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A comprehensive review of existing corpora and methods for creating annotated corpora for event extraction tasks
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作者 Mohd Hafizul Afifi Abdullah Norshakirah Aziz +3 位作者 Said Jadid Abdulkadir Kashif Hussain Hitham Alhussian Noureen Talpur 《Journal of Data and Information Science》 CSCD 2024年第4期196-238,共43页
Purpose:The purpose of this study is to serve as a comprehensive review of the existing annotated corpora.This review study aims to provide information on the existing annotated corpora for event extraction,which are ... Purpose:The purpose of this study is to serve as a comprehensive review of the existing annotated corpora.This review study aims to provide information on the existing annotated corpora for event extraction,which are limited but essential for training and improving the existing event extraction algorithms.In addition to the primary goal of this study,it provides guidelines for preparing an annotated corpus and suggests suitable tools for the annotation task.Design/methodology/approach:This study employs an analytical approach to examine available corpus that is suitable for event extraction tasks.It offers an in-depth analysis of existing event extraction corpora and provides systematic guidelines for researchers to develop accurate,high-quality corpora.This ensures the reliability of the created corpus and its suitability for training machine learning algorithms.Findings:Our exploration reveals a scarcity of annotated corpora for event extraction tasks.In particular,the English corpora are mainly focused on the biomedical and general domains.Despite the issue of annotated corpora scarcity,there are several high-quality corpora available and widely used as benchmark datasets.However,access to some of these corpora might be limited owing to closed-access policies or discontinued maintenance after being initially released,rendering them inaccessible owing to broken links.Therefore,this study documents the available corpora for event extraction tasks.Research limitations:Our study focuses only on well-known corpora available in English and Chinese.Nevertheless,this study places a strong emphasis on the English corpora due to its status as a global lingua franca,making it widely understood compared to other languages.Practical implications:We genuinely believe that this study provides valuable knowledge that can serve as a guiding framework for preparing and accurately annotating events from text corpora.It provides comprehensive guidelines for researchers to improve the quality of corpus annotations,especially for event extraction tasks across various domains.Originality/value:This study comprehensively compiled information on the existing annotated corpora for event extraction tasks and provided preparation guidelines. 展开更多
关键词 Information extraction Event extraction Text mining Large language model Natural language processing
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Experimental investigation on coal pore-fracture variation and fractal characteristics synergistically affected by solvents for improving clean gas extraction 被引量:1
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作者 Feilin Han Sheng Xue +3 位作者 Chunshan Zheng Zhongwei Chen Guofu Li Bingyou Jiang 《International Journal of Mining Science and Technology》 SCIE EI CAS CSCD 2024年第3期413-425,共13页
Chemical solvents instead of pure water being as hydraulic fracturing fluid could effectively increase permeability and improve clean methane extraction efficiency.However,pore-fracture variation features of lean coal... Chemical solvents instead of pure water being as hydraulic fracturing fluid could effectively increase permeability and improve clean methane extraction efficiency.However,pore-fracture variation features of lean coal synergistically affected by solvents have not been fully understood.Ultrasonic testing,nuclear magnetic resonance analysis,liquid phase mass spectrometry was adopted to comprehensively analyze pore-fracture change characteristics of lean coal treated by combined solvent(NMP and CS_(2)).Meanwhile,quantitative characterization of above changing properties was conducted using geometric fractal theory.Relationship model between permeability,fractal dimension and porosity were established.Results indicate that the end face fractures of coal are well developed after CS2and combined solvent treatments,of which,end face box-counting fractal dimensions range from 1.1227 to 1.4767.Maximum decreases in ultrasonic longitudinal wave velocity of coal affected by NMP,CS_(2)and combined solvent are 2.700%,20.521%,22.454%,respectively.Solvent treatments could lead to increasing amount of both mesopores and macropores.Decrease ratio of fractal dimension Dsis 0.259%–2.159%,while permeability increases ratio of NMR ranges from 0.1904 to 6.4486.Meanwhile,combined solvent could dissolve coal polar and non-polar small molecules and expand flow space.Results could provide reference for solvent selection and parameter optimization of permeability-enhancement technology. 展开更多
