98 CNY/kg sludge in the experiment. By preliminary economic analysis, the dehydration cost takes an important part of the total sludge treatment cost. The treatment cost of the coke wastewater sludge with 50 wt.% moisture was calculated to be about 1.45 CNY/kg sludge dry basis. The treatment cost of the coke wastewater sludge could be effectively controlled by decreasing the water content of the sludge. These findings suggest that an economic dewatering pretreatment method could be combined to cut the total treatment cost in an actual treatment process. 展开更多
关键词 thermal plasma plasma torch SLUDGE SYNGAS leachate toxicity
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