关键词 Clean gas extraction Chemical solvent Experimental investigation Fractal characteristics Pore fracture
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Influence of ion species on extraction characteristicsof mixed ion beams
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作者 Ao Xu Pingping Gan +1 位作者 Xiang Wan Yuanjie Shi 《Chinese Physics B》 SCIE EI CAS CSCD 2024年第9期444-449,共6页
The spatial distributions of different kinds of ions are usually not completely the same in the process of extracting.In order to study the reason for the different characteristics of ion extraction, a simplified simu... The spatial distributions of different kinds of ions are usually not completely the same in the process of extracting.In order to study the reason for the different characteristics of ion extraction, a simplified simulation model of Cu+ andCr+ ions extraction process was established by 2D3V (two-dimensional in space and three- dimensional in velocity space)particle-in-cell (PIC) method. The effects of different extraction voltages from 0 V to 500 V on the density distribution ofCu+ and Cr+ ions and the change of plasma emission surface were analyzed. On the basis of this model, the ion densitydistribution characteristics of Cu+ ions mixed with Li+, Mg+, K+, Fe+, Y+, Ag+, Xe+, Au+, and Pb+ ions respectivelyunder 200-V extraction voltage are further simulated, and it is revealed that the atomic mass of the ions is the key reason fordifferent ion density distributions when different kinds of ions are mixed and extracted, which provides support for furtherunderstanding of ion extraction characteristics. 展开更多
关键词 extraction ion species density distribution atomic mass
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Mass Spectrometry-based Deep Coverage Proteome:Evaluation of Cellular Protein Extraction Methods
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作者 XU Xia QIN Weida +3 位作者 LI Ruomeng WANG Qianqian LIU Ning LI Gongyu 《高等学校化学学报》 SCIE EI CAS CSCD 北大核心 2024年第11期98-107,共10页
The current study comprehensively evaluates four different protein extraction methods based on urea,sodium dodecyl sulfate(SDS),anionic surfactants(BT),and total RNA extractor(Trizol),aiming to optimize the sample pre... The current study comprehensively evaluates four different protein extraction methods based on urea,sodium dodecyl sulfate(SDS),anionic surfactants(BT),and total RNA extractor(Trizol),aiming to optimize the sample preparation workflow for mass spectrometry-based proteomics.Using HeLa cells as an example,we found that the method employing the mass spectrometry-compatible surfactant BT reagent significantly reduces the total time consumed for protein extraction and minimizes protein losses during the sample preparation process.Further integrating the four protein extraction methods,we identified over 7000 proteins from HeLa cells without relying on pre-fractionation techniques,and 2990 of them were quantified using label-free quantification.It is worth noting that the BT and SDS methods demonstrate higher efficiency in extracting membrane proteins,while the Urea and Trizol methods are more effective in extracting proteins from nuclear and cytoplasmic fractions.In summary,this study provides a novel solution for deep proteome coverage,particularly in the context of cellular protein extraction,by integrating mass spectrometry-compatible surfactants with traditional extraction methods to effectively enhance protein identification numbers. 展开更多
关键词 SURFACTANT Protein extraction PROTEOMICS Mass spectrometry
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Influence of extraction voltage on electron and ion behavior characteristics
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作者 徐翱 甘娉娉 +1 位作者 石元杰 陈磊 《Chinese Physics B》 SCIE EI CAS CSCD 2024年第4期553-559,共7页
The characteristics of the extracted ion current have a significant impact on the design and testing of ion source performance.In this paper,a 2D in space and 3D in velocity space particle in cell(2D3V PIC)method is u... The characteristics of the extracted ion current have a significant impact on the design and testing of ion source performance.In this paper,a 2D in space and 3D in velocity space particle in cell(2D3V PIC)method is utilized to simulate plasma motion and ion extraction characteristics under various initial plasma velocity distributions and extraction voltages in a Cartesian coordinate system.The plasma density is of the order of 10^(15)m^(-3)-10^(16)m^(-3)and the extraction voltage is of the order of 100 V-1000 V.The study investigates the impact of various extraction voltages on the velocity and density distributions of electrons and positive ions,and analyzes the influence of different initial plasma velocity distributions on the extraction current.The simulation results reveal that the main reason for the variation of extraction current is the spacecharge force formed by the relative aggregation of positive and negative net charges.This lays the foundation for a deeper understanding of extraction beam characteristics. 展开更多
关键词 extraction voltage PLASMA ion beam ion current
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Extraction of reflected waves from acoustic logging data using variation mode decomposition and curvelet transform
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作者 Fan-Tong Kong Yong-Xiang Liu +3 位作者 Xi-Hao Gu Li Zhen Cheng-Ming Luo Sheng-Qing Li 《Petroleum Science》 SCIE EI CAS CSCD 2024年第5期3142-3156,共15页
Remote reflection waves, essential for acquiring high-resolution images of geological structures beyond boreholes, often suffer contamination from strong direct mode waves propagating along the borehole.Consequently, ... Remote reflection waves, essential for acquiring high-resolution images of geological structures beyond boreholes, often suffer contamination from strong direct mode waves propagating along the borehole.Consequently, the extraction of weak reflected waves becomes pivotal for optimizing migration image quality. This paper introduces a novel approach to extracting reflected waves by sequentially operating in the spatial frequency and curvelet domains. Using variation mode decomposition(VMD), single-channel spatial domain signals within the common offset gather are iteratively decomposed into high-wavenumber and low-wavenumber intrinsic mode functions(IMFs). The low-wavenumber IMF is then subtracted from the overall waveform to attenuate direct mode waves. Subsequently, the curvelet transform is employed to segregate upgoing and downgoing reflected waves within the filtered curvelet domain. As a result, direct mode waves are substantially suppressed, while the integrity of reflected waves is fully preserved. The efficacy of this approach is validated through processing synthetic and field data, underscoring its potential as a robust extraction technique. 展开更多
关键词 Borehole acoustic reflection imaging Variation mode decomposition Curvelet transform Weak signal extraction
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An air combat maneuver pattern extraction based on time series segmentation and clustering analysis
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作者 Zhifei Xi Yingxin Kou +2 位作者 Zhanwu Li Yue Lv You Li 《Defence Technology(防务技术)》 SCIE EI CAS CSCD 2024年第6期149-162,共14页
Target maneuver recognition is a prerequisite for air combat situation awareness,trajectory prediction,threat assessment and maneuver decision.To get rid of the dependence of the current target maneuver recognition me... Target maneuver recognition is a prerequisite for air combat situation awareness,trajectory prediction,threat assessment and maneuver decision.To get rid of the dependence of the current target maneuver recognition method on empirical criteria and sample data,and automatically and adaptively complete the task of extracting the target maneuver pattern,in this paper,an air combat maneuver pattern extraction based on time series segmentation and clustering analysis is proposed by combining autoencoder,G-G clustering algorithm and the selective ensemble clustering analysis algorithm.Firstly,the autoencoder is used to extract key features of maneuvering trajectory to remove the impacts of redundant variables and reduce the data dimension;Then,taking the time information into account,the segmentation of Maneuver characteristic time series is realized with the improved FSTS-AEGG algorithm,and a large number of maneuver primitives are extracted;Finally,the maneuver primitives are grouped into some categories by using the selective ensemble multiple time series clustering algorithm,which can prove that each class represents a maneuver action.The maneuver pattern extraction method is applied to small scale air combat trajectory and can recognize and correctly partition at least 71.3%of maneuver actions,indicating that the method is effective and satisfies the requirements for engineering accuracy.In addition,this method can provide data support for various target maneuvering recognition methods proposed in the literature,greatly reduce the workload and improve the recognition accuracy. 展开更多
关键词 Maneuver pattern extraction Data mining Fuzzy segmentation Selective ensemble clustering
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Online identification and extraction method of regional large-scale adjustable load-aggregation characteristics
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作者 Siwei Li Liang Yue +1 位作者 Xiangyu Kong Chengshan Wang 《Global Energy Interconnection》 EI CSCD 2024年第3期313-323,共11页
This article introduces the concept of load aggregation,which involves a comprehensive analysis of loads to acquire their external characteristics for the purpose of modeling and analyzing power systems.The online ide... This article introduces the concept of load aggregation,which involves a comprehensive analysis of loads to acquire their external characteristics for the purpose of modeling and analyzing power systems.The online identification method is a computer-involved approach for data collection,processing,and system identification,commonly used for adaptive control and prediction.This paper proposes a method for dynamically aggregating large-scale adjustable loads to support high proportions of new energy integration,aiming to study the aggregation characteristics of regional large-scale adjustable loads using online identification techniques and feature extraction methods.The experiment selected 300 central air conditioners as the research subject and analyzed their regulation characteristics,economic efficiency,and comfort.The experimental results show that as the adjustment time of the air conditioner increases from 5 minutes to 35 minutes,the stable adjustment quantity during the adjustment period decreases from 28.46 to 3.57,indicating that air conditioning loads can be controlled over a long period and have better adjustment effects in the short term.Overall,the experimental results of this paper demonstrate that analyzing the aggregation characteristics of regional large-scale adjustable loads using online identification techniques and feature extraction algorithms is effective. 展开更多
关键词 Load aggregation Regional large-scale Online recognition Feature extraction method
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Study on the green extraction of corncob xylan by deep eutectic solvent
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作者 Bingyu Jiao Le Wang +3 位作者 Haitao Gui Zifu Ni Rong Du Yuansen Hu 《Grain & Oil Science and Technology》 CAS 2024年第1期50-59,共10页
Corn as one of the world's major food crops,its by-product corn cob is also rich in resources.However,the unreasonable utilization of corn cob often causes the environmental pollution,waste of resources and other ... Corn as one of the world's major food crops,its by-product corn cob is also rich in resources.However,the unreasonable utilization of corn cob often causes the environmental pollution,waste of resources and other problems.As one of the most abundant polymers in nature,xylan is widely used in food,medicine,materials and other fields.Corn cob is rich in xylan,which is an ideal raw material for extracting xylan.However,the intractable lignin is covalently linked to xylan,which increases the difficulty of xylan extraction.It has been reported that the deep eutectic solvent(DES)could preferentially dissolve lignin in biomass,thereby dissolving the xylan.Then,the xylan in the extract was separated by ethanol precipitation method.The xylan precipitate was obtained after centrifugation,while the supernatant was retained.The components of the supernatant after ethanol precipitation were separated by the rotary evaporator.The ethanol,water and DES were collected for the subsequent extraction of corn cob xylan.In this study,a novel way was provided for the green production of corn cob xylan.The DES was used to extract xylan from corn cob which was used as the raw material.The effects of solid-liquid ratio,reaction time,reaction temperature and water content of DES on the extraction rate of corn cob xylan were investigated by the single factor test.Furthermore,the orthogonal test was designed to optimize the xylan extraction process.The structure of corn cob xylan was analyzed and verified.The results showed that the optimum extraction conditions of corn cob xylan were as follows:the ratio of corn cob to DES was 1:15(g:mL),the extraction time was 3 h,the extraction temperature was 60℃,and the water content of DES was 70%.Under these conditions,the extraction rate of xylan was 16.46%.The extracted corn cob xylan was distinctive triple helix of polysaccharide,which was similar to the structure of commercially available xylan.Xylan was effectively and workably extracted from corn cob by the DES method.This study provided a new approach for high value conversion of corn cob and the clean production of xylan. 展开更多
关键词 CORNCOB Deep eutectic solvent XYLAN Process optimization extraction
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Extraction,chemical components,bioactive functions and adulteration identification of walnut oils:A review
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作者 Yuan Gao Jia Hu +6 位作者 Xia Su Qi Li Caihong Su Yongling Li Gaiqin Ma Siyu Zhang Xiuzhu Yu 《Grain & Oil Science and Technology》 CAS 2024年第1期30-41,共12页
Walnut oil is a functional wood oil known to researchers that may potentially be a large source of Chinese edible oils.There are various extraction methods for walnut oil,including traditional(pressing,solvent-and enz... Walnut oil is a functional wood oil known to researchers that may potentially be a large source of Chinese edible oils.There are various extraction methods for walnut oil,including traditional(pressing,solvent-and enzymeassisted extraction)and novel methods(microwave,ultrasound,supercritical CO_(2),subcritical and other extraction technologies).Walnut oil is rich in nutrients,including phytosterols,tocopherols,polyphenols,squalene and minerals.It provides many health benefits,such as antioxidant,antitumor,anti-inflammatory,antidiabetic and lipid metabolism-related functions.In addition,the authentication of walnut oil has received much research attention.The present review provides detailed research on walnut oil extraction,composition,health benefits and adulteration identification methods.The path toward further walnut oil improvement in the context of the market value of walnut oil is also discussed. 展开更多
关键词 extraction technology Chemical composition Bioactive AUTHENTICATION
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Evaluation of yields and quality parameters of oils from Cornus wilsoniana fruit extracted by subcritical n-butane extraction and conventional methods 被引量:1
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作者 Jingjing Xiao Jingzhi Wu +3 位作者 Yan Chao Rukuan Liu Changzhu Li Zhihong Xiao 《Grain & Oil Science and Technology》 2022年第4期204-212,共9页
Cornus wilsoniana fruit oil is a very important woody oil and is the main raw material of biodiesel.In this study,the oil yield,physicochemical properties,fatty acid composition,rheological properties,thermal stabilit... Cornus wilsoniana fruit oil is a very important woody oil and is the main raw material of biodiesel.In this study,the oil yield,physicochemical properties,fatty acid composition,rheological properties,thermal stability,and Fourier transform infrared(FTIR)spectra of C.wilsoniana fruit oil obtained by subcritical n-butane extraction(SBE)and conventional methods such as pressing extraction(PE)and Soxhlet extraction(SE)were determined to study the influence of different extraction methods on the quality and yield of C.wilsoniana fruit oil.The oil yield of SBE(19.47%)was higher than that of PE(9.93%)but slightly lower than that of SE(21.08%).All of the extracted oils exhibited similar physicochemical properties,and the SBE oil was richer in polyunsaturated fatty acids(PUFA)than that of the PE oil,with an approximate 1:2 ratio of total saturated fatty acids against unsaturated fatty acids.The results of rheological behavior and thermal stability showed that all extracted oils had Newtonian flow characteristics,wherein the SBE oil exhibited lower viscosity and higher thermal stability.Furthermore,scanning electron microscopy(SEM)images of the surface topography indicated that different oil extraction methods will affect the residual oil content of the C.wilsoniana fruit powder.Compared with PE,the pores on the surface of the C.wilsoniana fruit powder after oil extraction were clearly visible,indicating that the driving force of SBE for oil extraction is stronger than that of PE.Based on the above results,it is implied that SBE is the best of the three methods for extracting C.wilsoniana fruit oil and can be potentially applied to extract other edible oils. 展开更多
关键词 Cornus wilsoniana fruit oil Subcritical n-butane extraction Pressing extraction Soxhlet extraction Thermal stability Rheological property
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Effect of Allelochemicals of Chinese-fir root extracted by supercritical CO_2 extraction on Chinese fir 被引量:9
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作者 林思祖 曹光球 +1 位作者 杜玲 王爱萍 《Journal of Forestry Research》 SCIE CAS CSCD 2003年第2期122-126,共5页
Allelochemicals of Chinese-fir root was extracted by technology ofsupercritical CO_2 extraction under orthogonal experiment design, and it was used to analyzeallelopathic activity of Chinese-fir through bioassay of se... Allelochemicals of Chinese-fir root was extracted by technology ofsupercritical CO_2 extraction under orthogonal experiment design, and it was used to analyzeallelopathic activity of Chinese-fir through bioassay of seed germination. The results showed thatas to the available rate of allelochemicals, the pressure and temperature of extraction were themost important factors. The allelochemicals of Chinese-fir root extracted by pure CO_2 and ethanolmixed with CO_2 have different allelopathic activities to seed germination, and the allelochemicalsextracted by ethanol mixed with CO_2 had stronger inhibitory effects on seed germination than thatextracted by pure CO_2. 展开更多
关键词 chinese fir autointoxication supercritical CO_2 extraction BIOASSAY SEEDGERMINATION
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Comparative study on yields and quality parameters of argan oils extracted by conventional and green extraction techniques
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作者 Hicham Mechqoq Mohamed El Yaagoubi +2 位作者 Svetlana Momchilova Fouad Msanda Noureddine El Aouad 《Grain & Oil Science and Technology》 2021年第3期125-130,共6页
Argan oil is most frequently sold as pure oil,which can be directly applied topically due to its cosmetological proprieties or ingested in order to provide several health benefits.It's also commonly mixed into a n... Argan oil is most frequently sold as pure oil,which can be directly applied topically due to its cosmetological proprieties or ingested in order to provide several health benefits.It's also commonly mixed into a number of cosmetic products like shampoos,soaps and conditioners.In this study we aimed to improve the argan oil extraction yield and quality parameters by comparing the effects of different extraction technologies.Argan kernel oils were extracted using four methods:mechanical cold press,Soxhlet extraction with n-hexane,supercritical fluid extraction(SFE),and enzyme assisted extraction with three different enzyme solutions cellulase(cellulast),pectinase(Pectinex)and a mixture of carbohydrase enzymes(Viscozyme®).The quality parameters was evaluated by determining the acid,peroxide and iodine values aswell as the extinction coefficients K_(232) and K_(270) as measures of conjugated dienes and trienes,respectively.The results showed that the highest yield(66.37%±3.3%)was obtained by enzyme assisted extraction using the carbohydrases enzymes mixture(Viscozyme®),followed by Soxhlet extraction(59.5%±3.1%)and pectinase extraction(52.03%±3.55%).All argan oils samples obtained by the different methods showed a good oxidation stability,with acid,peroxide and iodine values lower than 0.8 mg/g,15 meq/kg and 110 g/100 g according to the official argan oil norm,respectively.The results of argan oils quality parameters demonstrated that the enzyme extracted argan oils showed low oxidation,with the following quality parameters:acid values(0.4-0.6 mg/g),iodine values(95-100 g/100 g),dienes(K_(232)<2),trienes(K_(270)<0.35),and peroxide values(<1.5 meq/kg).The results proved that the enzyme assisted extraction method can be applied to improve the argan oil yield without affecting the oil quality.The enzyme extraction method may be a great alternative to solvent and cold press extractions for this eco-friendly processing approach. 展开更多
关键词 Argan oil Cold press Soxhlet extraction Supercritical fluid extraction Enzyme assisted extraction
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Extraction of betulin from bark of Betula platyphylla by supercritical carbon dioxide extraction 被引量:4
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作者 张玉红 于涛 王洋 《Journal of Forestry Research》 SCIE CAS CSCD 2003年第3期202-204,共3页
Betulin, which is a medicinal pentacyclic triterpene, is abundant in the bark of white birch (Betula platyphlly). The bark of birch was collected at Tayuan Forest Farm of Jiagedaqi, Heilongjiang Province in September ... Betulin, which is a medicinal pentacyclic triterpene, is abundant in the bark of white birch (Betula platyphlly). The bark of birch was collected at Tayuan Forest Farm of Jiagedaqi, Heilongjiang Province in September 2000. Supercritical fluid extraction (SFE) that is a new separation technology has been used for the processing pharmaceutical and natural products. In this paper, the extraction of betulin from the bark of birch by supercritical CO2 extraction was studied. The authors investigated and analyzed a few parameters such as modifier dosage, extraction pressure and extraction temperature. The optimal extrac-tion conditions showed that the modifier dosage used for per gram bark powder was 1.5 mL, the extraction pressure was at 20 Mpa, and the extraction temperature was at 55 C. The velocity of flow of liquid CO2 was at 10 kg/h. The pressure and tem-perature in separation vessel were at 5.5 Mpa and 50 C, respectively. 展开更多
关键词 Betula platyphlly BETULIN Supercritical CO2 extraction
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Optimal ultrasonic extraction condition and determination of polysaccharides in Tilia amurensis flowers 被引量:2
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作者 穆立蔷 刘立平 马大龙 《Journal of Forestry Research》 SCIE CAS CSCD 2010年第1期77-80,I0003,共5页
Seven extracting temperatures (25, 35, 45, 55, 65, 75, 85℃) and extracting time (30, 40, 50, 60, 70, 80, 90 min) were designed for selecting the optimal extracting time and extracting temperature for ultrasonic e... Seven extracting temperatures (25, 35, 45, 55, 65, 75, 85℃) and extracting time (30, 40, 50, 60, 70, 80, 90 min) were designed for selecting the optimal extracting time and extracting temperature for ultrasonic extraction of T. amurensis flowers. Polysaccharides from T. amurensis flowers were isolated and determined by spectrophotometry. Results show that the optimal ultrasonic temperature was 75℃ and ex tracting time 52 min. The content of polysaccharides in T. amurensis flowers measured by anthrone--H2SO4 colorimetry under 580 nm, was 9.74% with 0.47% of relative standard deviation (RSD, n=3). This study demonstrated that ultrasonic extraction method was simple, and the color of the treated samples was stable in 4 h. The average recovery value for the polysaccharides measured was 99.48%±1.01%, with 0.112% of RSD (n=3). 展开更多
关键词 best extracting condition POLYSACCHARIDES Tilia amurensis flowers ultrasonic extraction
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Deep eutectic solvents and alkaline extraction of protein from seabuckthorn seed meal: a comparison study 被引量:6
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作者 Junjie Lin Huan Xiang +2 位作者 Dongxiao Sun-Waterhouse Chun Cui Wei Wang 《Food Science and Human Wellness》 SCIE 2022年第4期1028-1035,共8页
Seabuckthorn seed meal(SSM) is a waste of oil extraction industry that rich in protein. In order to seek suitable protein extraction method, three different deep eutectic solvents(DESs)(including choline chlorideglyce... Seabuckthorn seed meal(SSM) is a waste of oil extraction industry that rich in protein. In order to seek suitable protein extraction method, three different deep eutectic solvents(DESs)(including choline chlorideglycerol, choline chloride-oxalic acid and choline chloride-urea) were developed for extracting protein from SSM and compared with alkaline. Result indicated that alkaline could effectively extract 56.9% protein from SSM and its protein content was 73.1%, higher than DES at 31.0%-41.4% and 64.3%-67.5%, respectively. However, compared to alkali, DES led to a product with less β-sheet, more β-turn, more essential amino acids, higher total amino acid content, especially choline chloride-urea which extracted protein showing an integrated and similar protein weight distribution compared to SSM. Also, this protein extracted chloride-urea showed a highest digestibility in vitro(by pepsin)(54.2%). These results indicated that choline chloride-urea extraction is better than alkaline extraction for SSM. 展开更多
关键词 Seabuckthorn seed meal Protein extraction Deep eutectic solvent Alkaline extraction and acid precipitation Amino acids
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Dynamic microwave-assisted extraction combined with liquid phase microextraction based on the solidification of a floating drop for the analysis of organochlorine pesticides in grains followed by GC 被引量:5
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作者 Guijie Li Xu Zhang +5 位作者 Tingting Liu Hongxiu Fan Hongcheng Liu Shangyu Li Dawei Wang Lan Ding 《Food Science and Human Wellness》 SCIE 2021年第3期375-382,共8页
A convenient,cost-effective and fast method using dynamic microwave-assisted extraction and liquid phase microextraction based on the solidification of a floating drop was proposed to analyze organochlorine pesticides... A convenient,cost-effective and fast method using dynamic microwave-assisted extraction and liquid phase microextraction based on the solidification of a floating drop was proposed to analyze organochlorine pesticides in grains including rice,maize and millet.Twelve samples can be processed simultaneously in the method.During the extraction process,10%acetonitrile-water solutions containing 110μL of n-hexadecane were used to extract organochlorine pesticides.Subsequently,1.0 g sodium chloride was placed in the extract,and then centrifuged and cooled.The n-hexadecane drops containing the analytes were solidifi ed and transferred for determination by gas chromatography-electron capture detector without any further filtration or cleaning process.Limits of detection for organochlorine pesticides were 0.97–1.01μg/kg and the RSDs were in the range of 2.6%–8.5%.The developed technology has succeeded in analyzing six real grains samples and the recoveries of the organochlorine pesticides were 72.2%–94.3%.Compared with the published extraction methods,the developed method was used to analyze organochlorine pesticides in grains,being more environmentally friendly,which is suitable for the daily determination of organochlorine pesticides. 展开更多
关键词 Dynamic microwave-assisted extraction Liquid phase microextraction Gas chromatography Organochlorine pesticides Grain
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A highly sensitive SPE-liquid/liquid extraction-RPLC analytical method for the determination of 6β-hydroxycortisol and cortisol in cancer patients' urine 被引量:3
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作者 Zhang Hong Fang Yu Li Ying Liang Aibin 《Journal of Medical Colleges of PLA(China)》 CAS 2010年第2期75-83,共9页
A highly sensitive SPE-liquid/liquid extraction RPLC method has been developed for the analysis of 6β-hydroxycortisol and cortisol in the urine of cancer patients. Methods: After SPE column purification and liquid-l... A highly sensitive SPE-liquid/liquid extraction RPLC method has been developed for the analysis of 6β-hydroxycortisol and cortisol in the urine of cancer patients. Methods: After SPE column purification and liquid-liquid extraction, the sample test solutions were analyzed with RPLC using a C18 analytical column. This improved analytical method has been validated for linearity, accuracy (recovery from urine), repeatability (within-day and between-day precision), specificity, sensitivity, and stability. This SPE-liquid/liquid extraction-RPLC is rapid, simple, accurate and reproducible. The technique is particularly useful for monitoring the CYP3A activity of cancer patients in clinical settings. The results are expressed as the ratio of 6β-hydroxycortisol to cortisol. Results: The CYP3A activity from a total of 153 samples was measured using this improved method. Considerable variation in the CYP3A activity of different cancer patients has been documented. Thus, personalized medical treatment based on the individual metabolic enzyme activity level is necessary. Conclusion: This new analytical method facilitates such individualized medical treatments. 展开更多
关键词 Solid phase extraction (SPE) Liquid/liquid extraction Reversed-phase high performance liquid chromatography (RPLC) CYP3A 6β-hydroxycortisol/cortisol Cancer
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ESPRIT-Based Feature Extraction of Helicopter Acoustic Signal
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作者 周忠来 栗苹 +1 位作者 郑链 施聚生 《Journal of Beijing Institute of Technology》 EI CAS 1999年第1期8-14,共7页
Aim To extract harmonic frequencies of helicopter acoustic signal as features for hel icopter identification. Methods Estimation of signal parameters via rotational invariance techniques(ESPRIT) was selected to ext... Aim To extract harmonic frequencies of helicopter acoustic signal as features for hel icopter identification. Methods Estimation of signal parameters via rotational invariance techniques(ESPRIT) was selected to extract harmonic frequencies from really measured helicopter acoustic signal and an algorithm based on the SVD TLS was used. Results ESPRIT correctly extracted harmonic frequencies of helicopter using the data of limited length under the variousflight conditions. Conclusion ESPRIT is an effective method of extracting harmonic frequencies and using harmonic frequencies of helicopter acoustic signal to recognize helicopter is feasible. 展开更多
关键词 HELICOPTER acoustic signal harmonic frequencies ESPRIT feature extraction
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Effect of Allelochemicals of Chinese-fir root extracted by supercritical CO2 extraction on Chinese fir 被引量:5
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作者 林思祖 曹光球 +1 位作者 杜玲 王爱萍 《Journal of Forestry Research》 SCIE CAS CSCD 2003年第2期122-126,185-186,共页
Allelochemicals of Chinese-fir root was extracted by technology of supercritical CO2 extraction under orthogonal experiment design, and it was used to analyze allelopathic activity of Chinese-fir through bioassay of s... Allelochemicals of Chinese-fir root was extracted by technology of supercritical CO2 extraction under orthogonal experiment design, and it was used to analyze allelopathic activity of Chinese-fir through bioassay of seed germination. The results showed that as to the available rate of allelochemicals, the pressure and temperature of extraction were the most important factors. The allelochemicals of Chinese-fir root extracted by pure CO2 and ethanol mixed with CO2 have different allelopathic activities to seed germination, and the allelochemicals extracted by ethanol mixed with CO2 had stronger inhibitory effects on seed germination than that extracted by pure CO2. 展开更多
关键词 Chinese fir Autointoxication Supercritical CO2 extraction BIOASSAY Seed germination
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